Acta Cryst. (2002). E58, m245-m247  [ doi:10.1107/S1600536802007237 ]

(4-tert-Butyl-2-methylthiosemicarbazido)(O-methyldithiophosphato)palladium(II)

M. Janca, J. Taraba and J. Príhoda

Online 11 May 2002

Key indicators

• Powder X-ray study
• T = 120 K
• Mean (C-C) = 0.009 Å
• R factor = 0.060
• wR factor = 0.110
• Data-to-parameter ratio = 16.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



WEIGH_01  Alert C Extra text has been found in the                              
          _refine_ls_weighting_scheme field. This should be in the              
          _refine_ls_weighting_details field.                                   
          Weighting scheme given as calc w = 1/[\s^2^(Fo^2^)+(0.0398P)^2^+3.35P 
          Weighting scheme identified as calc                                   


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check

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