(IUCr) Crystallography Journals Online checkcif report

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Acta Cryst. (2002). E58, m248-m250 [ doi:10.1107/S1600536802007468 ]

-Guanidinido-bis[(terpyridine)platinum(II)] tris(hexafluorophosphate) acetonitrile solvate

M. Kato, A. Toshikawa and S. Kishi

Online 11 May 2002

Key indicators

Single-crystal X-ray study
T = 296 K
Mean (C-C) = 0.020 Å
R factor = 0.058
wR factor = 0.174
Data-to-parameter ratio = 13.0

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_202  Alert C Isotropic non-H Atoms in Anion/Solvent       =          3

PLAT_321  Alert C Check Hybridisation of  C(17)  in solvent/ion           ?

PLAT_420  Alert C D-H Without Acceptor       N(5)   -   H(14)             ?

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     26
                   N2  -PT1 -N4  -C16     0.00  5.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     42
                   N4  -PT1 -N2  -C6   -115.00  5.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     43
                   N4  -PT1 -N2  -C10    61.00  5.00   1.555   1.555   1.555   1.555

PLAT_733  Alert C Torsion Calc     22.9(9), Rep     23.0(3) ....       3.00 s.u-Ratio
                     PT1 -N4  -C16 -N4     1.555   1.555   1.555   2.655

General Notes



ABSTM_02  The ratio of expected to reported Tmax/Tmin(RR) is > 2.00             
          Tmin and Tmax reported:      0.418     0.999                          
          Tmin and Tmax expected:      0.033     0.603                          
          RR =      7.713                                                       
          Please check that your absorption correction is appropriate.          


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 7 Alert Level C = Please check