# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' Template texray.inf' _shelx_refln_list_code 4 _shelx_F_calc_maximum 421.73 _exptl_crystal_F_000 1832.00 _reflns_d_resolution_high 0.7085 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 13.2736 _cell_length_b 13.5405 _cell_length_c 17.3572 _cell_angle_alpha 90.000 _cell_angle_beta 92.007 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 131067.05 81019.91 3219.95 o 2 0 0 32326.48 36837.95 1403.79 o 3 0 0 40128.14 47679.36 1071.86 o 4 0 0 10820.39 10711.35 281.39 o 5 0 0 6997.29 6938.70 213.38 o 6 0 0 2141.09 2165.17 116.76 o 7 0 0 6374.26 6042.67 214.13 o 8 0 0 31220.99 31769.35 1003.45 o 9 0 0 9889.66 9740.96 310.73 o 10 0 0 22127.48 23298.28 609.92 o 11 0 0 1980.30 2038.00 223.96 o 12 0 0 30.15 200.06 144.57 o 13 0 0 1707.55 1373.41 344.25 o 14 0 0 5717.68 4495.00 537.73 o 15 0 0 11338.29 11896.22 892.40 o 16 0 0 4946.51 4719.72 595.17 o 17 0 0 14.59 24.77 283.23 o 18 0 0 4047.56 4416.75 658.35 o 2 1 0 4049.90 4021.17 204.61 o 4 1 0 14520.65 15448.67 324.24 o 5 1 0 3574.37 3555.25 129.47 o 6 1 0 2631.12 2908.29 100.33 o 7 1 0 21635.20 20980.56 470.24 o 8 1 0 16410.32 16342.67 312.12 o 9 1 0 6408.25 6396.25 174.91 o 10 1 0 293.29 303.95 77.10 o 11 1 0 3330.60 3158.87 181.59 o 12 1 0 3720.16 3717.25 232.28 o 13 1 0 3078.99 2872.56 307.13 o 14 1 0 139.98 174.24 218.07 o 15 1 0 146.61 52.48 212.87 o 16 1 0 614.14 828.76 243.74 o 17 1 0 226.10 271.97 231.05 o 18 1 0 662.72 1096.77 312.40 o 0 2 0 85886.55 99449.70 3917.06 o 1 2 0 17811.53 20261.09 410.59 o 3 2 0 1208.84 1281.03 87.62 o 4 2 0 643.63 756.25 70.20 o 5 2 0 130.73 72.84 42.17 o 6 2 0 9937.93 9816.61 351.25 o 7 2 0 837.83 897.45 71.58 o 8 2 0 17994.33 17817.29 340.13 o 9 2 0 54242.39 55357.46 1000.63 o 10 2 0 28315.13 28559.32 546.78 o 11 2 0 13667.08 13244.33 332.39 o 12 2 0 3710.71 3501.22 189.82 o 13 2 0 976.34 866.57 230.15 o 14 2 0 1859.35 1947.39 289.75 o 15 2 0 0.24 25.01 176.79 o 16 2 0 49.54 -180.15 180.15 o 17 2 0 1055.19 889.23 274.35 o 18 2 0 3542.39 4211.96 455.00 o 1 3 0 5598.57 6542.49 168.29 o 2 3 0 88359.11 100230.13 2228.69 o 3 3 0 26793.27 28231.54 867.58 o 5 3 0 47690.14 48705.53 1082.78 o 6 3 0 1580.26 1573.01 95.06 o 7 3 0 10305.91 9884.74 392.95 o 8 3 0 16200.84 16513.17 377.85 o 9 3 0 2207.26 2066.24 102.12 o 10 3 0 791.59 663.08 117.59 o 11 3 0 2847.37 3192.17 158.48 o 12 3 0 352.16 359.10 153.75 o 13 3 0 4731.27 4249.83 357.96 o 14 3 0 2676.60 2389.51 438.12 o 15 3 0 1837.10 1757.07 300.10 o 16 3 0 68.58 -170.98 181.52 o 17 3 0 541.70 463.94 242.24 o 18 3 0 89.61 70.45 222.55 o 0 4 0 4306.17 4203.88 292.56 o 1 4 0 7.86 26.21 75.76 o 2 4 0 1168.32 1383.16 77.89 o 3 4 0 8606.33 8996.75 273.93 o 4 4 0 32123.34 34440.80 713.25 o 5 4 0 782.77 708.84 135.99 o 6 4 0 152.63 122.25 75.12 o 7 4 0 309.59 284.25 70.15 o 8 4 0 14891.32 14183.39 408.52 o 9 4 0 34064.73 33186.69 837.43 o 10 4 0 21207.83 20332.56 507.47 o 11 4 0 11226.62 10579.54 294.37 o 12 4 0 6715.65 6089.25 391.90 o 13 4 0 423.99 468.29 157.34 o 14 4 0 858.03 738.21 291.84 o 15 4 0 936.00 676.63 240.21 o 16 4 0 2040.78 2455.84 339.30 o 17 4 0 2245.04 2228.98 345.22 o 18 4 0 1179.79 1576.30 306.40 o 1 5 0 22735.22 23450.77 736.36 o 2 5 0 35987.61 36562.26 861.06 o 3 5 0 15913.62 16209.11 329.81 o 4 5 0 26754.10 26747.46 576.73 o 5 5 0 14382.67 14224.60 348.19 o 7 5 0 7199.48 6785.21 225.21 o 8 5 0 6562.83 6451.44 200.86 o 9 5 0 448.77 374.92 90.01 o 10 5 0 1323.06 1206.23 137.31 o 11 5 0 657.64 538.61 103.42 o 12 5 0 3155.30 2653.75 209.83 o 13 5 0 13847.55 14037.40 515.83 o 14 5 0 16594.68 15926.86 749.81 o 15 5 0 4340.13 3845.72 375.14 o 16 5 0 73.49 -139.02 198.17 o 17 5 0 5503.11 6169.71 507.11 o 0 6 0 15390.08 15540.46 762.09 o 1 6 0 19871.80 19661.43 646.37 o 2 6 0 20665.84 20834.01 537.69 o 3 6 0 18339.94 19172.69 443.82 o 4 6 0 3216.17 3049.02 125.51 o 5 6 0 47585.73 47801.43 991.50 o 6 6 0 40838.06 40923.24 864.39 o 7 6 0 12243.24 12181.95 734.81 o 8 6 0 124.97 90.57 100.05 o 9 6 0 4585.70 4274.13 287.22 o 10 6 0 4688.59 3953.23 196.58 o 11 6 0 8.82 -60.89 102.86 o 12 6 0 2119.07 2153.62 169.29 o 13 6 0 3234.13 3301.30 345.04 o 14 6 0 2519.45 2338.98 314.59 o 15 6 0 165.27 -100.67 189.33 o 16 6 0 32.03 284.72 224.47 o 17 6 0 214.06 329.16 241.41 o 1 7 0 8383.50 8306.75 362.51 o 2 7 0 20084.73 21579.71 725.52 o 3 7 0 13004.89 13076.71 388.55 o 4 7 0 36951.59 38428.58 823.66 o 5 7 0 19408.09 18519.43 394.67 o 6 7 0 804.21 648.99 96.67 o 7 7 0 1118.18 910.81 125.07 o 8 7 0 411.99 159.14 151.19 o 9 7 0 827.94 764.21 125.92 o 10 7 0 47.93 12.01 114.99 o 11 7 0 1858.29 1823.47 160.62 o 12 7 0 620.71 524.49 153.80 o 13 7 0 436.42 428.75 169.01 o 14 7 0 1891.63 1370.13 290.41 o 15 7 0 1199.41 894.40 252.39 o 16 7 0 675.88 327.94 240.62 o 17 7 0 396.74 416.69 224.26 o 0 8 0 39.59 -84.00 193.48 o 1 8 0 856.75 886.64 164.78 o 2 8 0 11715.16 11750.03 502.20 o 3 8 0 17965.61 18534.93 666.97 o 4 8 0 12065.16 11377.28 372.75 o 5 8 0 3257.26 3400.04 181.69 o 6 8 0 3246.31 3259.24 183.40 o 7 8 0 1161.81 968.42 132.74 o 8 8 0 1868.93 1688.46 128.89 o 9 8 0 1553.80 1609.65 158.59 o 10 8 0 813.00 895.21 144.78 o 11 8 0 383.67 382.73 131.04 o 12 8 0 9359.21 8941.33 379.37 o 13 8 0 4979.77 5310.50 326.66 o 14 8 0 68.93 343.24 204.24 o 15 8 0 2591.10 2302.61 326.10 o 16 8 0 2779.29 2945.19 370.05 o 1 9 0 21399.70 23133.28 806.99 o 2 9 0 40158.89 40876.86 1330.87 o 3 9 0 13657.30 13510.61 557.29 o 4 9 0 8074.27 7934.49 529.48 o 5 9 0 1112.76 1024.67 160.38 o 6 9 0 307.84 351.73 137.25 o 7 9 0 2226.87 1947.57 164.02 o 8 9 0 1569.06 1291.28 149.29 o 9 9 0 16.70 -31.06 110.56 o 10 9 0 781.02 794.91 120.02 o 11 9 0 625.95 448.18 169.17 o 12 9 0 1262.23 1389.15 198.32 o 13 9 0 442.95 502.19 235.46 o 14 9 0 62.67 227.10 196.09 o 15 9 0 339.03 -4.70 304.23 o 16 9 0 3110.72 3186.78 375.25 o 0 10 0 9733.87 8641.09 620.30 o 1 10 0 15686.13 14270.87 1318.67 o 2 10 0 97.20 58.37 182.77 o 3 10 0 7230.12 6469.29 390.26 o 4 10 0 14975.43 14329.86 603.34 o 5 10 0 4532.34 4223.92 318.08 o 6 10 0 5.94 -42.06 156.71 o 7 10 0 143.76 89.09 126.45 o 8 10 0 1609.91 1783.40 174.18 o 9 10 0 140.76 115.93 120.93 o 10 10 0 2115.77 2259.76 276.52 o 11 10 0 4473.76 4867.75 295.71 o 12 10 0 7893.16 7323.40 361.38 o 13 10 0 1307.52 1459.06 202.68 o 14 10 0 390.79 1089.29 240.13 o 15 10 0 3708.49 3793.94 387.31 o 1 11 0 3984.88 3662.76 319.92 o 2 11 0 2517.71 2614.74 284.97 o 3 11 0 3123.18 3013.00 300.44 o 4 11 0 375.02 175.75 202.83 o 5 11 0 190.91 391.94 292.92 o 6 11 0 8524.94 8347.55 462.75 o 7 11 0 35098.41 34941.87 1195.70 o 8 11 0 40644.30 40446.96 1058.49 o 9 11 0 6647.07 6537.79 288.93 o 10 11 0 377.79 281.05 135.86 o 11 11 0 8855.18 8636.45 403.95 o 12 11 0 13829.25 14262.73 576.24 o 13 11 0 6072.14 6454.35 343.26 o 14 11 0 1450.38 2552.27 518.35 o 15 11 0 287.29 485.70 182.65 o 0 12 0 7554.65 7602.23 645.43 o 1 12 0 611.06 567.88 230.38 o 2 12 0 364.45 639.68 235.05 o 3 12 0 351.67 534.25 225.44 o 4 12 0 3245.95 3204.54 319.24 o 5 12 0 4501.03 4150.48 353.45 o 6 12 0 4926.40 5048.81 382.19 o 7 12 0 414.57 538.05 235.45 o 8 12 0 57.43 313.89 214.81 o 9 12 0 579.99 943.43 242.36 o 10 12 0 1292.20 939.77 256.70 o 11 12 0 845.28 972.06 203.92 o 12 12 0 129.94 263.52 165.56 o 13 12 0 13.03 223.33 252.23 o 14 12 0 474.96 255.94 318.76 o 1 13 0 10164.97 10566.58 652.07 o 2 13 0 8289.96 8355.07 493.86 o 3 13 0 4660.53 4904.98 404.74 o 4 13 0 1697.38 1745.40 290.57 o 5 13 0 863.85 749.87 253.79 o 6 13 0 815.80 786.47 389.84 o 7 13 0 5995.35 5862.86 425.02 o 8 13 0 7932.96 8416.30 509.48 o 9 13 0 347.50 243.07 250.02 o 10 13 0 1017.65 927.30 269.33 o 11 13 0 3682.68 3955.88 360.21 o 12 13 0 1599.16 2005.49 282.63 o 13 13 0 79.80 475.99 291.84 o 0 14 0 8495.50 9185.29 736.60 o 1 14 0 947.30 816.83 274.43 o 2 14 0 322.72 266.78 248.38 o 3 14 0 3217.74 3573.67 365.24 o 4 14 0 2170.48 2238.50 324.89 o 5 14 0 29.34 -82.26 235.63 o 6 14 0 763.44 532.03 247.17 o 7 14 0 755.05 732.43 265.21 o 8 14 0 11.96 -166.73 199.69 o 9 14 0 106.98 108.16 304.05 o 10 14 0 53.46 287.53 404.56 o 11 14 0 570.54 533.71 229.37 o 12 14 0 769.64 1724.78 479.58 o 1 15 0 7323.38 7557.90 509.77 o 2 15 0 8955.37 8891.26 551.41 o 3 15 0 7661.33 7942.57 530.45 o 4 15 0 3536.04 3514.42 382.26 o 5 15 0 1696.34 1454.46 314.26 o 6 15 0 250.75 275.70 268.23 o 7 15 0 64.37 -222.14 234.28 o 8 15 0 467.10 314.96 271.38 o 9 15 0 113.42 37.75 245.17 o 10 15 0 310.36 826.70 433.99 o 11 15 0 1.36 0.15 206.12 o 0 16 0 2079.68 959.52 435.07 o 1 16 0 614.27 182.04 276.37 o 2 16 0 3767.06 3646.80 408.57 o 3 16 0 885.72 996.41 312.48 o 4 16 0 194.71 -241.33 256.65 o 5 16 0 4741.54 5540.10 471.68 o 6 16 0 9443.28 10577.56 624.74 o 7 16 0 1939.22 2110.42 351.85 o 8 16 0 7.82 -198.44 255.21 o 9 16 0 3890.27 4084.05 418.32 o 10 16 0 3143.72 2846.26 542.76 o 1 17 0 433.69 438.42 524.99 o 2 17 0 1571.99 1329.13 355.95 o 3 17 0 124.54 101.65 290.31 o 4 17 0 470.25 649.97 468.09 o 5 17 0 1499.32 987.00 327.31 o 6 17 0 1689.32 1404.81 358.93 o 7 17 0 2266.29 2033.76 415.69 o 8 17 0 1657.42 2137.45 357.43 o 0 18 0 398.80 339.58 478.51 o 1 18 0 35.14 50.35 335.10 o 2 18 0 719.91 894.82 364.79 o 3 18 0 2133.22 2367.54 423.29 o 4 18 0 1251.21 1214.77 370.20 o 5 18 0 124.61 -159.68 296.95 o 6 18 0 160.99 104.64 429.69 o 1 19 0 191.22 -114.44 336.40 o -18 1 1 876.46 1395.20 326.29 o -17 1 1 490.07 402.10 230.47 o -16 1 1 7340.22 7106.38 486.73 o -15 1 1 15667.19 14489.89 709.07 o -14 1 1 9541.25 9191.73 535.81 o -13 1 1 561.69 411.85 208.90 o -12 1 1 922.50 795.71 221.20 o -11 1 1 1611.51 1735.29 124.78 o -10 1 1 2988.43 3153.07 127.78 o -9 1 1 5981.43 6016.17 169.62 o -8 1 1 5511.49 5686.44 158.16 o -7 1 1 98.86 90.19 56.64 o -6 1 1 30758.37 31255.57 566.91 o -5 1 1 526.82 542.24 59.40 o -4 1 1 414.51 385.16 53.66 o -3 1 1 7131.65 7573.54 162.33 o -2 1 1 12797.71 14131.19 256.32 o 0 1 1 177857.13 205127.89 8047.71 o 2 1 1 123.59 259.69 35.64 o 3 1 1 69788.37 78302.52 1380.37 o 4 1 1 94875.83 102906.63 2016.02 o 5 1 1 15137.28 14583.02 519.03 o 6 1 1 15040.37 14342.69 530.27 o 7 1 1 1799.49 2072.03 89.50 o 8 1 1 13672.89 13884.54 296.27 o 9 1 1 12434.58 12208.00 254.08 o 10 1 1 15860.60 14372.05 337.38 o 11 1 1 695.07 843.20 134.99 o 12 1 1 10155.25 9943.71 362.22 o 13 1 1 10105.60 9014.36 411.89 o 14 1 1 2394.40 2121.57 443.69 o 15 1 1 611.56 334.55 212.78 o 16 1 1 351.91 676.31 233.23 o 17 1 1 68.76 65.86 210.55 o 18 1 1 3597.37 3695.82 433.58 o -18 2 1 1521.97 1834.04 538.63 o -17 2 1 23.13 175.45 226.67 o -16 2 1 462.33 424.49 224.25 o -15 2 1 223.67 243.03 212.85 o -14 2 1 199.60 301.96 213.33 o -13 2 1 775.18 773.89 226.64 o -12 2 1 6700.84 6528.90 310.10 o -11 2 1 3553.57 3520.19 209.40 o -10 2 1 7736.47 8157.56 209.32 o -9 2 1 6872.24 6893.71 186.53 o -8 2 1 10410.42 10228.94 239.02 o -7 2 1 45327.37 49416.87 878.38 o -6 2 1 12272.75 13485.03 276.92 o -5 2 1 4505.05 4542.94 163.17 o -4 2 1 58170.50 59014.40 1625.31 o -2 2 1 3347.31 3167.90 107.51 o 0 2 1 37385.04 43593.02 826.06 o 1 2 1 3.61 160.79 50.69 o 2 2 1 33768.85 39946.75 2408.86 o 3 2 1 46.45 250.27 74.82 o 4 2 1 14265.04 15863.75 345.14 o 6 2 1 26.87 33.63 22.69 o 7 2 1 16448.18 16431.71 333.87 o 8 2 1 37397.09 37821.61 637.87 o 9 2 1 29875.22 28459.21 990.15 o 10 2 1 803.32 720.97 112.91 o 11 2 1 4796.46 5006.30 235.36 o 12 2 1 3898.40 3642.26 220.62 o 13 2 1 970.88 1022.93 199.40 o 14 2 1 349.15 223.11 199.14 o 15 2 1 1247.87 1605.20 287.63 o 16 2 1 449.29 398.89 226.79 o 17 2 1 16.88 -150.53 201.43 o 18 2 1 212.89 26.19 400.07 o -18 3 1 516.67 662.15 266.34 o -17 3 1 354.40 316.61 237.52 o -16 3 1 27.01 -66.43 203.02 o -15 3 1 9.90 108.59 205.51 o -14 3 1 1.50 88.40 197.84 o -13 3 1 261.16 139.95 198.29 o -12 3 1 7863.51 7402.25 364.65 o -11 3 1 17337.49 16364.85 439.95 o -10 3 1 31448.51 31307.69 613.92 o -9 3 1 23046.04 23592.94 520.42 o -8 3 1 6695.00 7016.18 255.14 o -7 3 1 4544.52 4627.26 168.96 o -6 3 1 72183.39 73756.84 1681.99 o -4 3 1 19880.43 19544.68 423.35 o -3 3 1 3755.49 3874.46 139.96 o -2 3 1 17308.10 18652.85 349.13 o -1 3 1 1675.44 2104.20 168.70 o 0 3 1 981.91 1113.02 73.84 o 1 3 1 662.31 951.42 112.08 o 2 3 1 8972.08 8985.41 619.16 o 3 3 1 2958.72 3099.25 181.09 o 4 3 1 324.92 308.72 68.01 o 5 3 1 60.45 64.76 65.89 o 6 3 1 1000.95 1008.97 113.27 o 7 3 1 122.45 71.11 56.18 o 8 3 1 13971.66 13993.99 282.29 o 9 3 1 31756.90 30810.13 543.25 o 10 3 1 40331.84 39470.02 859.09 o 11 3 1 7927.13 7679.79 269.97 o 12 3 1 1478.33 1599.50 153.58 o 13 3 1 4179.98 4269.79 277.07 o 14 3 1 8761.83 8057.14 499.79 o 15 3 1 8369.77 7983.33 514.18 o 16 3 1 3496.01 4046.83 536.66 o 17 3 1 2855.06 2434.08 347.29 o 18 3 1 1852.46 1889.96 347.23 o -18 4 1 1009.08 1327.87 845.55 o -17 4 1 3051.82 3379.34 399.82 o -16 4 1 975.84 777.21 246.36 o -15 4 1 1727.95 1992.32 320.40 o -14 4 1 7060.25 6984.33 476.66 o -13 4 1 11885.91 10995.53 578.88 o -12 4 1 1031.53 1122.98 140.43 o -11 4 1 5188.61 5163.76 200.12 o -10 4 1 25970.83 25994.77 518.45 o -9 4 1 9005.95 8602.39 230.67 o -8 4 1 33.94 58.40 53.03 o -7 4 1 5329.73 5183.13 203.16 o -6 4 1 2940.08 2763.46 113.32 o -5 4 1 22178.42 22756.98 497.13 o -4 4 1 11049.60 11385.09 280.93 o -3 4 1 2042.90 1994.45 87.77 o -2 4 1 59336.55 64345.45 1118.10 o -1 4 1 64402.43 69060.73 1541.88 o 0 4 1 27995.06 28644.83 575.47 o 1 4 1 23306.72 24945.88 600.28 o 2 4 1 14751.54 15307.66 419.46 o 3 4 1 969.64 835.09 104.14 o 4 4 1 6383.99 7377.00 231.19 o 5 4 1 61002.10 61871.41 1239.09 o 6 4 1 6546.99 6632.79 233.58 o 7 4 1 4918.74 4954.04 306.92 o 8 4 1 5094.38 4561.60 173.87 o 9 4 1 3584.02 3275.99 139.75 o 10 4 1 0.43 54.97 94.59 o 11 4 1 12.40 -18.26 90.72 o 12 4 1 1422.49 876.56 298.86 o 13 4 1 10894.19 8955.82 1118.22 o 14 4 1 12174.14 10957.97 596.49 o 15 4 1 4658.52 4615.83 399.23 o 16 4 1 240.58 279.94 209.89 o 17 4 1 4570.10 4940.12 513.15 o 18 4 1 5606.66 6151.44 964.19 o -18 5 1 110.10 237.28 297.23 o -17 5 1 49.25 14.19 216.04 o -16 5 1 86.42 0.62 213.80 o -15 5 1 357.60 -2.36 199.94 o -14 5 1 4410.95 4390.71 387.94 o -13 5 1 1961.48 1743.92 277.21 o -12 5 1 3930.29 4066.60 211.40 o -11 5 1 2803.14 2507.56 194.35 o -10 5 1 935.37 766.24 176.62 o -9 5 1 297.30 185.19 88.88 o -8 5 1 4802.01 5037.37 178.04 o -7 5 1 1368.71 1149.53 96.81 o -6 5 1 3908.24 3693.90 165.48 o -5 5 1 319.79 368.69 103.53 o -4 5 1 9632.30 9388.32 238.84 o -3 5 1 8516.47 8679.07 205.96 o -2 5 1 55748.20 59384.63 1187.68 o -1 5 1 6936.13 7190.63 237.05 o 0 5 1 1587.63 1775.63 154.97 o 1 5 1 1462.68 1321.60 107.16 o 2 5 1 16338.21 18164.62 471.17 o 3 5 1 2285.71 2158.45 140.86 o 4 5 1 15674.65 16044.03 464.54 o 5 5 1 8.11 -49.38 74.32 o 6 5 1 50195.16 51285.91 1052.74 o 7 5 1 38450.55 37545.91 868.86 o 8 5 1 6054.76 5744.70 236.41 o 9 5 1 293.40 287.22 107.50 o 10 5 1 91.14 141.84 100.73 o 11 5 1 44.07 -53.79 94.44 o 12 5 1 21.95 37.92 118.96 o 13 5 1 305.39 330.78 161.29 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