(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, m331-m333 [ doi:10.1107/S1600536802010140 ]

Bis[2-(1-methyl-1H-imidazol-2-yl-3-iosulfanyl)-6-(1-methyl-1H-imidazol-2-ylsulfanyl)pyridine] tetrachloroferrate tetrafluoroborate

G. R. Lewis, P. Hubberstey and C. L. Sampson

Online 14 June 2002

Key indicators

Single-crystal X-ray study
T = 150 K
Mean (C-C) = 0.006 Å
R factor = 0.049
wR factor = 0.095
Data-to-parameter ratio = 18.5

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level A:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           29.04                 
         From the CIF: _reflns_number_total               8426                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns        10005                           
         Completeness (_total/calc)             84.22%                          
          Alert A: < 85% complete (theta max?)                                  


 1 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 0 Alert Level C = Please check