(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, o738-o739 [ doi:10.1107/S1600536802010176 ]

Ethyl N-(5-bromo-3-phenylindol-2-yl)carbamate

B. H. M. Mruthyunjayaswamy, O. B. Ijare, Y. Jadegoud, A. Ray Chaudhuri and T. N. Guru Row

Online 14 June 2002

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.004 Å
R factor = 0.037
wR factor = 0.084
Data-to-parameter ratio = 16.8

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.43                 
         From the CIF: _reflns_number_total               6698                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         7145                           
         Completeness (_total/calc)             93.74%                          
          Alert C: < 95% complete                                               

PLAT_420  Alert C D-H Without Acceptor       N(4)   -   H(4A)             ?

PLAT_725  Alert C D-H     Calc     0.96991, Rep     0.98000, Dev.      0.01 Ang.
                     C33  -H33B    1.555   1.555


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 3 Alert Level C = Please check