Acta Cryst. (2002). E58, m344-m346  [ doi:10.1107/S160053680201036X ]

Ring contraction in a dinuclear zinc(II) complex of a Robson macrocycle

W. Wongratchasee, S. Chantrapromma, H.-K. Fun, A. Usman, C. Karalai, C. Ponglimanont and K. Chantrapromma

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.005 Å
• Disorder in solvent or counterion
• R factor = 0.056
• wR factor = 0.154
• Data-to-parameter ratio = 19.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_302  Alert C Anion/Solvent Disorder .......................      36.00 Perc.


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check

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