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Acta Cryst. (2002). E58, m363-m365  [ doi:10.1107/S1600536802010838 ]

Tris[bis(diphenylphosphino)methane-[kappa]2P,P']rhenium(I) perrhenate

K. H. Whitmire, D. R. Derringer and K. R. Kongkasuwan

Online 29 June 2002

Key indicators

checkCIF results

No syntax errors found

GLOBAL _publ field problems





Red Alert Alert Level A:


PUBL_003  Alert A The contact author's name is missing,                         
           _publ_contact_author_name.                                            

ADDSYM reports no extra symmetry


Red Alert Alert Level A:



ABSTM_02  Alert A The ratio of Tmax/Tmin expected RT(exp) is > 1.30             
          An absorption correction should be applied.                           
          Tmin and Tmax expected:      0.325     0.457                          
          RT(exp) =      1.406
Author response: We measured psi scans for this crystal and found them to be flat so no correction was applied. 
THETM_01  Alert A The value of sine(theta_max)/wavelength is less than 0.550    
          Calculated sin(theta_max)/wavelength =    0.4813
Author response: The crystal was weakly diffracting. We have refined the structure so as to maintain a high data to parameter ratio. The structure is quite reasonable and refines will with acceptable residuals. Part of the weakness of the data can be attributed to the disorder that is observed. 
General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           20.00                 
         From the CIF: _reflns_number_total               5937                  
         From the CIF: _diffrn_reflns_limit_ max hkl    0.   36.   16.          
         From the CIF: _diffrn_reflns_limit_ min hkl  -17.    0.    0.          
         TEST1: Expected hkl limits for theta max                               
         Calculated maximum hkl   17.   36.   18.                               
         Calculated minimum hkl  -17.  -36.  -18.                               
          ALERT: Expected hkl max differ from CIF values                        


 3 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 0 Alert Level C = Please check

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