# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' sm0300 DN6034 C13 H7 N3 O3 Se1 Br2 in space group Pbca' _shelx_refln_list_code 4 _shelx_F_calc_maximum 377.77 _exptl_crystal_F_000 1872.00 _reflns_d_resolution_high 0.8011 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' _cell_length_a 13.8685 _cell_length_b 8.6075 _cell_length_c 25.2330 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7486.24 7772.00 56.47 o 4 0 0 2378.30 2283.24 45.55 o 6 0 0 1992.96 1777.84 37.21 o 8 0 0 84236.39 88562.75 910.96 o 10 0 0 5328.11 6016.00 219.14 o 12 0 0 196.60 248.57 24.59 o 14 0 0 1925.59 2039.82 70.16 o 16 0 0 953.71 1087.62 36.69 o 2 1 0 10281.36 9960.14 240.75 o 4 1 0 11822.64 13143.08 117.10 o 6 1 0 3488.89 3126.37 124.09 o 8 1 0 1513.44 1372.80 218.89 o 10 1 0 6.52 -18.93 40.28 o 12 1 0 670.98 748.07 37.63 o 14 1 0 106.45 91.00 24.45 o 16 1 0 150.50 160.14 22.28 o 0 2 0 7679.10 7052.06 83.27 o 2 2 0 54050.62 57719.93 460.70 o 4 2 0 8364.93 8838.93 102.88 o 6 2 0 9879.86 11412.66 464.69 o 8 2 0 19918.25 21683.32 467.21 o 10 2 0 4603.89 4631.28 134.40 o 12 2 0 6.77 54.19 19.42 o 14 2 0 89.96 103.50 23.50 o 16 2 0 26.84 4.07 17.38 o 2 3 0 110778.20 114835.53 1845.49 o 4 3 0 28389.16 30827.03 409.75 o 6 3 0 75511.45 80384.31 2946.07 o 8 3 0 6668.40 6815.11 338.81 o 10 3 0 5426.62 5395.71 149.85 o 12 3 0 3.19 -18.20 47.94 o 14 3 0 1753.35 1599.36 53.70 o 16 3 0 520.50 610.61 26.36 o 0 4 0 6149.08 6255.74 224.94 o 2 4 0 13101.71 14477.40 218.29 o 4 4 0 281.85 226.72 15.89 o 6 4 0 10940.42 10762.88 237.01 o 8 4 0 462.37 550.06 28.53 o 10 4 0 567.17 540.44 33.69 o 12 4 0 23.73 34.90 22.82 o 14 4 0 2206.69 2247.67 66.23 o 16 4 0 20.27 19.83 11.41 o 2 5 0 32170.36 31228.63 377.80 o 4 5 0 30979.01 31383.50 407.56 o 6 5 0 22390.40 22392.60 384.57 o 8 5 0 3.18 -38.98 54.33 o 10 5 0 2598.79 2637.18 79.70 o 12 5 0 16.98 -24.18 46.18 o 14 5 0 846.53 889.70 38.32 o 0 6 0 23612.56 24156.41 382.34 o 2 6 0 9724.49 9942.21 250.79 o 4 6 0 191.33 193.97 19.02 o 6 6 0 6.81 31.10 15.75 o 8 6 0 3444.96 3306.50 102.19 o 10 6 0 2012.15 1973.83 62.82 o 12 6 0 532.16 574.01 32.47 o 14 6 0 576.67 771.82 27.86 o 2 7 0 3122.93 3009.16 93.06 o 4 7 0 3014.41 2815.88 89.51 o 6 7 0 539.43 599.80 32.20 o 8 7 0 80.05 86.52 23.90 o 10 7 0 538.00 501.45 33.83 o 12 7 0 1656.72 1592.07 47.46 o 0 8 0 12191.37 13926.96 339.19 o 2 8 0 7204.94 7583.12 186.80 o 4 8 0 2135.05 2003.45 59.42 o 6 8 0 1236.90 1356.38 49.34 o 8 8 0 3147.32 3008.96 86.95 o 10 8 0 174.72 130.67 20.65 o 2 9 0 133.79 142.21 22.28 o 4 9 0 5.68 -4.89 16.84 o 6 9 0 373.95 373.31 26.22 o 8 9 0 581.49 529.10 28.40 o 0 10 0 1990.99 2193.14 64.19 o 2 10 0 413.34 561.08 30.02 o 4 10 0 93.89 74.16 16.84 o 6 10 0 486.60 455.87 22.69 o 1 1 1 15582.31 15409.57 172.51 o 2 1 1 7329.31 6691.40 61.52 o 3 1 1 1995.89 1909.51 67.01 o 4 1 1 20637.20 21730.58 146.82 o 5 1 1 48459.56 51229.63 1101.88 o 6 1 1 2264.77 2418.92 44.30 o 7 1 1 3099.76 3256.07 94.40 o 8 1 1 13380.87 14797.25 240.97 o 9 1 1 1070.27 1208.29 80.93 o 10 1 1 31363.55 33046.90 1812.69 o 11 1 1 713.26 768.21 36.01 o 12 1 1 128.13 108.66 23.23 o 13 1 1 8335.04 8385.09 202.87 o 14 1 1 667.77 755.01 39.94 o 15 1 1 3033.79 3166.41 91.16 o 16 1 1 2570.98 2552.48 84.08 o 17 1 1 14.33 -0.68 11.41 o 0 2 1 766.97 920.81 20.86 o 1 2 1 30077.62 27874.79 1263.12 o 2 2 1 21153.19 21249.07 309.26 o 3 2 1 4218.66 4661.25 108.49 o 4 2 1 18175.30 18413.34 149.00 o 5 2 1 1423.59 1421.35 27.50 o 6 2 1 465.35 417.06 16.58 o 7 2 1 11105.35 11637.79 609.89 o 8 2 1 14778.47 15890.93 1033.85 o 9 2 1 2688.93 2869.67 147.60 o 10 2 1 16589.72 16595.86 357.43 o 11 2 1 1013.12 951.78 41.18 o 12 2 1 6715.34 6669.59 178.16 o 13 2 1 1140.72 1167.38 49.88 o 14 2 1 2602.54 2376.05 73.86 o 15 2 1 1442.40 1487.95 46.76 o 16 2 1 1725.61 1695.16 53.03 o 17 2 1 707.17 690.86 27.05 o 1 3 1 1759.80 1840.75 50.89 o 2 3 1 4125.65 3955.45 71.06 o 3 3 1 1025.14 1072.33 70.21 o 4 3 1 236.97 203.49 36.13 o 5 3 1 3.45 52.05 10.80 o 6 3 1 251.13 322.95 13.73 o 7 3 1 1586.89 1879.84 48.06 o 8 3 1 5257.82 5564.02 424.90 o 9 3 1 333.39 316.35 17.37 o 10 3 1 383.06 425.06 29.75 o 11 3 1 1696.13 1720.88 55.06 o 12 3 1 703.19 654.20 39.81 o 13 3 1 3331.35 3312.12 88.58 o 14 3 1 3.38 0.00 47.94 o 15 3 1 189.00 238.93 21.46 o 16 3 1 735.44 772.70 31.12 o 0 4 1 202.10 248.45 8.88 o 1 4 1 1246.67 1278.39 27.30 o 2 4 1 7237.65 6926.15 158.84 o 3 4 1 14973.67 16548.95 248.70 o 4 4 1 13010.05 13952.86 239.18 o 5 4 1 2316.22 2469.02 76.04 o 6 4 1 2748.73 2829.08 88.30 o 7 4 1 5147.85 5177.60 127.52 o 8 4 1 601.94 552.69 29.21 o 9 4 1 4942.07 4911.74 141.50 o 10 4 1 1667.99 1665.12 52.61 o 11 4 1 3469.37 3425.33 105.46 o 12 4 1 8065.92 7862.54 191.12 o 13 4 1 102.63 90.46 23.63 o 14 4 1 3803.02 3605.22 114.76 o 15 4 1 1283.93 1327.18 42.96 o 16 4 1 1650.76 1537.94 50.20 o 1 5 1 1284.68 1278.31 33.17 o 2 5 1 1157.70 1199.35 41.59 o 3 5 1 175.55 214.48 16.98 o 4 5 1 7274.33 6994.45 194.01 o 5 5 1 513.20 725.07 29.35 o 6 5 1 2044.25 1949.25 58.74 o 7 5 1 913.84 948.48 37.37 o 8 5 1 1804.47 1667.99 50.30 o 9 5 1 2002.14 1969.17 62.27 o 10 5 1 3049.59 3021.19 84.62 o 11 5 1 0.02 36.40 18.88 o 12 5 1 5.50 23.77 41.02 o 13 5 1 1040.97 944.65 41.45 o 14 5 1 400.11 383.65 28.80 o 15 5 1 442.10 464.26 22.01 o 0 6 1 709.94 599.06 28.26 o 1 6 1 201.16 264.06 22.68 o 2 6 1 284.22 366.90 26.35 o 3 6 1 1244.55 1233.01 38.74 o 4 6 1 222.95 302.50 23.91 o 5 6 1 150.09 147.37 21.19 o 6 6 1 3677.83 3436.47 115.00 o 7 6 1 1037.67 993.10 40.77 o 8 6 1 700.40 642.52 34.92 o 9 6 1 930.51 839.63 41.72 o 10 6 1 562.79 575.76 38.18 o 11 6 1 1820.63 1661.67 55.06 o 12 6 1 1526.09 1534.52 51.11 o 13 6 1 6.73 33.55 14.40 o 14 6 1 1665.05 1607.03 45.43 o 1 7 1 267.24 313.92 27.85 o 2 7 1 343.73 423.96 30.84 o 3 7 1 55.92 91.13 18.47 o 4 7 1 1763.38 1773.42 50.16 o 5 7 1 532.91 618.41 32.47 o 6 7 1 1011.68 1016.32 40.77 o 7 7 1 447.16 449.39 31.52 o 8 7 1 3231.90 3087.02 96.06 o 9 7 1 28.25 22.68 39.52 o 10 7 1 2046.69 1862.94 57.11 o 11 7 1 304.49 278.75 25.95 o 12 7 1 73.83 71.17 17.93 o 13 7 1 1020.72 1016.51 31.13 o 0 8 1 1203.95 1260.24 49.74 o 1 8 1 806.79 804.52 40.63 o 2 8 1 938.91 962.06 48.51 o 3 8 1 1039.87 1110.38 47.56 o 4 8 1 27.68 71.03 18.34 o 5 8 1 453.78 420.32 31.92 o 6 8 1 55.87 34.91 21.87 o 7 8 1 360.05 325.07 29.21 o 8 8 1 201.92 173.05 25.13 o 9 8 1 82.99 114.91 16.98 o 10 8 1 95.98 70.63 17.79 o 11 8 1 132.26 196.95 17.79 o 1 9 1 82.47 109.74 19.69 o 2 9 1 3.66 55.82 15.89 o 3 9 1 127.96 142.48 22.68 o 4 9 1 268.81 269.36 24.72 o 5 9 1 420.49 431.05 28.12 o 6 9 1 122.19 123.33 20.78 o 7 9 1 409.74 390.44 29.07 o 8 9 1 1154.00 1194.05 39.69 o 9 9 1 0.19 9.10 24.85 o 0 10 1 197.65 186.09 22.41 o 1 10 1 0.83 0.00 26.35 o 2 10 1 374.21 460.67 27.31 o 3 10 1 5.64 16.03 14.53 o 4 10 1 330.68 297.92 20.79 o 5 10 1 34.72 29.74 13.17 o 6 10 1 2.18 -11.95 11.95 o 0 0 2 11557.95 11658.19 51.14 o 1 0 2 734.87 1119.98 100.88 o 2 0 2 9704.75 9821.07 72.20 o 3 0 2 76574.19 81434.10 681.25 o 4 0 2 15254.92 15716.56 263.06 o 5 0 2 142707.16 149464.11 4493.27 o 6 0 2 569.13 558.31 18.82 o 7 0 2 499.66 671.52 17.19 o 8 0 2 5358.57 5519.12 94.91 o 9 0 2 14089.16 15057.61 523.71 o 10 0 2 11557.19 12422.68 653.59 o 11 0 2 7451.63 7596.78 180.43 o 12 0 2 7215.35 7390.35 184.89 o 13 0 2 3432.27 4065.75 113.89 o 14 0 2 2720.44 2952.48 96.03 o 15 0 2 15.10 29.74 19.15 o 16 0 2 572.04 553.25 27.72 o 17 0 2 277.67 236.11 16.85 o 1 1 2 725.70 659.61 14.23 o 2 1 2 18475.56 18188.85 289.23 o 3 1 2 43409.20 43243.15 551.97 o 4 1 2 4.12 25.38 14.33 o 5 1 2 27654.61 28803.73 327.08 o 6 1 2 3974.58 4273.76 83.77 o 7 1 2 11438.58 12164.70 450.10 o 8 1 2 5433.12 6205.53 395.43 o 9 1 2 105.43 114.40 33.89 o 10 1 2 1013.44 963.83 136.17 o 11 1 2 3342.24 3513.16 101.78 o 12 1 2 139.74 183.77 22.41 o 13 1 2 114.34 107.03 29.20 o 14 1 2 255.94 222.09 28.80 o 15 1 2 17.09 -6.79 48.89 o 16 1 2 407.93 445.73 28.80 o 17 1 2 124.75 126.32 14.40 o 0 2 2 5017.70 4738.69 61.12 o 1 2 2 1350.53 1517.77 32.73 o 2 2 2 25672.38 25961.20 965.28 o 3 2 2 57788.45 57174.09 756.17 o 4 2 2 2838.23 3011.25 79.47 o 5 2 2 49406.94 51971.49 705.36 o 6 2 2 25.97 52.03 15.89 o 7 2 2 554.36 728.79 55.98 o 8 2 2 2096.64 2218.09 89.83 o 9 2 2 232.78 275.35 16.40 o 10 2 2 2352.20 2357.94 68.95 o 11 2 2 3538.97 3534.44 102.88 o 12 2 2 1036.13 1018.92 43.76 o 13 2 2 729.20 791.58 44.70 o 14 2 2 1871.99 1799.02 60.09 o 15 2 2 28.33 124.27 20.51 o 16 2 2 269.49 244.65 24.18 o 1 3 2 38268.19 37181.44 281.86 o 2 3 2 3716.93 3568.46 182.50 o 3 3 2 55193.82 55909.23 687.14 o 4 3 2 3154.59 3099.35 83.81 o 5 3 2 25587.64 26782.40 917.09 o 6 3 2 18113.88 19224.51 799.42 o 7 3 2 11338.01 12205.25 616.89 o 8 3 2 3983.80 3867.01 284.20 o 9 3 2 2230.95 2270.51 177.67 o 10 3 2 237.36 181.07 24.31 o 11 3 2 14124.32 13766.06 350.78 o 12 3 2 832.73 850.86 43.75 o 13 3 2 139.64 181.46 26.35 o 14 3 2 260.66 291.78 29.20 o 15 3 2 7.05 21.87 16.30 o 16 3 2 986.87 1021.19 34.25 o 0 4 2 17.97 87.45 7.28 o 1 4 2 306.91 301.66 70.78 o 2 4 2 1951.86 1987.67 65.02 o 3 4 2 1553.10 1608.28 47.32 o 4 4 2 802.38 863.32 26.63 o 5 4 2 2277.38 2194.17 73.04 o 6 4 2 836.93 874.43 30.17 o 7 4 2 567.02 555.67 27.99 o 8 4 2 45.67 0.00 43.87 o 9 4 2 797.23 778.03 35.74 o 10 4 2 749.14 704.76 37.36 o 11 4 2 30.32 -43.87 57.99 o 12 4 2 563.07 530.25 39.53 o 13 4 2 182.54 201.16 26.22 o 14 4 2 34.34 35.86 20.37 o 15 4 2 129.43 64.38 18.34 o 16 4 2 573.30 567.22 23.65 o 1 5 2 26188.96 25783.60 337.17 o 2 5 2 68.83 96.84 16.03 o 3 5 2 7648.65 7166.21 197.63 o 4 5 2 5712.59 5513.47 126.21 o 5 5 2 2889.60 2842.41 95.51 o 6 5 2 1921.76 1879.49 52.08 o 7 5 2 10875.58 10596.48 280.00 o 8 5 2 3639.84 3627.06 100.98 o 9 5 2 11708.06 11257.55 312.32 o 10 5 2 933.66 903.09 44.84 o 11 5 2 426.39 409.99 33.83 o 12 5 2 87.30 79.05 24.72 o 13 5 2 90.12 19.69 49.71 o 14 5 2 760.86 773.88 36.01 o 15 5 2 24.16 22.55 12.50 o 0 6 2 3854.51 3595.42 114.48 o 1 6 2 157.56 183.37 20.37 o 2 6 2 2204.67 2419.03 67.04 o 3 6 2 9830.85 10132.42 270.32 o 4 6 2 724.23 700.69 32.07 o 5 6 2 7191.27 7150.85 164.87 o 6 6 2 220.32 244.09 24.99 o 7 6 2 152.58 241.77 23.36 o 8 6 2 1418.00 1261.47 45.94 o 9 6 2 650.69 623.61 37.09 o 10 6 2 158.18 136.64 25.40 o 11 6 2 47.62 49.85 22.00 o 12 6 2 1067.33 997.95 40.50 o 13 6 2 89.72 127.13 21.19 o 14 6 2 1173.62 1146.00 33.17 o 1 7 2 4724.48 4788.74 147.88 o 2 7 2 104.62 193.96 20.92 o 3 7 2 356.38 394.21 30.02 o 4 7 2 30.44 19.69 19.01 o 5 7 2 833.59 866.08 36.96 o 6 7 2 199.85 205.10 23.09 o 7 7 2 992.75 983.70 43.35 o 8 7 2 4.36 -39.66 44.28 o 9 7 2 1795.86 1692.77 55.33 o 10 7 2 0.08 2.72 15.75 o 11 7 2 0.16 13.99 16.03 o 12 7 2 2.49 29.34 13.45 o 13 7 2 376.69 425.13 22.01 o 0 8 2 1764.27 1793.67 58.46 o 1 8 2 178.24 206.05 27.84 o 2 8 2 183.17 221.54 25.94 o 3 8 2 7145.45 8007.26 192.66 o 4 8 2 21.58 15.75 51.61 o 5 8 2 5953.34 5642.24 154.11 o 6 8 2 87.96 14.53 51.20 o 7 8 2 341.31 233.65 27.71 o 8 8 2 242.53 242.06 24.59 o 9 8 2 0.15 15.62 15.21 o 10 8 2 501.10 526.75 29.75 o 11 8 2 286.41 298.73 21.06 o 1 9 2 147.29 241.64 27.44 o 2 9 2 74.61 90.05 20.24 o 3 9 2 2.04 -7.20 42.37 o 4 9 2 386.31 462.01 28.94 o 5 9 2 0.18 9.24 16.16 o 6 9 2 375.25 391.24 26.90 o 7 9 2 1.08 -4.62 16.71 o 8 9 2 116.15 112.19 18.61 o 9 9 2 43.36 61.53 12.50 o 0 10 2 95.15 114.64 18.34 o 1 10 2 412.10 406.88 27.31 o 2 10 2 93.85 91.27 17.11 o 3 10 2 1187.00 1419.82 44.31 o 4 10 2 15.92 7.47 24.18 o 5 10 2 534.53 479.37 23.78 o 6 10 2 0.40 4.89 22.55 o 1 1 3 25679.90 23644.45 120.75 o 2 1 3 27757.96 25713.74 182.38 o 3 1 3 7551.72 6777.38 78.16 o 4 1 3 9541.78 9759.44 103.78 o 5 1 3 48380.18 48153.00 553.04 o 6 1 3 15694.45 16007.14 428.79 o 7 1 3 1691.00 1640.71 32.23 o 8 1 3 2464.61 2725.70 64.14 o 9 1 3 3188.09 3396.03 215.01 o 10 1 3 4268.40 4547.07 280.40 o 11 1 3 4024.29 3931.28 127.68 o 12 1 3 1100.49 1137.05 44.57 o 13 1 3 19048.27 19086.52 416.88 o 14 1 3 11.36 16.43 30.83 o 15 1 3 4687.29 4714.47 133.34 o 16 1 3 17.27 30.42 16.16 o 17 1 3 120.89 82.59 14.40 o 0 2 3 86762.73 93221.80 788.78 o 1 2 3 68951.89 67151.95 3571.05 o 2 2 3 534.02 454.75 19.37 o 3 2 3 3899.67 3860.97 67.54 o 4 2 3 4240.74 4411.31 115.70 o 5 2 3 0.00 77.82 20.17 o 6 2 3 197.24 284.84 41.29 o 7 2 3 29067.87 28658.80 1043.25 o 8 2 3 12443.32 12883.83 554.00 o 9 2 3 9911.63 10788.86 670.26 o 10 2 3 71.02 147.23 19.83 o 11 2 3 937.73 920.76 40.22 o 12 2 3 16.78 0.00 52.70 o 13 2 3 1000.90 1022.30 48.51 o 14 2 3 300.02 263.66 31.65 o 15 2 3 2657.46 2645.39 77.27 o 16 2 3 171.40 155.26 19.70 o 1 3 3 407.65 344.92 9.19 o 2 3 3 3238.65 2964.26 58.99 o 3 3 3 7899.74 7894.95 347.01 o 4 3 3 2608.55 2484.56 159.78 o 5 3 3 424.49 347.07 45.10 o 6 3 3 2046.71 2305.05 109.76 o 7 3 3 765.56 817.60 60.47 o 8 3 3 2553.95 2421.68 178.26 o 9 3 3 222.02 193.02 21.46 o 10 3 3 1043.86 1064.60 41.99 o 11 3 3 109.24 141.80 23.63 o 12 3 3 45.64 108.65 21.73 o 13 3 3 942.01 1038.58 46.88 o 14 3 3 523.28 495.20 33.28 o 15 3 3 168.59 181.74 21.33 o 16 3 3 21.83 39.39 14.53 o 0 4 3 9659.79 8821.21 293.89 o 1 4 3 1987.08 2045.57 90.05 o 2 4 3 5574.81 5409.48 148.94 o 3 4 3 78.44 94.40 11.14 o 4 4 3 94.81 115.18 13.45 o 5 4 3 849.32 822.96 29.22 o 6 4 3 4801.03 5187.62 119.88 o 7 4 3 23607.20 22720.72 378.89 o 8 4 3 11825.25 11062.88 282.09 o 9 4 3 6816.69 6492.12 164.96 o 10 4 3 1530.71 1461.10 48.93 o 11 4 3 5254.84 4831.82 150.64 o 12 4 3 1050.83 992.03 47.16 o 13 4 3 399.81 415.55 33.83 o 14 4 3 0.16 -41.56 41.56 o 15 4 3 3122.99 3186.25 89.98 o 1 5 3 7638.74 7257.00 181.82 o 2 5 3 2094.66 1939.38 60.79 o 3 5 3 369.09 397.90 24.45 o 4 5 3 8.20 17.25 38.84 o 5 5 3 1926.52 2023.82 59.01 o 6 5 3 1601.88 1505.83 43.77 o 7 5 3 67.82 36.54 20.92 o 8 5 3 1.22 14.26 17.66 o 9 5 3 935.32 874.55 40.49 o 10 5 3 1743.84 1620.18 57.50 o 11 5 3 217.60 244.90 27.44 o 12 5 3 284.14 331.58 29.75 o 13 5 3 1599.41 1399.32 46.22 o 14 5 3 130.74 175.22 17.79 o 15 5 3 133.02 125.51 16.44 o 0 6 3 3514.97 3422.22 91.46 o 1 6 3 841.92 820.19 31.80 o 2 6 3 2569.18 2450.55 76.85 o 3 6 3 1353.45 1498.68 47.84 o 4 6 3 159.63 120.48 22.41 o 5 6 3 46.91 30.15 57.18 o 6 6 3 3488.76 3296.61 95.93 o 7 6 3 849.10 844.48 37.77 o 8 6 3 1586.50 1524.35 50.43 o 9 6 3 786.55 794.45 41.44 o 10 6 3 358.36 268.83 29.21 o 11 6 3 3085.19 2894.90 92.11 o 12 6 3 464.07 459.73 31.11 o 13 6 3 68.08 147.77 18.06 o 14 6 3 176.88 159.88 15.49 o 1 7 3 501.99 488.12 30.97 o 2 7 3 3782.57 3941.15 127.25 o 3 7 3 1138.52 1412.82 50.01 o 4 7 3 2419.76 2574.11 77.52 o 5 7 3 3140.04 3216.16 97.95 o 6 7 3 1549.21 1333.88 46.22 o 7 7 3 193.63 170.74 26.89 o 8 7 3 1.76 -31.51 40.20 o 9 7 3 908.10 851.73 40.77 o 10 7 3 9.05 6.65 36.67 o 11 7 3 1153.66 1078.23 38.87 o 12 7 3 1.31 0.00 31.51 o 13 7 3 3029.50 2977.31 70.03 o 0 8 3 713.71 688.17 41.30 o 1 8 3 293.67 267.87 30.29 o 2 8 3 45.29 79.86 22.14 o 3 8 3 436.41 475.87 37.90 o 4 8 3 4.18 16.30 46.45 o 5 8 3 331.08 291.65 30.97 o 6 8 3 24.06 29.74 50.39 o 7 8 3 582.71 528.77 34.51 o 8 8 3 15.19 50.66 16.98 o 9 8 3 12.97 -4.35 17.25 o 10 8 3 61.95 84.35 16.43 o 11 8 3 10.19 19.69 12.77 o 1 9 3 6.09 22.27 17.93 o 2 9 3 642.98 624.03 32.34 o 3 9 3 0.62 20.92 36.26 o 4 9 3 1139.89 1216.24 45.12 o 5 9 3 810.62 849.54 37.10 o 6 9 3 276.55 246.14 23.09 o 7 9 3 195.55 123.47 21.19 o 8 9 3 89.08 113.01 17.52 o 9 9 3 1.78 0.00 24.72 o 0 10 3 438.29 464.36 28.12 o 1 10 3 43.47 25.40 16.03 o 2 10 3 30.86 22.14 15.08 o 3 10 3 76.58 57.32 16.98 o 4 10 3 1.32 -3.80 26.48 o 5 10 3 443.01 419.56 22.69 o 6 10 3 35.10 72.80 11.68 o 0 0 4 136893.91 144893.31 656.77 o 1 0 4 3486.03 3404.10 43.33 o 2 0 4 476.26 627.23 14.00 o 3 0 4 51465.17 48139.66 581.42 o 4 0 4 405.80 378.16 8.65 o 5 0 4 61289.27 61913.88 764.24 o 6 0 4 2888.10 3503.74 126.27 o 7 0 4 837.87 770.04 16.31 o 8 0 4 46416.24 45697.44 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o 7 9 11 946.72 865.53 26.37 o 0 10 11 7.33 3.40 11.27 o 1 10 11 6.13 -1.09 12.09 o 0 0 12 53255.79 54373.85 315.54 o 1 0 12 25708.03 25219.46 214.48 o 2 0 12 1191.43 1304.16 37.93 o 3 0 12 2516.71 2518.76 115.11 o 4 0 12 2305.72 2390.71 51.85 o 5 0 12 50.55 119.65 24.99 o 6 0 12 3391.87 3671.18 70.73 o 7 0 12 25779.54 25476.16 280.85 o 8 0 12 17072.06 17144.36 334.10 o 9 0 12 178.16 243.54 23.23 o 10 0 12 5.05 21.87 37.89 o 11 0 12 1689.06 1795.63 50.98 o 12 0 12 4168.18 4340.28 130.82 o 13 0 12 218.83 348.41 26.49 o 14 0 12 1698.14 1702.74 47.45 o 15 0 12 1282.41 1369.06 41.46 o 16 0 12 398.49 508.57 24.46 o 1 1 12 8932.35 8988.97 405.46 o 2 1 12 5778.84 5343.55 102.99 o 3 1 12 181.53 171.37 55.69 o 4 1 12 58.15 126.61 32.80 o 5 1 12 4533.14 4618.24 158.36 o 6 1 12 1142.98 1325.33 47.64 o 7 1 12 1411.97 1472.79 113.57 o 8 1 12 227.02 260.80 22.00 o 9 1 12 5279.06 5171.38 139.62 o 10 1 12 771.54 836.84 36.28 o 11 1 12 19.74 33.00 21.32 o 12 1 12 448.86 429.55 30.70 o 13 1 12 1140.21 1223.41 44.58 o 14 1 12 0.68 0.00 32.60 o 15 1 12 969.18 1076.97 36.70 o 0 2 12 10840.27 10034.73 142.24 o 1 2 12 4643.33 4373.22 80.81 o 2 2 12 4712.06 5130.12 111.13 o 3 2 12 4654.88 4886.91 75.29 o 4 2 12 6853.93 7407.01 320.27 o 5 2 12 4240.86 4499.82 194.40 o 6 2 12 12905.99 13834.32 225.09 o 7 2 12 10511.86 10882.77 186.24 o 8 2 12 5311.59 5311.19 135.81 o 9 2 12 288.88 265.70 24.72 o 10 2 12 107.04 104.18 20.78 o 11 2 12 353.83 427.90 28.12 o 12 2 12 1250.54 1201.99 46.07 o 13 2 12 383.31 501.27 29.61 o 14 2 12 1353.20 1237.28 39.56 o 15 2 12 376.78 384.47 23.91 o 1 3 12 13854.38 13483.00 181.05 o 2 3 12 8889.41 8112.56 144.46 o 3 3 12 55.44 139.82 78.78 o 4 3 12 2650.93 2638.12 148.62 o 5 3 12 10223.00 10768.85 488.46 o 6 3 12 1643.81 1586.58 35.52 o 7 3 12 956.19 989.82 36.42 o 8 3 12 3686.94 3594.07 96.35 o 9 3 12 3166.17 3142.21 94.15 o 10 3 12 7518.39 7283.00 169.10 o 11 3 12 2.45 20.24 19.56 o 12 3 12 215.04 254.82 24.18 o 13 3 12 2138.19 2225.12 70.58 o 14 3 12 10.86 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402.08 358.63 27.17 o 5 6 12 270.41 283.22 26.49 o 6 6 12 316.15 342.04 32.19 o 7 6 12 4010.36 3893.98 124.27 o 8 6 12 1651.52 1518.60 49.75 o 9 6 12 526.09 477.94 31.11 o 10 6 12 21.66 33.14 16.16 o 11 6 12 210.09 204.84 20.65 o 12 6 12 60.92 52.97 14.53 o 1 7 12 14.51 -1.49 20.92 o 2 7 12 1249.52 1131.71 49.06 o 3 7 12 46.04 32.46 55.14 o 4 7 12 1185.67 1246.51 49.74 o 5 7 12 200.74 267.59 26.08 o 6 7 12 94.89 0.00 58.00 o 7 7 12 22.78 38.30 17.11 o 8 7 12 497.67 510.96 29.48 o 9 7 12 130.34 111.38 17.93 o 10 7 12 569.84 563.87 27.99 o 11 7 12 32.43 58.67 12.36 o 0 8 12 1439.01 1436.34 49.48 o 1 8 12 251.18 318.40 27.03 o 2 8 12 138.74 155.25 23.36 o 3 8 12 43.08 26.76 20.92 o 4 8 12 297.04 316.91 26.76 o 5 8 12 1076.57 1175.44 42.27 o 6 8 12 1227.28 1238.92 39.42 o 7 8 12 611.58 627.18 30.30 o 8 8 12 564.90 582.22 27.85 o 9 8 12 35.21 39.52 12.50 o 1 9 12 659.27 618.64 31.39 o 2 9 12 44.91 20.51 36.94 o 3 9 12 181.19 198.18 22.14 o 4 9 12 0.48 -12.63 27.98 o 5 9 12 0.21 -6.93 24.99 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432.45 16.71 o 2 3 13 24.92 81.98 38.71 o 3 3 13 357.42 396.05 16.30 o 4 3 13 5863.90 5678.01 200.22 o 5 3 13 832.09 903.14 53.81 o 6 3 13 291.63 231.33 24.45 o 7 3 13 1742.36 1861.81 54.11 o 8 3 13 13.72 25.26 17.79 o 9 3 13 993.72 1003.13 38.73 o 10 3 13 83.36 84.75 18.88 o 11 3 13 35.45 53.24 19.97 o 12 3 13 885.57 836.92 37.50 o 13 3 13 193.41 185.41 21.60 o 14 3 13 156.70 188.53 18.20 o 15 3 13 154.36 161.92 17.12 o 0 4 13 35552.10 34077.69 534.94 o 1 4 13 3430.58 3390.58 167.19 o 2 4 13 6466.81 6162.44 101.61 o 3 4 13 195.51 204.97 21.60 o 4 4 13 384.83 421.26 25.95 o 5 4 13 545.96 513.40 29.48 o 6 4 13 513.66 483.23 28.94 o 7 4 13 3596.51 3354.58 119.62 o 8 4 13 7822.72 7785.72 175.13 o 9 4 13 7748.68 7802.12 174.71 o 10 4 13 972.40 901.35 41.58 o 11 4 13 1280.16 1168.60 43.76 o 12 4 13 7.57 -12.09 16.57 o 13 4 13 314.80 296.82 23.37 o 14 4 13 33.59 28.52 13.58 o 1 5 13 76.98 62.48 19.56 o 2 5 13 1661.88 1599.63 47.72 o 3 5 13 2635.77 2533.01 73.58 o 4 5 13 478.27 586.88 31.11 o 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3 14 23.24 51.34 16.43 o 7 3 14 8875.25 8542.27 252.76 o 8 3 14 420.59 471.52 28.26 o 9 3 14 1771.93 1665.21 54.79 o 10 3 14 3461.02 3596.82 119.06 o 11 3 14 652.64 693.86 36.55 o 12 3 14 168.71 153.08 19.56 o 13 3 14 73.04 127.94 17.66 o 14 3 14 27.02 35.99 12.90 o 0 4 14 1203.92 1162.23 29.29 o 1 4 14 158.18 144.37 24.38 o 2 4 14 2003.98 1919.88 42.83 o 3 4 14 188.00 163.00 22.96 o 4 4 14 444.31 380.51 27.71 o 5 4 14 51.97 38.57 17.52 o 6 4 14 985.27 1101.11 41.04 o 7 4 14 0.08 14.94 42.51 o 8 4 14 49.35 62.07 20.51 o 9 4 14 714.46 761.00 37.23 o 10 4 14 41.67 75.11 19.01 o 11 4 14 19.22 -48.08 48.08 o 12 4 14 443.74 382.02 26.36 o 13 4 14 11.75 3.94 15.21 o 14 4 14 81.66 54.60 14.13 o 1 5 14 12180.39 12117.25 311.62 o 2 5 14 248.12 284.57 28.25 o 3 5 14 423.97 374.67 26.35 o 4 5 14 1386.89 1390.86 47.16 o 5 5 14 1025.59 1071.10 40.36 o 6 5 14 513.29 459.32 30.97 o 7 5 14 2023.08 2103.79 59.55 o 8 5 14 1718.94 1724.04 53.83 o 9 5 14 2447.87 2392.84 68.41 o 10 5 14 474.75 484.72 29.62 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3625.97 3709.14 120.59 o 2 1 27 84.49 144.51 22.41 o 3 1 27 29.41 27.03 18.34 o 4 1 27 2913.51 2897.13 82.86 o 5 1 27 198.05 168.84 20.92 o 6 1 27 334.54 374.53 27.31 o 7 1 27 739.72 691.27 31.66 o 8 1 27 277.29 217.76 19.02 o 0 2 27 1374.25 1372.73 47.98 o 1 2 27 674.43 665.63 34.24 o 2 2 27 1078.91 1067.12 42.27 o 3 2 27 770.99 767.72 36.01 o 4 2 27 16.03 9.91 17.52 o 5 2 27 485.06 491.00 28.39 o 6 2 27 1798.67 1669.55 47.19 o 7 2 27 582.67 533.73 27.58 o 8 2 27 76.14 128.35 13.85 o 1 3 27 490.88 540.71 29.21 o 2 3 27 236.57 217.07 23.23 o 3 3 27 0.48 15.08 31.78 o 4 3 27 5.16 4.48 28.25 o 5 3 27 35.95 -4.07 39.39 o 6 3 27 114.65 113.69 19.02 o 7 3 27 1207.06 1107.04 32.63 o 0 4 27 0.06 4.48 36.67 o 1 4 27 603.76 553.95 32.61 o 2 4 27 313.18 265.85 23.77 o 3 4 27 880.36 885.55 35.47 o 4 4 27 99.03 96.03 16.16 o 5 4 27 1256.20 1207.06 35.08 o 6 4 27 770.76 679.74 25.15 o 1 5 27 58.56 82.31 15.08 o 2 5 27 5.04 14.40 21.87 o 3 5 27 28.25 19.42 11.82 o 0 0 28 9.10 38.16 19.29 o 1 0 28 1185.79 1223.09 43.76 o 2 0 28 1273.79 1390.90 46.08 o 3 0 28 0.33 -21.87 33.55 o 4 0 28 570.86 536.81 29.35 o 5 0 28 109.64 106.62 19.83 o 6 0 28 4131.67 3846.72 99.45 o 7 0 28 527.78 582.91 26.09 o 1 1 28 112.59 93.72 22.14 o 2 1 28 96.15 74.30 20.92 o 3 1 28 66.26 -15.62 39.39 o 4 1 28 1181.24 1130.47 38.33 o 5 1 28 304.37 299.27 25.40 o 6 1 28 31.91 14.94 28.79 o 7 1 28 6.82 8.96 12.22 o 0 2 28 9.41 7.47 17.11 o 1 2 28 0.03 -17.38 17.38 o 2 2 28 929.19 979.01 35.88 o 3 2 28 36.30 24.99 16.43 o 4 2 28 61.34 67.23 18.47 o 5 2 28 38.36 9.64 16.71 o 6 2 28 1182.38 1122.11 35.21 o 7 2 28 0.08 -15.08 20.64 o 1 3 28 94.32 98.34 20.92 o 2 3 28 4.53 -30.42 33.41 o 3 3 28 27.74 19.29 15.62 o 4 3 28 2307.01 2197.85 73.47 o 5 3 28 0.51 3.26 21.87 o 6 3 28 86.72 110.43 13.45 o 0 4 28 529.36 569.17 26.90 o 1 4 28 413.64 419.26 24.45 o 2 4 28 10.57 31.78 13.31 o 3 4 28 59.33 46.72 16.03 o 4 4 28 101.93 69.82 13.72 o 1 1 29 640.45 641.46 30.03 o 2 1 29 72.80 74.57 19.15 o 3 1 29 1344.74 1338.24 42.69 o 4 1 29 2174.58 2096.18 72.64 o 5 1 29 18.07 49.98 14.94 o 6 1 29 235.95 243.71 18.88 o 0 2 29 244.75 223.73 23.77 o 1 2 29 1401.09 1432.37 43.91 o 2 2 29 846.90 909.98 36.96 o 3 2 29 11.34 -7.74 30.69 o 4 2 29 56.76 67.23 15.08 o 5 2 29 216.92 204.44 17.12 o 1 3 29 28.17 40.75 14.80 o 2 3 29 103.89 117.08 17.25 o 3 3 29 110.55 125.51 16.30 o 4 3 29 430.96 425.68 22.01 o 0 4 29 492.91 463.35 21.47 o 1 4 29 206.11 208.93 16.71 o 2 4 29 1037.97 1074.23 33.31 o 0 0 30 4.50 30.02 16.03 o 1 0 30 3427.34 3179.69 88.23 o 2 0 30 191.26 151.18 18.88 o 3 0 30 360.03 357.84 24.45 o 4 0 30 0.22 12.09 23.63 o 5 0 30 0.23 0.00 19.96 o 1 1 30 531.18 548.10 27.45 o 2 1 30 1.91 14.67 12.77 o 3 1 30 210.46 229.84 19.02 o 4 1 30 270.14 248.06 19.15 o 5 1 30 111.99 121.57 16.30 o 0 2 30 560.02 503.02 26.36 o 1 2 30 212.54 222.64 18.34 o 2 2 30 34.74 28.52 14.26 o 3 2 30 197.35 182.98 16.98 o 4 2 30 18.57 33.68 11.95 o 1 3 30 1431.85 1377.33 39.44 o 2 3 30 38.94 41.70 12.90 o 1 1 31 571.84 586.09 24.32 o 2 1 31 197.59 216.94 16.57 o