Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 58| Part 8

ISSN: 2056-9890

August 2002 issue

Highlighted illustration

Cover illustration: This is the first crystal structure determination of N,N'-o-phenylenedioxamate, a well known ligand in many mono- and polymetallic systems, where it acts a bridge transmitting antiferro-, ferri- and ferromagnetic interactions between nearest-neighbour magnetic centres. See Martín, Beitia, Ugalde, Vitoria & Cortés [Acta Cryst. E58, o913-o915].

inorganic compounds

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Ammonium mercury(II) dichloride nitrate, (NH₄)₂HgCl₂(NO₃)₂

P. Nockemann and G. Meyer

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Samarium orthosilicate oxyapatite, Sm₅(SiO₄)₃O

M. G. Morgan, M. Wang and A. Mar

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metal-organic compounds

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Di-μ-iodo-bis{[bis(trans-cinnamaldehyde)ethylenediimine-κ²N,N′]copper(I)}

G. Kickelbick, M. Amirnasr, A. D. Khalaji and S. Dehghanpour

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Hexakis(μ₃-pyridine-2-thiolato-κ³N:S:S)hexasilver(I), [Ag₆(μ₃-SPy)₆]

L. Han, Z. Chen, J. Luo, M. Hong and R. Cao

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trans-Dichlorobis(4-cyanopyridine)palladium(II)

S. A. Barnett, A. J. Blake, N. R. Brooks, N. R. Champness, P. Hubberstey, S. J. Teat and M. Schröder

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Chloromethyl(η⁴-norbornadiene)platinum(II), an unsymmetrical substituted precursor for Pt^II complexes

G. Kickelbick, F. Stöhr and U. Schubert

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fac-Bis(2-aminomethylbenzimidazole)(2-aminomethylbenzimidazolato)nickel(II) dicyanamide monohydrate

Y. He, H.-Z. Kou, B. C. Zhou, M. Xiong, R.-J. Wang and Y. Li

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Supramolecular self-assembly via inter-ligands hydrogen bonds in [Cu(H₂O)₂(NO₃)₂(tb)] (tb is thiabendazole)

V. Sethuraman, N. Stanley, P. Thomas Muthiah and C. Karunakaran

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Chloro(nitrato)[1,4,7-tris(4-vinyl)benzyl-1,4,7-triazacyclononane]copper(II)

J. R. Deschamps, C. M. Hartshorn, A. Singh and E. L. Chang

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The complex salt benzodiimidazolium tetrachlorozincate

C.-X. Cai, L. Xu, Y.-Q. Tian and X.-Z. You

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Co(dmgH)₂(NO₂)[C₆H₃(CH₃)₂NH₂]–Co(dmgH)₂(NO₂)(C₆H₃Cl₂NH₂) cocrystal

B. Calmuschi, I. Kalf, M. Kirch, K. Thamer and U. Englert

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Dibromodicarbonylbis(triphenylphosphine)ruthenium(II) dichloromethane solvate

E. Lozano Diz, B. Therrien, A. Neels and G. Süss-Fink

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Chloro-cis-dihydro-mer-tris(triphenylphosphine)rhodium(III) dichloromethane hemisolvate

W. Clegg, M. R. J. Elsegood, N. C. Norman and N. L. Pickett

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Hydridodichlorotris(methyldiphenylphosphine)rhodium(III) dichloromethane trisolvate

W. Clegg, A. J. Scott, N. C. Norman, E. G. Robins and G. R. Whittell

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Trichloro(perdeuteroacetonitrile)bis(triphenylphosphine)rhodium(III)

W. Clegg, A. J. Scott, N. C. Norman, E. G. Robins and G. R. Whittell

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(η⁵-Pentamethylcyclopentadienyl)(η⁵-5,6,7-trihydro-4,8-dimethyl-s-indacenyl)iron(II)

P. G. Jones, H. Hopf and T. Hartig

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(η⁵-Pentamethylcyclopentadienyl)(η⁵-5,6,7-trihydro-4,8-dimethyl-s-indacenyl)ruthenium(II)

P. G. Jones, H. Hopf and T. Hartig

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Bis(trimethylammonium) tetrachloromercurate(II) at 343 K

M. Amami, S. Van Smaalen and A. Ben Salah

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A trinuclear molybdenum cluster coordinated by N-phenylanthranilate

Y. Kang, Z.-J. Li, Y.-Y. Qin, Y.-B. Chen, R.-F. Hu, Y.-H. Wen, J.-K. Cheng and Y.-G. Yao

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[(1RS,7RS,8RS,14RS)-5,12-Dimethyl-7,14-diphenyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene-κ⁴N^1,4,8,11]nickel(II) perchlorate

N. F. Curtis and D. C. Weatherburn

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Dichlorobis(trans-2-styrylbenzoxazole-κ²N,N′)cobalt(II)

H.-M. Liu, J.-P. Zhuang, W. Zhang and W.-Q. Zhang

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Dichloro{2,2′-thiobis[(4S)-4-isopropyl-1,3-oxazolinylphenyl]}zinc(II)

H. Kooijman, A. L. Spek, C. Zondervan and B. L. Feringa

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Bis[μ-bis(diphenylphosphino)methane-κ²P:P′]bis[(saccharinato-κN)palladium(I)] dichloromethane solvate

W. Henderson, B. K. Nicholson and D. C. Chung

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Bis(μ-2,2′′-dimethoxy-m-terphenyl)di-μ₃-iodo-bis(tetrahydrofuran)tetralithium(I)

G. W. Rabe, M. Zhang-Preße and G. P. A. Yap

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[5-Amino-6,8-dichloro-2,3-bis(2-pyridyl)quinoxaline]dichlorozinc(II)

D.-L. An, M. Du, X.-H. Bu, K. Biradha and M. Shionoya

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Bis(diethyldithiocarbamato)(4,7-dimethyl-1,10-phenanthroline)cadmium(II) acetonitrile solvate

T. Guo, C. S. Lai, X. J. Tan, C. S. Teo and E. R. T. Tiekink

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Di-n-butylbis(2′,4′-difluoro-4-hydroxybiphenyl-3-carboxylato-O,O′)tin(IV)

K. Hans, M. Parvez, F. Ahmad, S. Ali, M. Mazhar and A. Munir

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trans-Bis(acetonitrile)tetraaquacobalt(II) dinitrate at 150 K

S. A. Barnett, A. J. Blake, N. R. Champness and C. Wilson

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Potassium trans-diaquabis(malonato)chromium(III) trihydrate

M. Lemmer, H.-W. Lerner and M. Bolte

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Tris(O,O′-dimethyldithiophosphato)chromium(III)

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A new heteronuclear trirutheniumcobalt cluster containing a bulky phosphine ligand, [CoRu₃(μ-H)₃(μ-CO)(CO)₁₀(PCy₃)]

E. Lozano Diz, B. Therrien and G. Süss-Fink

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[1,4-Bis(pyridyl-2-ylmethyl)-1,4-diazacycloheptane]chlorocobalt(II) perchlorate

Y.-M. Guo, M. Du, S.-T. Chen and X.-H. Bu

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A comparative study of the interactions of cobalt(III) with naphtholate and phenolate moieties

M. S. Shongwe, S. A. Al-Juma and M. A. Fernandes

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A methyl-coordinated Rh^III ion in methylpentaamminerhodium(III)–chloropentaamminerhodium(III)–dithionate (0.73/2.27/3)

P. Harris and P. Kofod

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Bis[aquabis(1,3-diphenylpropane-1,3-dionato-κ²O,O′)dioxouranium(VI)] dicyclohexyl-18-crown-6-ether chloroform disolvate

H.-K. Fun, S. Kannan, S. Chantrapromma, I. A. Razak and A. Usman

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organic compounds

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Indole-3-spiro-N-methyl-2′-pyrrolidine-3′-spiro-9′′-anthracene-2,10′′-dione

A. Abdul Ajees, S. Manikandan and R. Raghunathan

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2-(2-Methoxyphenylhydrazono)-3-oxobutanoic acid

A. Rani, A. P. Saha and S. M. Prasad

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Triphenyl(benzoylmethyl)phosphonium nitrate: a three-dimensional hydrogen-bonded network

M. Baby Mariyatra, K. Panchanatheswaran and A. E. Goeta

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3-Methoxy-1′-phenyl-4′β,5-dihydro-1H-pyrazolo[4′,3′:16,17]estra-1,3,5(10)-triene

V. König, T. R. Schneider, E. Frank, B. Aukszi, G. Schneider and J. Wölfling

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Synthesis and absolute configuration of methyl (–)-(3R)-8-(4-bromophenyl)-7-(naphthalen-1-ylmethyl)-5-oxo-2,3-dihydro-5H-thiazolo[3,2-a]pyridine-3-carboxylate

V. Åberg, D. Boström, A. Fischer and F. Almqvist

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2,3,1′,3′-Tetrahydro-[1,2′]biindenylidene

J. Jovanovic, W. Elling, M. Schürmann, H. Preut and M. Spiteller

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Hydrogen-bonded supramolecular ribbons in the antifolate drug pyrimethamine

V. Sethuraman and P. Thomas Muthiah

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[Hydroxy(4-pyridyl)methyl]phosphonic acid monohydrate

X.-Y. Yi, Y.-Z. Li and L.-M. Zheng

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L-Histidinium dinitrate

N. Benali-Cherif, L. Benguedouar, A. Cherouana, L. Bendjeddou and H. Merazig

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4,4′-Bipyridin-1-ium bromide monohydrate

P. A. Iyere, W. Y. Boadi, R. S. Brooks, D. Atwood and S. Parkin

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2-(2,4-Dibromophenylamino)-7-nitrobenzisoselenazol-3-one

L. Dupont, M. Messali, L. Christiaens and G. Evrard

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Triphenylboroxin N,N-diethylhydroxylamine adduct (dimethylformamide solvate)

W. Kliegel, K. Drückler, B. O. Patrick, S. J. Rettig and J. Trotter

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cis,cis-Ceratospongamide monohydrate

M. Doi and A. Asano

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A novel three-dimensional supramolecule of 2,2′-dithiodibenzoic acid–4,4′-bipyridine (1/1)

W. Bi, D. Sun, R. Cao and M. Hong

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3,5-Difluorobenzonitrile

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2,3,6,7-Tetrakis(2-cyanoethylthio)tetrathiafulvalene

G. Liu, G. Xue, W. Yu, W. Xu and Q. Fang

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The 1:1 proton-transfer compound of benzylamine with 3,5-dinitrosalicylic acid

G. Smith, U. D. Wermuth and P. C. Healy

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1-Benzyl-4,5-diphenyl-3-vinylimidazolium bromide

R. T. Stibrany, J. A. Potenza and H. J. Schugar

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Four-centre hydrogen bonds: a triethanolamine–triethanolamine oxide complex

T. Kemmitt, G. J. Gainsford, P. J. Steel and J. Wikaira

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2-Hydroxybenzoic acid salt of physostigmine

J. L. Flippen-Anderson, J. R. Deschamps, A. Brossi and N. H. Greig

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(2E)-3-[(1E)-2-(5-Nitroisoxazol-3-yl)vinyloxy]prop-2-enal

R. Gilardi, R. Evans and M.-X. Zhang

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Bis(2-pyridylmethyl)ammonium perchlorate

R. J. Butcher, Y. Gultneh and A. R. Khan

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4,7-Dichlorotricyclo[3.1.1.0^3,6]heptane-2-carboxylic acid

R. Gilardi, R. J. Butcher and A. Bashir-Hashemi

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Bis(L-proline) hydrogen nitrate

S. Pandiarajan, B. Sridhar and R. K. Rajaram

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3,5-Dinitrosalicylic acid-phenazine (1/1)

V. S. Senthil Kumar, S. S. Kuduva and G. R. Desiraju

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4-Dimethylamino-4′-nitrobenzophenone

T. Kolev, M. Schürmann, D.-Chr. Kleb, H. Preut and P. Bleckmann

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1,4-Dichloro-1,4-diphenyl-2,3-diazabuta-1,3-diene

V. K. Tandon, A. Sharon, R. Bandichhor and P. R. Maulik

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The pseudoguaianolide peruvin

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Melampodinone

F. R. Fronczek and N. H. Fischer

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A new polymorph of atranorin, a lichen paradepside

Y.-H. Liu, S. L. Robbs, F. R. Fronczek, S. F. Watkins and N. H. Fischer

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DL-Valinium dihydrogen phosphate

B. S. Ravikumar, B. Sridhar and R. K. Rajaram

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L-Methioninium nitrate

S. Pandiarajan, B. Sridhar and R. K. Rajaram

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3-Benzylidene-1-(2,6-dichlorophenyl)indolin-2-one

S. Thamotharan, V. Parthasarathi, L. Vijayalakshmi, B. Anuradha, B. Desai and A. Shah

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Tetramethyl biphenyl-3,5,3′,5′-tetracarboxylate benzene sesquisolvate

S. J. Coles, P. A. Gale, M. B. Hursthouse and C. N. Warriner

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(3-Methoxyphenyl)acetic acid

A. R. Choudhury and T. N. Guru Row

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N-(p-Tolyl)maleamic acid

S. M. Prasad, R. B. P. Sinha, D. K. Mandal and A. Rani

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4-Chloro-2-(4-chlorophenyl)-1-formyl-1,2-dihydroquinoline

S. Thinagar, D. Velmurugan, V. Rajakannan, I.-H. Suh and S. Akila

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4,4′-[2,2′-(Piperidine-1,4-diyldiethylene)di(tosylimino)]diphthalonitrile

U. Çoruh, N. Akdemir, E. Agar, E. M. Vázquez-López and A. Erdönmez

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20-Oxopregn-5-ene-3β,16α-diyl diacetate

L. C. R. Andrade, J. A. Paixão, M. J. M. de Almeida, M. M. Cruz Silva, M. J. S. M. Moreno, M. L. Sá e Melo and A. S. Campos Neves

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trans-Bis(1H-benzimidazole-1-thione-κS)tetrachlorotellurium methanol disolvate

H. Fleischer and D. Schollmeyer

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Guanidinium pyromellitate

Y.-Q. Sun, J. Zhang and G.-Y. Yang

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N-(1-Phenylethyl)indole-2-carboxamide dimethylformamide solvate

Q. Y. Yang, L. Q. Qiu, Z. Y. Zhou, J. Y. Qi and A. S. C. Chan

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(E)-5-Methyl-2-(2-methylstyryl)pyrrole

A. Višnjevac, N. Basarić, B. Kojić-Prodić and M. Šindler-Kulyk

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(R,S)-1,2-Bis(benzylsulfinyl)ethane

J.-R. Li, R.-H. Zhang and X.-H. Bu

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Diethyl N,N′-o-phenylenedioxamate

S. Martín, J. I. Beitia, M. Ugalde, P. Vitoria and R. Cortés

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1,4-Bis(benzimidazol-2-yl)butane

C. Chen, C. Su, A. Xu, H. Zhang, X. Feng and B. Kang

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Redetermination of 3-hydroxy-2-naphthoic acid

M. U. Schmidt, G. Wagner and M. Bolte

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Quinoline N-oxide dihydrate from powder data

S. N. Ivashevskaja, L. A. Aleshina, V. P. Andreev, Y. P. Nizhnik and V. V. Chernyshev

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2,4,6-Trimethyl-1,3,5-tris(2-pyrimidinylthiomethyl)benzene chloroform hemisolvate

Y. Zheng, J.-R. Li, Y.-B. Xie and X.-H. Bu

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endo-6,syn-7-Dichloro-exo-6-phenylsulfonylbicyclo[3.1.1]heptane

O. Ya. Borbulevych, A. V. Semenov, V. A. Vasin and V. V. Razin

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Redetermination of silicon(IV) acetate

L. Wicke, E. Alig, H.-W. Lerner and M. Bolte

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2,2′-Diamino-4,4′-bi-1,3-thiazolium dichloride

J.-G. Liu, D.-J. Xu, Y.-Z. Xu, J.-Y. Wu and M. Y. Chiang

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trans-2-(2-Naphthyl)-3-(phenylselenyl)tetrahydropyran

C. E. F. Rickard, M. A. Brimble, G. Pavia and R. J. Stevenson

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cis-2-(2-Methoxyphenyl)-3-(phenylselenyl)tetrahydropyran

C. E. F. Rickard, M. A. Brimble, G. Pavia and R. J. Stevenson

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Montanastatin, cyclo[–(Val-D-Hyv-D-Val-Lac)₂–]

M. Doi and A. Asano

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Diethylammonium 5-phenyltetrazolate

I. A. Guzei and G. A. Bikzhanova

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Disappearance of inter- and intramolecular stacking due to one-atom addition in `propylene-linker' in a pyrazolo[3,4-d]pyrimidine-based flexible molecule

K. Avasthi, S. M. Farooq, A. Sharon and P. R. Maulik

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The supramolecular structure of N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycylglycinate contains a unique O—H⋯N(nitroso) hydrogen bond

J. N. Low, A. Quesada, C. Glidewell, M. A. Fontecha, P. Arranz, M. L. Godino and R. López

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2,4,5-Trichloroacetanilide

L. Mahalakshmi, V. Upadhyaya and T. N. Guru Row

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N,N-Dimethylammonium N′,N′-dimethylcarbamate

U. Kreher, C. L. Raston, C. R. Strauss and P. J. Nichols

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1,4,7,11,14,17-Hexaazacycloicosane-9,19-diol hexahydrobromide

F. Liang, Y.-Z. Li, C.-T. Wu and S.-M. Liu

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4,4′-[2,2-Methylenebis(4-chlorophenoxy)]diphthalonitrile

U. Çoruh, S. Işık, N. Akdemir, E. Ag~ar, E. M. Vázquez-López and A. Erdönmez

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10-Acetonyl-10-hydroxyphenanthren-9(10H)-one

A. Usman, I. A. Razak, H.-K. Fun, S. Chantrapromma, Y. Zhang and J.-H. Xu

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Pyridinium 2,2′-dithiodisalicylate

Y. Kang, R.-F. Hu, Y.-Y. Qin, Z.-J. Li, Y.-B. Chen, Y.-H. Wen, J.-K. Cheng and Y.-G. Yao

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2,3-Lutidine

A. D. Bond and J. E. Davies

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Ethyl 2-(cyclopentyloxy)-5-ethyl-4-hydroxy-6-methylnicotinate

S. Boland, C. Cauvin, B. Norberg, K. Le Van, B. Georges, L. Hevesi and F. Durant

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addenda and errata

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3,3′-Benzylidenebis(4-hydroxy-6-methylcoumarin). Erratum

L. Vijayalakshmi, V. Parthasarathi, V. Vora, B. Desai and A. Shah

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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