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Acta Cryst. (2002). E58, o831-o833  [ doi:10.1107/S1600536802011820 ]

Triphenylboroxin N,N-diethylhydroxylamine adduct (dimethylformamide solvate)

W. Kliegel, K. Drückler, B. O. Patrick, S. J. Rettig and J. Trotter

Abstract: N,N-Diethylhydroxylamine(O-B)triphenylboroxin N,N-dimethylformamide [2-(diethylammoniooxy)-2,4,6-triphenyl-1,3,5-trioxa-4,6-dibora-2-boratacyclohexane N,N-dimethylformamide], C22H26B3NO4·C3H7NO, contains one molecule of N,N-diethylhydroxylamine in its N-oxide form added to a boroxin heterocycle, with N,N-dimethylformamide solvent linked by an O...H-N hydrogen bond to the protonated hydroxylamine moiety.


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