Acta Cryst. (2002). E58, m569-m570  [ doi:10.1107/S1600536802016987 ]

Diaquadihydroxohexakis(tri-tert-butoxysilanethiolato)octalithium(I)-toluene (1/2)

K. Baranowska, J. Chojnacki, W. Wojnowski and I. Krossing

Online 27 September 2002

Key indicators

• Single-crystal X-ray study
• T = 200 K
• Mean (C-C) = 0.003 Å
• Disorder in solvent or counterion
• R factor = 0.036
• wR factor = 0.105
• Data-to-parameter ratio = 17.5

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_213  Alert C Atom C20     has ADP max/min Ratio ...........       3.20 prolate

PLAT_302  Alert C Anion/Solvent Disorder .......................      50.00 Perc.


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 2 Alert Level C = Please check

Copyright © International Union of Crystallography
IUCr Webmaster