Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 58| Part 12

ISSN: 2056-9890

December 2002 issue

Highlighted illustration

Cover illustration: This molecule, with an ether and two ester functionalities, is a polymerizing agent known for some years, but only now crystallographically characterized. See Flörke, Röder & Kramer [Acta Cryst. E58, o1343-o1344].

inorganic compounds

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A novel polyoxometalate supramolecular compound: [La(H₂O)₉]₂[V₁₀O₂₈]·8H₂O

X.-H. Peng, Y.-Z. Li, L.-X. Cai, L.-F. Wang and J.-G. Wu

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K₆[Mo₆V₂O₂₆]·4H₂O

N. Strukan, M. Devčić, B. Kamenar and G. Giester

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Na₃Cr₂(AsO₄)₃: trisodium dichromium(III) triarsenate

B. Bouzemi, H. Boughzala and T. Jouini

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CsAl(MoO₄)₂

P. E. Tomaszewski, A. Pietraszko, M. Mączka and J. Hanuza

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Manganese(II) sulfate tetrahydrate (ilesite)

P. Held and L. Bohatý

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Samarium chloride sulfide thiosilicate, Sm₃ClS₂[SiS₄]

S. T. Hatscher and W. Urland

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Cd₃Se₃O₁₀, isotypic with its mercury analogue

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Pentapotassium trihydrogenhexatungstoplatinate(IV) hexahydrate, K₅[H₃PtW₆O₂₄]·6H₂O

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metal-organic compounds

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Pentacyanoferrate(III)-μ-cyano-triaquatetrakis(dimethylformamide)europium(III) hydrate

J.-R. Li, L.-Z. Cai, R.-Q. Zou, G.-W. Zhou, G.-C. Guo, X.-H. Bu and J.-S. Huang

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Aquabenzoatobis(1,10-phenanthroline-κ²N,N′)manganese(II) perchlorate dimethylformamide solvate

X. Zhang, C. Fan, W. Wang, C. Chen and Q. Liu

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A one-dimensional Co^II coordination polymer exhibiting an unusual conformation for 1,2-bis(4-pyridyl)ethane

F. A. Almeida Paz, A. D. Bond, Y. Z. Khimyak and J. Klinowski

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Triphenyl(benzoylmethyl)phosphonium hexabromodicadmate(II): supramolecular aggregation through extensive C—H⋯Br and C—H⋯O interactions

M. Baby Mariyatra, K. Panchanatheswaran and A. E. Goeta

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Bis(1,1,3,3-tetramethyl-1,3-dibenzoatodistannoxane)

M. M. Amini, S. H. Abadi, M. Mirzaee, T. Lügger, F. E. Hahn and S. W. Ng

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trans-Diaquabis(2-pyridylethanol-N,O)nickel(II) disaccharinate

S. Hamamci, V. T. Yilmaz and C. Thöne

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trans-Diaquabis(2-pyridylethanol-N,O)cobalt(II) disaccharinate

V. T. Yilmaz, S. Hamamci and C. Thöne

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trans-Bis[ethane-1,2-diylbis(diphenylphosphane)-κ2P,P′]bis(thiocyanato-κN)molybdenum(II) toluene solvate

A. I. Philippopoulos, B. Ziemer and A. C. Filippou

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Bis[μ-η⁵:η¹-2-(cyclopentadienyl)ethoxy]bis[(η⁵-cyclopentadienyl)(1,2-dimethoxyethane-κO)yttrium]

H. Schumann, S. Dechert, I. I. Pestova and M. N. Bochkarev

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Ammine[2-hydroxy-1-naphthaldehyde 4-piperidylthiosemicarbazonato]nickel(II)

J. Valdés-Martínez, S. Hernández-Ortega and V. Bautista Jimenez

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Di-μ-chloro-bis[(2,2′:6,2′′-terpyridine)copper(II)] diperchlorate

J. Valdés-Martínez, D. Salazar-Mendoza and R. A. Toscano

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trans-Carbonylchlorobis(tribenzylphosphine)rhodium(I)

A. Muller, A. Roodt, S. Otto, Å. Oskarsson and S. Yong

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A germanium–silver complex containing aGe—Ag bond, Ag[Ge(OC₆HPh₄-2,3,5,6)₃(AgOSO₂CF₃)]·4C₆H₆

C. S. Weinert, P. E. Fanwick and I. P. Rothwell

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Bis(μ-quinoline N-oxide-κ²O:O)bis[dichlorocopper(II)], a powder diffraction study

S. N. Ivashevskaja, L. A. Aleshina, V. P. Andreev, Y. P. Nizhnik and V. V. Chernyshev

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N-(4-Bromobenzyl)pyridinium bis(2-thioxo-1,3-dithiole-4,5-dithiolato)nickel(III)

W.-J. Tong, L. Liu, Q.-J. Meng and Y.-Z. Li

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[Bis(2-mercapto-1-methylimidazol-3-yl)borato](triphenylphosphine)gold(I)

A. A. Mohamed, D. Rabinovich and J. P. Fackler

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Lithium tetrakis(tri-tert-butoxysilanethiolato)gallate(III)

K. Baranowska, J. Chojnacki, W. Wojnowski and E. Wurster

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catena-Poly[[[diaquacadmium(II)]-di-μ-4,4′-trimethylenedipyridine-κ²N:N′] dinitrate 4,4′-trimethylenedipyridine monohydrate]

F. A. Almeida Paz, A. D. Bond, Y. Z. Khimyak and J. Klinowski

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Redetermination of bis(2,2′-bipyridine-κ²N,N′)iodocopper(II) iodide

Y. Liu, D.-J. Xu, J.-Y. Wu and M. Y. Chiang

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Polymeric (diphenylphosphinato)tetrahydrofuranlithium

N. Kongprakaiwoot, R. L. Luck and E. Urnezius

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A potential synthon for models of vanadium haloperoxidase: (3,5-dimethylpyrazole)bis[2-hydroxy-2-methylbutanoato(1–)]oxovanadium(IV)

S. L. Raishbrook, P. Turner and R. Codd

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A 1:1 adduct between bis(chlorodimethylstannyl)methane and hexamethylphosphoric acid triamide (HMPA)

S. Mandolesi, M. Schürmann, H. Preut and T. Mitchell

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Tetrafluorodipyridinegermanium, [GeF₄(C₅H₅N)₂]

D. T. Tran, P. Y. Zavalij and S. R. J. Oliver

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Bis(μ-N-methyl-N-phenyldithiocarbamato)[bis(N-methyl-N-phenyldithiocarbamato)zinc(II)]

I. Baba, L. H. Lee, Y. Farina, A. H. Othman, A. R. Ibrahim, A. Usman, H.-K. Fun and S. W. Ng

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Diaqua(N-salicylidene-L-2-phenylglycinate-κ³N,O,O′)copper(II)

J. Weng, M. Hong, R. Cao, W. Bi and A. S. C. Chan

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Hexacarbonyldicobalt(0) complex of 5,6,11,12-tetradehydrodibenzo[a,e]cyclooctene, [(η²-C₁₆H₈)Co₂(CO)₆]

A. Orita, L. Jiang, F. Ye, N. Imai, H. Akashi and J. Otera

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The bis(maleonitriledithiolato)zincate(II) complex of the monoprotonated 4,4′-bipyridine cation

H. Xu, J. Xie, X. Ren and Y. Chen

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Tetrabutylammonium tetrakis(nitrato-κ²O,O′)[1,3,5-tris(pyrazolyl)methane-κ³N]cerate(III)

S.-J. Chen, Y.-Z. Li, X.-T. Chen, Y.-J. Shi and X.-Z. You

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Tris(N-butyl-N-ethyldithiocarbamato)bismuth(III)

I. Baba, K. Karimah, Y. Farina, A. H. Othman, A. R. Ibrahim, A. Usman, H.-K. Fun and S. W. Ng

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Bis(4-hydroxybenzoato-κO)bis(nicotinamide-κN)zinc(II)

H. Necefoğlu, T. Hökelek, C. C. Ersanlı and A. Erdönmez

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Pentaaqua(μ-pyridine-2,6-dicarboxylato-N,O,O′,O′′)(pyridine-2,6-dicarboxylato-N,O,O′')dinickel(II) dihydrate

Y.-H. Wen, Z.-J. Li, Y.-Y. Qin, Y. Kang, Y.-B. Chen, J.-K. Cheng and Y.-G. Yao

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Aqua[( $\pm$ )-lactate-O,O′](1,10-phenanthroline-κ²N,N′)copper(II) nitrate

G. Medina, L. Gasque and S. Bernès

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Dichloro[2,2′-hydroxy(ethoxy)methylenedipyridine-κ²N,N′]palladium(II)

J.-K. Cheng, Z.-J. Li, Y. Kang, Y.-B. Chen, Y.-Y. Qin, Y.-H. Wen and Y.-G. Yao

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[8,8′-(Propane-1,3-diyldioxy)diquinoline-κ⁴N,O,O′,N′]silver(I) trifluoromethanesulfonate

A.-W. Xu, Y.-P. Cai, L.-Z. Zhang, C.-Y. Su and B.-S. Kang

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Benzyltrimethylammonium bis(2-thioxo-1,3-dithiole-4,5-dithiolato)nickelate(III)

W. Xu, W. Yu, G. Xue and Q. Fang

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Tris(2,2′-bipyridyl-N,N′)iron(II) bis[tetrachloroferrate(III)]

L. M. D. Ariyananda and R. E. Norman

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Tricarbonyl(methyl)(η⁵-1,2,4-tricyclohexylcyclopentadienyl)molybdenum

H. Sitzmann, M. D. Walter and G. Wolmershäuser

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organic compounds

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Norbornane-endo-cis-2,3-dicarboxylic acid

A. S. Batsanov and J. L. Hesselink

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2-Norbornene-exo,endo-5,6-dicarboxylic acid

A. S. Batsanov and J. L. Hesselink

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10-[2-(4-Hydroxyphenyl)ethyl]-3,3,6,6,9-pentamethyl-3,4,6,7,9,10-hexahydroacridine-1,8(2H,5H)-dione

P. R. Seshadri, D. Velmurugan, T. Josephrajan, V. T. Ramakrishnan and M. J. Kim

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Acetophenone (2,4-dinitrophenyl)hydrazone

S. Shan, D.-J. Xu, J.-Y. Wu and M. Y. Chiang

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2-Methoxybenzaldehyde thiosemicarbazone

S. Selvanayagam, M. Yogavel, V. Rajakannan, D. Velmurugan, S. Shanmuga Sundara Raj and H.-K. Fun

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A host–guest 1:2 inclusion compound of 1,1,6,6-tetraphenylhexa-2,4-diyne-1,6-diol and 4-methoxybenzaldehyde

C. Wang, N. Gong and Y. Lu

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4-Chlorobenzohydrazide

I. Saraogi, B. H. M. Mruthyunjayaswamy, O. B. Ijare, Y. Jadegoud and T. N. Guru Row

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Methyl 4-oxahepta-1,6-diene-2,6-dicarboxylate

U. Flörke, T. Röder and T. Kramer

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Paracetamol monohydrate at 150 K

A. Parkin, S. Parsons and C. R. Pulham

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A hydrate of carbamoylmethyl 3,4,5-trihydroxybenzoate with three different molecular conformations

A. Parkin, S. Parsons, J. H. Robertson and P. A. Tasker

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Diglycinium sulfate

A. Cherouana, N. Benali-Cherif, L. Bendjeddou and H. Merazig

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Tris(1-propan-2-onyl oxime)amine

M. J. Goldcamp, J. A. K. Bauer and M. J. Baldwin

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cyclo-Bis(paraquat-m-terphenylene) tetrakis(hexafluorophosphate) tetrahydrate

T. Ravishankar, K. Chinnakali, K. Srinivasan, P. Rajakumar, A. Usman and H.-K. Fun

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16-(3-Pyridylmethylene)androst-4-ene-3,17-dione

G. Vasuki, V. Parthasarathi, K. Ramamurthi, S. Dubey and D. P. Jindal

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17a-Allyl-17a-aza-D-homoandrost-4-en-3-one

G. Vasuki, V. Parthasarathi, K. Ramamurthi, P. Piplani and D. P. Jindal

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3-Methyl-1,5-dinitro-9-phenacyl-3-azabicyclo[3.3.1]non-7-en-6-one

O. Y. Borbulevych, I. V. Shahkheldyan, O. V. Leonova, Y. M. Atroshchenko and E. N. Alifanova

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4-[(2-Hydroxyphenylamino)phenylmethylene]-5-methyl-2-phenyl-2H-pyrazol-3(4H)-one

J.-L. Wang, S.-M. Zhang and F.-M. Miao

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1-(3,5-Dimethoxyphenyl)-2-{2-[(3,5-dimethoxyphenyl)hydroxymethyl]-4-methoxyphenyl}ethanol

Q. Yin and W.-Q. Zhang

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N-(2-Bromophenyl)phthalimide

J.-Y. Wu, M.Y.-N. Chiang and W.-F. Zeng

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L-Aspartic acid nitrate–L-aspartic acid (1/1)

B. Sridhar, N. Srinivasan and R. K. Rajaram

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Dicyanodurene–p-tetrafluorodiiodobenzene (1/1)

D. Britton and W. B. Gleason

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3-Phenylpyrazole, a pseudosymmetric structure with Z′ = 6

A. Haghiri, H.-W. Lerner, M. Wagner and J. W. Bats

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Bis(pyridine)iodonium(I) tetrafluoroborate

C. Álvarez-Rúa, S. García-Granda, A. Ballesteros, F. González-Bobes and J. M. González

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1,4-Diazaspiro[4.5]decane-2,3-dione

D. Stasko, M. C. Davis and R. D. Chapman

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(2-Ethoxycarbonyl-3,5-dihydroxyphenyl)acetic acid monohydrate, an intermediate in the Pechmann reaction

R. L. Luck and G. D. Mendenhall

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2-Chloro-1,1-dimethyl-2-phenyl-2,3-dihydro-1H-1,2-benzazoniaborolate

H.-B. Tong, X.-H. Wei, S.-P. Huang, J.-F. Li and D.-S. Liu

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A novel diterpene lactone

A. C. Doriguetto, H. S. Vieira, J. A. Ellena, J. A. Takahashi, M. A. D. Boaventura and Y. P. Mascarenhas

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1-(3-Chlorophenyl)-4-(3-chloropropyl)piperazinium chloride

C. L. Homrighausen and J. A. Krause Bauer

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Guaninium dinitrate dihydrate

K. Bouchouit, N. Benali-Cherif, L. Benguedouar, L. Bendheif and H. Merazig

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1-(6-Methylpyridin-2-yl)-2-phenylethanedione

Y. Li, A. Usman, Y. Zhang, H.-K. Fun and J.-H. Xu

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Methyl (1SR,8RS,10SR)-3,5-dichloro-1-(4-methoxyphenyl)-8-(phenylthio)-11-oxa-4-azatricyclo[6.2.1.0^2,7]undeca-2,4,6-triene-10-carboxylate

A. Usman, T. K. Sarkar, N. Panda and H.-K. Fun

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(rac-5RS,7RS,8SR)-Spiro[7-methoxycarbonyl-1-aza-3-thiabicyclo[3.3.0]octane-8,1′-acenaphthylen]-2′-one

T. V. Sundar, V. Parthasarathi, C. Álvarez-Rúa, S. García-Granda, A. Saxena, P. Pardasani and R. T. Pardasani

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3,4,6-Tris(pyrazol-1-yl)pyridazine

A. J. Blake, P. Hubberstey and A. D. Mackrell

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(11SR,15SR)-9,10,11,15-Tetrahydro-9-[(1SR)-1-methoxyethyl]-9,10-[3′,4′]furanoanthracene-12,14-dione

W. Clegg and R. W. Harrington

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(3aSR,9aSR)-3a,4,9,9a-Tetrahydro-4-[(1SR)-1-methoxyethyl]-2-methyl-4,9-[1′,2′]benzeno-1H-benzo[f]isoindole-1,3-(2H)-dione

W. Clegg and R. W. Harrington

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2(S)-N-tert-Butoxycarbonylamino-N-methoxy-N-methylbutanamide

P. Sawatzki, T. Mikeska, M. Nieger, H. Hupfer and T. Kolter

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2-[2′-(Phenylsulfonyl)ethyl]cyclopentanone

W. A. Loughlin, M. A. McCleary and P. C. Healy

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Methyl (E)-3-acetamido-2-pentenoate

X. Chen, R. Guo and Z. Zhou

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Ethyl (E)-2-acetyl-3-amino-3-phenyl-2-propylenoate

X. Chen, R. Guo and Z. Zhou

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Methyl (E)-3-acetamido-4-methyl-2-pentenoate

X. Chen, R. Guo and Z. Zhou

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Methyl 3-benzoyl-8-hydroxy-5-methoxyindolizine-1-carboxylate

A. Usman, Y. Li, Y. Zhang, H.-K. Fun and J.-H. Xu

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2-(p-Methoxyphenyl)-3-[o-(methylaminothiocarbonyl)phenyl]-1,3,2-oxazaphospholidine 2-sulfide

S.-L. Deng, D.-Z. Liu and W. Li

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2-Chloro-1,3-dioxa-2σ³λ³-phosphaanthracen-4-one

P. G. Jones, C. Kunze, H. Thönnessen and R. Schmutzler

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2-Chloro-1,3-dioxa-2σ³λ³-phosphaphenanthren-4-one

P. G. Jones, C. Kunze, M. Freytag and R. Schmutzler

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A second polymorph of p-nitrobenzamide

P. G. Jones, H. Thönnessen, R. Schmutzler and A. K. Fischer

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1-(Phenylethynyl)adamantane

A. L. Raine, C. M. Williams and P. V. Bernhardt

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6,6′-Dichloro-3,3′-(butane-1,4-diyldioxy)diflavone

S. Thinagar, D. Velmurugan, S. C. Gupta, H. Merazig and S. Bouacida

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Propiophenone 2,4-dinitrophenylhydrazone

S. Shan, D.-J. Xu, J.-Y. Wu and M. Y. Chiang

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2-(p-Bromophenylhydrazono)-3-oxobutanoic acid

S. M. Prasad, S. C. Gupta and A. Rani

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(1R,2R)-2-(Methylphenylamino)-1,2-dihydronaphthalen-1-ol–water (4/1)

K. Fagnou, M. Lautens and A. J. Lough

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6-(4-Chlorophenyl)-4-[4-(dimethylamino)phenyl]-2-(pyrrolidin-1-yl)nicotinonitrile

S. Thinagar, D. Velmurugan, S. Shanmuga Sundara Raj, H.-K. Fun and V. Raghukumar

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S,S′-(But-2-yne-1,4-diyl)bis(L-cysteine) monohydrate

Y.-M. Shi and W.-Q. Zhang

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6-Ethyl-5,7-dimethyl-6H-1,4-diazepine-2,3-dicarbonitrile

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2(S),6(R)-Dimethyl-4-(4-methoxyphenyl)-5(R)-ethyl-3-cyclohexene-1(S)-carboxylic acid and its enantiomer: potential therapeutic agents for prostate cancer

S. Xie, Y. Hou, C. Y. Meyers and P. D. Robinson

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2a′,8a′-Dichloro-3,8-dioxo-1′,2′,2a′,8a′-tetrahydrodispiro[cyclopropane-1,1′-cyclobuta[b]naphthalene-2′,1′′-cyclopropane]

A. Usman, H.-K. Fun, L. Wang, Y. Zhang and J.-H. Xu

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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