Acta Cryst. (2002). E58, m775-m776  [ doi:10.1107/S1600536802021773 ]

Tris(2,2'-bipyridyl-N,N')iron(II) bis[tetrachloroferrate(III)]

L. M. D. Ariyananda and R. E. Norman

Online 30 November 2002

Key indicators

• Single-crystal X-ray study
• T = 100 K
• Mean (C-C) = 0.004 Å
• R factor = 0.043
• wR factor = 0.072
• Data-to-parameter ratio = 14.4

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     27
                   N1  -FE1 -N6  -C26   -44.00  1.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     28
                   N1  -FE1 -N6  -C30   143.00  1.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     37
                   N2  -FE1 -N4  -C16   -70.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     38
                   N2  -FE1 -N4  -C20   116.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     52
                   N3  -FE1 -N5  -C21   126.30  0.80   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     53
                   N3  -FE1 -N5  -C25   -52.10  0.90   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     62
                   N4  -FE1 -N2  -C6    -23.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     63
                   N4  -FE1 -N2  -C10   164.00  2.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     77
                   N5  -FE1 -N3  -C11   154.60  0.70   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     78
                   N5  -FE1 -N3  -C15   -28.90  0.90   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     87
                   N6  -FE1 -N1  -C1    131.00  1.00   1.555   1.555   1.555   1.555

PLAT_710  Alert C Delete 1-2-3 or 2-3-4 (CIF) Linear Torsion Angle #     88
                   N6  -FE1 -N1  -C5    -52.00  1.00   1.555   1.555   1.555   1.555


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 12 Alert Level C = Please check

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