Acta Cryst. (2002). E58, i124-i126  [ doi:10.1107/S1600536802021694 ]

Samarium chloride sulfide thiosilicate, Sm₃ClS₂[SiS₄]

S. T. Hatscher and W. Urland

Online 30 November 2002

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (S-Si) = 0.002 Å
• R factor = 0.020
• wR factor = 0.038
• Data-to-parameter ratio = 21.1

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           28.25                 
         From the CIF: _reflns_number_total               2446                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         2654                           
         Completeness (_total/calc)             92.16%                          
          Alert C: < 95% complete                                               

RINTA_01  Alert C The value of Rint is greater than 0.10                        
          Rint given   0.107                                                    


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 2 Alert Level C = Please check

Copyright © International Union of Crystallography
IUCr Webmaster