(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, m715-m717 [ doi:10.1107/S1600536802019980 ]

trans-Carbonylchlorobis(tribenzylphosphine)rhodium(I)

A. Muller, A. Roodt, S. Otto, Å. Oskarsson and S. Yong

Online 15 November 2002

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.010 Å
R factor = 0.048
wR factor = 0.091
Data-to-parameter ratio = 10.1

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level A:



DIFF_020  Alert A _diffrn_standards_interval_count and                          
          _diffrn_standards_interval_time are missing. Number of measurements   
          between standards or time (min) between standards.                    

DIFF_022  Alert A _diffrn_standards_decay_% is missing                          
          Percentage decrease in standards intensity.                           


 Alert Level B:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           31.66                 
         From the CIF: _reflns_number_total              11180                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns        12659                           
         Completeness (_total/calc)             88.32%                          
          Alert B: < 90% complete (theta max?)                                  


 2 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 0 Alert Level C = Please check