Acta Cryst. (2002). E58, o1449-o1451  [ doi:10.1107/S1600536802021608 ]

(1R*,2R*)-2-(Methylphenylamino)-1,2-dihydronaphthalen-1-ol-water (4/1)

K. Fagnou, M. Lautens and A. J. Lough

Online 30 November 2002

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.004 Å
• R factor = 0.037
• wR factor = 0.090
• Data-to-parameter ratio = 7.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



PLAT_420  Alert B D-H Without Acceptor       O1W    -   H2W               ?

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           26.02                 
         From the CIF: _reflns_number_total               5415                  
         Count of symmetry unique reflns         5422                           
         Completeness (_total/calc)             99.87%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured         0                           
         Fraction of Friedel pairs measured     0.000                           
         Are heavy atom types Z>Si present           no                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.          


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 0 Alert Level C = Please check

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