Acta Cryst. (2002). E58, m710-m711  [ doi:10.1107/S1600536802020184 ]

Ammine[2-hydroxy-1-naphthaldehyde 4-piperidylthiosemicarbazonato]nickel(II)

J. Valdés-Martínez, S. Hernández-Ortega and V. Bautista Jimenez

Online 15 November 2002

Key indicators

• Single-crystal X-ray study
• T = 291 K
• Mean (C-C) = 0.006 Å
• R factor = 0.042
• wR factor = 0.110
• Data-to-parameter ratio = 13.4

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_353  Alert C Long    N-H Bond (0.87A)   N(4)   -   H(4C)  =       1.01 Ang.

PLAT_420  Alert C D-H Without Acceptor       N(4)   -   H(4A)             ?

PLAT_420  Alert C D-H Without Acceptor       N(4)   -   H(4C)             ?


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 3 Alert Level C = Please check

Copyright © International Union of Crystallography
IUCr Webmaster