Acta Cryst. (2002). E58, m718-m720  [ doi:10.1107/S1600536802020585 ]

A germanium-silver complex containing aGe-Ag bond, Ag[Ge(OC₆HPh₄-2,3,5,6)₃(AgOSO₂CF₃)]·4C₆H₆

C. S. Weinert, P. E. Fanwick and I. P. Rothwell

Online 15 November 2002

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.004 Å
• R factor = 0.039
• wR factor = 0.074
• Data-to-parameter ratio = 18.6

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



ABSTM_02  Alert B The ratio of expected to reported Tmax/Tmin(RR') is < 0.75    
          Tmin and Tmax reported:      0.574     0.814                          
          Tmin' and Tmax expected:      0.775     0.814                         
          RR' =      0.740                                                      
          Please check that your absorption correction is appropriate.          


 Alert Level C:



ABSMU_01  Alert C The ratio of given/expected absorption coefficient lies       
          outside the range 0.99 <> 1.01                                        
          Calculated value of mu =     0.838                                    
          Value of mu given      =     0.825                                    

ABSTY_02  Alert C An _exptl_absorpt_correction_type has been given without      
          a literature citation. This should be contained in the                
          _exptl_absorpt_process_details field.                                 
          Absorption correction given as empirical                              

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.90                 
         From the CIF: _reflns_number_total              21443                  
         From the CIF: _diffrn_reflns_limit_ max hkl   18.   30.   35.          
         From the CIF: _diffrn_reflns_limit_ min hkl    0.    0.  -35.          
         TEST1: Expected hkl limits for theta max                               
         Calculated maximum hkl   18.   32.   35.                               
         Calculated minimum hkl  -18.  -32.  -35.                               
          ALERT: Expected hkl max differ from CIF values                        


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 2 Alert Level C = Please check

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