(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2002). E58, o1430-o1431 [ doi:10.1107/S1600536802021219 ]

2-(p-Methoxyphenyl)-3-[o-(methylaminothiocarbonyl)phenyl]-1,3,2-oxazaphospholidine 2-sulfide

S.-L. Deng, D.-Z. Liu and W. Li

Online 30 November 2002

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.011 Å
R factor = 0.045
wR factor = 0.103
Data-to-parameter ratio = 11.8

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_601  Alert C Structure Contains Solvent Accessible VOIDS of      46.00 A   3

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           25.03                 
         From the CIF: _reflns_number_total              10230                  
         Count of symmetry unique reflns         6733                           
         Completeness (_total/calc)            151.94%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured      3497                           
         Fraction of Friedel pairs measured     0.519                           
         Are heavy atom types Z>Si present          yes                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.          


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check