# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' ya6141 in P-1 (-90 deg. C)' _shelx_refln_list_code 4 _shelx_F_calc_maximum 248.48 _exptl_crystal_F_000 736.00 _reflns_d_resolution_high 0.7499 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.5120 _cell_length_b 10.5128 _cell_length_c 14.5755 _cell_angle_alpha 99.713 _cell_angle_beta 99.927 _cell_angle_gamma 103.383 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 7946.22 8838.53 1094.09 o 3 0 0 1367.64 1148.23 110.62 o 4 0 0 341.99 254.87 30.78 o 5 0 0 4030.14 3898.18 444.00 o 6 0 0 9622.90 9306.65 864.26 o 7 0 0 5978.86 5862.01 455.59 o 8 0 0 1628.58 1333.11 111.79 o 9 0 0 1478.69 1495.28 125.92 o 10 0 0 27.48 43.98 32.81 o 11 0 0 248.00 266.25 80.78 o 12 0 0 337.63 305.93 87.51 o 13 0 0 1577.56 1411.76 236.18 o -13 1 0 1553.56 1459.17 237.47 o -12 1 0 134.92 145.95 69.61 o -11 1 0 868.30 758.54 96.18 o -10 1 0 168.94 192.18 44.09 o -9 1 0 1546.69 1481.79 150.36 o -8 1 0 10023.09 9370.96 872.09 o -7 1 0 14461.29 13850.58 1467.34 o -6 1 0 5353.65 5462.65 510.97 o -5 1 0 5608.72 6226.97 777.14 o -4 1 0 4121.44 3964.74 496.99 o -3 1 0 220.98 3.87 9.74 o -2 1 0 9229.76 8022.56 388.01 o -1 1 0 23520.86 16158.72 724.39 o 0 1 0 54628.77 35000.63 2653.24 o 1 1 0 9822.46 7250.30 449.75 o 2 1 0 2632.97 2185.15 169.73 o 3 1 0 4987.64 5435.79 419.07 o 4 1 0 84.74 103.39 15.57 o 5 1 0 7648.65 6835.69 526.15 o 6 1 0 10898.53 10707.22 822.13 o 7 1 0 7445.05 6825.93 528.32 o 8 1 0 2309.38 2283.53 183.92 o 9 1 0 1082.24 1014.40 136.13 o 10 1 0 14.18 8.59 47.98 o 11 1 0 707.08 730.87 142.37 o 12 1 0 786.10 717.98 141.79 o -13 2 0 2832.01 2138.20 324.26 o -12 2 0 974.07 916.66 155.11 o -11 2 0 1870.68 2112.42 325.12 o -10 2 0 0.89 13.66 16.27 o -9 2 0 6101.28 5201.39 243.54 o -8 2 0 18900.56 16737.46 764.69 o -7 2 0 14229.84 12282.08 562.37 o -6 2 0 5325.18 4109.77 203.16 o -5 2 0 9584.40 7614.06 370.46 o -4 2 0 13529.52 11820.29 571.63 o -3 2 0 1856.09 2277.92 114.20 o -2 2 0 868.81 1821.53 241.76 o -1 2 0 10034.53 10230.38 1268.40 o 0 2 0 15005.52 12928.47 984.84 o 1 2 0 15295.76 3292.33 5646.07 o 2 2 0 6284.16 5402.05 414.16 o 3 2 0 2286.73 2456.79 192.17 o 4 2 0 386.53 436.68 40.55 o 5 2 0 6828.46 6143.62 473.88 o 6 2 0 22225.05 21694.92 1659.06 o 7 2 0 10309.97 9132.45 703.73 o 8 2 0 4572.08 4600.97 728.44 o 9 2 0 2517.71 2734.73 405.47 o 10 2 0 310.96 340.02 93.10 o 11 2 0 188.56 234.03 80.06 o 12 2 0 530.44 592.38 132.91 o -13 3 0 3372.22 2700.59 346.89 o -12 3 0 3511.07 3638.33 538.67 o -11 3 0 2653.08 3275.46 160.52 o -10 3 0 151.44 197.19 25.87 o -9 3 0 1961.66 1682.73 86.58 o -8 3 0 9870.26 9762.76 476.63 o -7 3 0 9753.11 8643.64 422.12 o -6 3 0 7992.18 9351.63 455.94 o -5 3 0 16432.03 19076.67 920.84 o -4 3 0 15734.79 19985.12 2474.78 o -3 3 0 2585.31 3593.36 454.31 o -2 3 0 13746.40 16107.03 1997.70 o -1 3 0 8824.32 12067.96 1500.42 o 0 3 0 3216.81 3306.57 309.45 o 1 3 0 7812.28 8709.97 668.46 o 2 3 0 1214.38 918.35 186.69 o 3 3 0 3311.12 2655.48 236.89 o 4 3 0 622.68 619.50 65.14 o 5 3 0 1411.42 1710.60 138.68 o 6 3 0 8218.15 8704.50 673.04 o 7 3 0 9620.01 9533.14 882.00 o 8 3 0 4462.16 4219.40 600.83 o 9 3 0 2523.07 3204.51 473.21 o 10 3 0 633.97 591.37 126.04 o 11 3 0 61.39 110.86 77.91 o 12 3 0 194.63 138.78 80.35 o -13 4 0 4007.20 3975.63 590.94 o -12 4 0 6122.75 5877.22 851.33 o -11 4 0 2534.09 2944.39 299.41 o -10 4 0 4.39 10.10 31.76 o -9 4 0 2470.88 2773.26 366.94 o -8 4 0 3654.79 3206.94 417.79 o -7 4 0 14109.22 17627.07 2192.62 o -6 4 0 14021.63 17506.19 2175.15 o -5 4 0 11903.90 33503.51 4160.39 o -4 4 0 4246.46 5004.27 631.48 o -3 4 0 8119.61 12766.32 1589.22 o -2 4 0 12569.59 15770.60 1957.45 o -1 4 0 12179.30 11958.53 1487.24 o 0 4 0 17448.57 17229.47 1582.77 o 1 4 0 22673.66 23911.36 1831.31 o 2 4 0 10334.96 3476.37 3738.70 o 3 4 0 2571.67 2485.79 209.78 o 4 4 0 71.33 94.05 19.54 o 5 4 0 432.50 538.53 51.12 o 6 4 0 2939.35 3056.09 292.94 o 7 4 0 5211.80 4961.92 466.08 o 8 4 0 2261.82 2259.65 338.44 o 9 4 0 1076.92 1132.19 192.78 o 10 4 0 559.38 601.40 134.06 o 11 4 0 45.59 78.06 74.19 o -13 5 0 3955.45 4314.93 643.65 o -12 5 0 4238.95 4099.23 607.13 o -11 5 0 274.35 312.77 68.46 o -10 5 0 65.05 11.02 39.72 o -9 5 0 124.06 431.97 186.05 o -8 5 0 692.22 760.81 133.34 o -7 5 0 11989.06 14818.87 1849.60 o -6 5 0 16397.56 20382.00 2532.07 o -5 5 0 7901.79 8759.75 1096.67 o -4 5 0 5197.93 5957.71 751.64 o -3 5 0 456.36 580.20 88.37 o -2 5 0 5326.82 9899.82 1244.19 o -1 5 0 15107.17 18133.37 2252.49 o 0 5 0 15267.36 17381.18 1595.68 o 1 5 0 10669.74 12941.12 995.80 o 2 5 0 7825.89 7734.72 598.95 o 3 5 0 1189.03 996.23 154.15 o 4 5 0 55.48 60.15 19.32 o 5 5 0 488.53 571.85 72.58 o 6 5 0 831.29 908.50 104.11 o 7 5 0 2179.23 2996.54 447.72 o 8 5 0 961.44 1498.13 249.50 o 9 5 0 586.86 708.39 157.26 o 10 5 0 596.47 846.03 183.18 o -13 6 0 2669.78 2324.96 371.09 o -12 6 0 1704.05 1992.15 222.25 o -11 6 0 265.12 273.70 70.93 o -10 6 0 92.78 138.35 78.63 o -9 6 0 361.09 440.13 111.00 o -8 6 0 3436.48 4223.69 551.70 o -7 6 0 10788.32 11852.55 1484.67 o -6 6 0 15031.45 22047.41 2745.61 o -5 6 0 8435.16 9710.48 1219.41 o -4 6 0 3635.72 3765.80 483.10 o -3 6 0 665.51 802.34 123.03 o -2 6 0 1897.59 2399.44 316.67 o -1 6 0 8675.11 9456.54 1185.04 o 0 6 0 8888.82 9101.06 844.55 o 1 6 0 7171.83 7957.87 739.47 o 2 6 0 10179.46 9768.41 755.94 o 3 6 0 3112.07 705.67 1340.68 o 4 6 0 10.73 29.60 29.00 o 5 6 0 1998.77 2247.53 233.38 o 6 6 0 2158.91 2169.17 240.04 o 7 6 0 1581.76 1815.80 284.87 o 8 6 0 1457.00 1443.27 237.18 o 9 6 0 1067.38 1024.63 188.05 o 10 6 0 598.74 844.31 182.75 o -13 7 0 3250.28 3147.07 492.69 o -12 7 0 2468.91 2723.75 379.40 o -11 7 0 1420.08 2089.65 312.23 o -10 7 0 24.11 48.41 72.04 o -9 7 0 321.52 433.83 120.31 o -8 7 0 1784.91 2853.89 398.59 o -7 7 0 3365.95 4537.35 590.51 o -6 7 0 8955.84 10992.48 1381.69 o -5 7 0 8087.94 9653.48 1217.27 o -4 7 0 4485.62 5726.26 733.45 o -3 7 0 2411.39 2817.51 372.24 o -2 7 0 10.92 99.11 52.28 o -1 7 0 1905.12 1643.07 224.29 o 0 7 0 4668.40 5542.26 523.22 o 1 7 0 5080.95 5387.21 508.49 o 2 7 0 5928.17 5935.12 559.88 o 3 7 0 2103.52 1567.25 481.38 o 4 7 0 324.85 454.76 66.98 o 5 7 0 1749.16 1901.99 196.28 o 6 7 0 652.42 606.27 128.04 o 7 7 0 771.37 827.98 161.27 o 8 7 0 1844.39 1751.21 284.73 o 9 7 0 1650.84 1688.04 280.58 o -12 8 0 3099.70 3390.53 354.72 o -11 8 0 4075.68 5050.10 673.58 o -10 8 0 688.21 737.18 152.53 o -9 8 0 542.47 668.29 144.94 o -8 8 0 1700.56 1840.15 268.12 o -7 8 0 3505.26 3729.28 491.55 o -6 8 0 9394.65 10132.56 1280.00 o -5 8 0 6797.14 8284.11 1053.99 o -4 8 0 560.43 597.96 110.43 o -3 8 0 172.16 235.32 84.22 o -2 8 0 292.65 359.06 81.21 o -1 8 0 855.00 828.41 128.62 o 0 8 0 4833.05 5189.64 491.49 o 1 8 0 5977.73 5599.74 529.71 o 2 8 0 5151.53 5502.15 521.97 o 3 8 0 2475.59 2514.43 249.78 o 4 8 0 312.50 255.19 50.66 o 5 8 0 82.67 69.75 68.03 o 6 8 0 226.70 229.30 92.52 o 7 8 0 604.79 682.32 150.96 o 8 8 0 2501.06 2607.69 403.89 o -12 9 0 3836.55 3597.44 370.25 o -11 9 0 3123.03 2837.56 399.88 o -10 9 0 1357.01 1243.48 208.11 o -9 9 0 97.40 117.87 96.82 o -8 9 0 1738.45 2004.71 296.62 o -7 9 0 2434.14 2724.13 376.25 o -6 9 0 6109.48 10098.90 1296.90 o -5 9 0 3726.06 3708.51 489.40 o -4 9 0 151.37 236.18 82.50 o -3 9 0 79.55 88.51 57.43 o -2 9 0 152.22 196.79 64.16 o -1 9 0 67.91 54.28 53.28 o 0 9 0 3922.48 4454.00 576.91 o 1 9 0 7455.15 7673.51 720.57 o 2 9 0 3180.65 3774.04 367.26 o 3 9 0 1899.75 1840.04 191.27 o 4 9 0 897.83 594.08 244.91 o 5 9 0 184.38 187.77 86.94 o 6 9 0 52.07 83.21 82.50 o 7 9 0 495.18 472.35 127.18 o -11 10 0 459.14 498.42 157.40 o -10 10 0 1124.11 1096.10 205.67 o -9 10 0 62.80 55.28 84.07 o -8 10 0 2042.53 3680.15 538.09 o -7 10 0 5172.79 4811.34 631.19 o -6 10 0 5796.94 5570.86 724.29 o -5 10 0 7186.14 9392.38 1205.09 o -4 10 0 1751.60 1699.65 247.78 o -3 10 0 391.42 388.28 95.67 o -2 10 0 432.24 392.58 87.08 o -1 10 0 1066.71 1043.53 162.70 o 0 10 0 4675.60 4270.96 552.85 o 1 10 0 5059.03 5191.20 494.40 o 2 10 0 756.60 796.05 99.53 o 3 10 0 518.32 540.79 81.88 o 4 10 0 1526.38 1595.09 261.81 o 5 10 0 263.47 265.97 107.85 o 6 10 0 233.93 273.99 110.28 o -10 11 0 2809.37 2616.71 380.69 o -9 11 0 245.82 210.40 105.13 o -8 11 0 2221.31 2163.84 322.11 o -7 11 0 4255.67 4443.25 599.11 o -6 11 0 2822.04 3153.09 437.98 o -5 11 0 3522.79 3304.05 447.43 o -4 11 0 5769.48 5292.29 687.91 o -3 11 0 2464.00 2357.48 325.12 o -2 11 0 413.94 433.25 101.26 o -1 11 0 169.12 90.52 61.30 o 0 11 0 1147.02 1038.95 161.56 o 1 11 0 1266.50 1152.24 177.31 o 2 11 0 446.89 416.11 71.43 o 3 11 0 665.19 657.69 139.07 o 4 11 0 795.59 796.33 159.84 o -9 12 0 48.64 77.20 111.14 o -8 12 0 1168.29 1201.65 233.17 o -7 12 0 687.97 529.50 138.64 o -6 12 0 356.21 363.93 117.44 o -5 12 0 2521.64 2338.86 334.57 o -4 12 0 5249.50 4858.18 636.35 o -3 12 0 2367.44 2053.12 294.33 o -2 12 0 9.49 -20.34 44.11 o -1 12 0 323.17 247.21 80.21 o 0 12 0 607.55 510.60 104.12 o 1 12 0 1801.20 1434.68 211.69 o 2 12 0 1205.80 1177.88 182.32 o 3 12 0 638.62 599.39 142.08 o -7 13 0 121.74 152.96 100.69 o -6 13 0 242.22 259.09 99.97 o -5 13 0 1558.15 1276.56 205.81 o -4 13 0 3060.59 2528.20 355.20 o -3 13 0 1306.58 959.89 166.14 o -2 13 0 14.01 -2.43 47.41 o -1 13 0 86.72 89.09 69.75 o 0 13 0 135.49 136.49 73.33 o 1 13 0 936.83 851.47 148.67 o -1 -13 1 2180.95 2006.72 282.87 o 0 -13 1 2338.60 2179.73 305.21 o 1 -13 1 2538.96 2200.93 307.93 o 2 -13 1 1897.85 1468.05 218.56 o 3 -13 1 185.39 83.64 68.32 o 4 -13 1 777.37 756.51 153.11 o 5 -13 1 1654.35 1360.63 219.28 o 6 -13 1 1292.92 1312.51 221.14 o 7 -13 1 2380.04 2071.46 317.53 o -3 -12 1 4.91 -0.57 63.02 o -2 -12 1 551.07 512.17 108.99 o -1 -12 1 2413.18 2429.23 334.29 o 0 -12 1 2639.69 2309.35 317.53 o 1 -12 1 3108.64 2719.55 367.80 o 2 -12 1 2761.36 2430.66 334.00 o 3 -12 1 649.77 619.45 129.05 o 4 -12 1 675.01 606.99 124.32 o 5 -12 1 1769.17 1698.21 255.51 o 6 -12 1 1456.40 1405.61 232.02 o 7 -12 1 2822.00 2671.14 384.84 o 8 -12 1 5670.13 5750.46 764.82 o 9 -12 1 1082.97 1153.24 233.46 o -4 -11 1 84.10 78.63 83.07 o -3 -11 1 11.81 -1.72 54.28 o -2 -11 1 229.10 269.03 58.81 o -1 -11 1 1560.86 1572.46 227.87 o 0 -11 1 3087.11 3158.24 421.22 o 1 -11 1 3270.86 3105.97 413.20 o 2 -11 1 1774.85 1748.48 252.08 o 3 -11 1 458.79 441.27 99.11 o 4 -11 1 680.79 658.55 128.76 o 6 -11 1 2438.66 2538.94 361.79 o 7 -11 1 8534.90 10253.44 1316.66 o 8 -11 1 9565.12 10853.70 1392.00 o 9 -11 1 1364.87 1482.37 255.08 o 10 -11 1 586.03 555.14 162.13 o -6 -10 1 1958.28 1936.97 314.38 o -5 -10 1 1127.42 1158.26 211.11 o -4 -10 1 46.14 89.23 51.68 o -3 -10 1 2.87 -1.03 29.82 o -2 -10 1 86.85 61.76 39.64 o -1 -10 1 3051.14 2843.01 379.12 o 0 -10 1 7430.07 7065.55 897.73 o 1 -10 1 4403.17 3926.07 511.31 o 2 -10 1 515.28 613.72 115.15 o 3 -10 1 433.76 402.32 95.82 o 4 -10 1 3.54 -10.89 51.99 o 5 -10 1 2513.01 2367.36 331.56 o 6 -10 1 5528.20 6966.73 903.46 o 7 -10 1 9615.18 10740.55 1368.80 o 8 -10 1 8296.39 8228.82 1059.58 o 9 -10 1 2174.85 2136.62 316.96 o 10 -10 1 154.32 253.36 183.90 o 11 -10 1 18.91 -25.22 55.16 o -7 -9 1 1245.40 1444.42 256.23 o -6 -9 1 1856.58 1922.22 310.51 o -5 -9 1 1094.02 332.16 624.24 o -4 -9 1 432.72 418.70 71.33 o -3 -9 1 1.70 35.45 37.29 o -2 -9 1 1495.82 1363.06 149.07 o -1 -9 1 7691.95 8056.36 754.73 o 0 -9 1 11897.44 11264.75 1412.62 o 1 -9 1 5493.19 5208.93 666.57 o 2 -9 1 943.26 894.72 142.08 o 3 -9 1 1426.65 1558.14 226.15 o 4 -9 1 864.46 851.76 142.65 o 5 -9 1 899.76 946.00 162.99 o 6 -9 1 4827.46 5148.78 670.29 o 7 -9 1 5001.65 6050.81 789.45 o 8 -9 1 3680.00 3763.08 506.87 o 9 -9 1 2165.99 2369.08 348.32 o 10 -9 1 513.39 477.94 138.64 o 11 -9 1 34.69 -7.63 59.94 o 12 -9 1 477.03 430.89 101.52 o -8 -8 1 1263.97 1574.90 269.84 o -7 -8 1 1375.88 1458.46 249.93 o -6 -8 1 1759.57 1752.07 284.87 o -5 -8 1 2963.44 1528.95 1107.48 o -4 -8 1 1552.12 1505.53 161.44 o -3 -8 1 10.85 33.95 30.70 o -2 -8 1 2460.59 2562.22 255.03 o -1 -8 1 10486.77 11883.94 1102.49 o 0 -8 1 11501.13 11673.37 1462.61 o 1 -8 1 8330.02 9392.81 1182.18 o 2 -8 1 4767.77 4420.48 568.89 o 3 -8 1 4156.51 4051.39 524.92 o 4 -8 1 2358.13 2951.28 393.58 o 5 -8 1 2360.81 2667.99 360.21 o 6 -8 1 7923.67 11272.06 1432.25 o 7 -8 1 3932.43 4601.80 606.27 o 8 -8 1 1025.64 1268.68 211.11 o 9 -8 1 2002.93 2042.81 291.61 o 10 -8 1 1373.78 1502.85 237.32 o 11 -8 1 38.76 31.08 59.04 o 12 -8 1 720.11 927.17 141.36 o -9 -7 1 698.48 673.58 152.68 o -8 -7 1 2002.36 1997.12 312.66 o -7 -7 1 1978.59 1897.44 295.47 o -6 -7 1 2138.11 2440.17 246.32 o -5 -7 1 5529.66 5428.99 515.61 o -4 -7 1 6940.94 7319.06 687.25 o -3 -7 1 216.03 322.73 55.38 o -2 -7 1 2443.68 2663.83 261.15 o -1 -7 1 3959.03 4265.58 407.25 o 0 -7 1 7221.44 7631.03 712.66 o 1 -7 1 7029.68 7337.97 924.94 o 2 -7 1 12967.43 14268.31 1782.00 o 3 -7 1 1980.85 2279.99 307.79 o 4 -7 1 330.97 298.48 70.18 o 5 -7 1 4223.76 4555.97 587.79 o 6 -7 1 7927.63 9933.34 1255.51 o 7 -7 1 4438.72 5404.15 697.50 o 8 -7 1 2100.07 2438.54 338.87 o 9 -7 1 3553.01 4772.10 628.18 o 10 -7 1 1238.55 1145.47 183.40 o 11 -7 1 32.54 18.09 48.66 o 12 -7 1 747.29 711.83 163.42 o 13 -7 1 1162.29 1049.98 216.27 o -10 -6 1 26.47 17.90 74.19 o -9 -6 1 340.77 444.57 124.75 o -8 -6 1 1174.29 1372.95 236.46 o -7 -6 1 1761.68 2050.69 318.96 o -6 -6 1 5007.80 5782.60 545.70 o -5 -6 1 8790.02 9792.88 910.77 o -4 -6 1 4272.50 3357.76 1249.71 o -3 -6 1 135.90 223.57 43.97 o -2 -6 1 1573.78 1877.53 187.91 o -1 -6 1 400.62 337.18 50.68 o 0 -6 1 4490.74 4952.40 466.30 o 1 -6 1 11971.02 11947.36 1491.25 o 2 -6 1 12926.39 14137.84 1763.09 o 3 -6 1 1198.03 1616.29 221.57 o 4 -6 1 1047.92 1130.33 163.56 o 5 -6 1 4727.07 5091.49 647.52 o 6 -6 1 11963.75 15415.54 1925.37 o 7 -6 1 14912.37 22135.93 2759.51 o 8 -6 1 8575.06 12703.01 1601.39 o 9 -6 1 5446.06 6211.22 797.76 o 10 -6 1 1871.75 2396.63 250.67 o 11 -6 1 243.06 302.64 74.37 o 12 -6 1 153.00 115.44 85.36 o 13 -6 1 408.29 261.53 106.85 o -11 -5 1 834.79 1002.14 195.64 o -10 -5 1 7.99 51.56 71.90 o -9 -5 1 8.31 8.74 58.87 o -8 -5 1 622.20 686.48 139.07 o -7 -5 1 4710.13 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