Acta Cryst. (2003). E59, o114-o116 [ doi:10.1107/S1600536802023413 ]
No syntax errors found ADDSYM reports no extra symmetry General Notes
REFLT_03 From the CIF: _diffrn_reflns_theta_max 28.42 From the CIF: _reflns_number_total 3701 Count of symmetry unique reflns 3137 Completeness (_total/calc) 117.98% TEST3: Check Friedels for noncentro structure Estimate of Friedel pairs measured 564 Fraction of Friedel pairs measured 0.180 Are heavy atom types Z>Si present no ALERT: MoKa measured Friedel data cannot be used to determine absolute structure in a light-atom study EXCEPT under VERY special conditions. It is preferred that Friedel data is merged in such cases.
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