Acta Cryst. (2003). E59, m74-m76  [ doi:10.1107/S1600536803001533 ]

Redetermination of chloro(triethanolaminato)zinc(II) at 150  K

M. Lutz and R. Bakker

Abstract: The X-ray crystal structure of the title compound, [ZnCl(C₆H₁₄NO₃)], was redetermined with a CCD area detector at 150  (2)  K. The crystal appeared to be non-merohedrally twinned. Appropriate handling of the twinning, together with the low measurement temperature, allowed the localization and refinement of the H atoms, which was not possible with the film data from the literature [Follner (1972), Acta Cryst. B28, 157-160]. The precision of the other geometrical data has also significantly improved.

Online 24 January 2003

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