Acta Crystallographica Section E

Structure Reports Online

Volume 59, Part 2 (February 2003)

	Cover illustration: Crystallographic characterization of this side product of a coupling reaction required synchrotron radiation in view of the weak diffraction from small crystals, which appear to be hollow in a scanning electron micrograph. - and nitro- stacking interactions are found in the crystal structure. See Kaafarani, Wex, Oliver, Krause Bauer & Neckers [Acta Cryst. E59, o227-o229].

• inorganic compounds
• metal-organic compounds
• organic compounds

inorganic compounds

metal-organic compounds

Acta Cryst. (2003). E59, m50-m52  [ doi:10.1107/S1600536802023425 ] Chloro[tris(perfluorophenyl)phosphine]gold(I) H. W. Chen and E. R. T. Tiekink Online 10 January 2003

Acta Cryst. (2003). E59, m53-m54  [ doi:10.1107/S1600536802023565 ] (O-Ethyldithiocarbonato)[tris(p-methoxyphenyl)phosphine]gold(I) S. Y. Ho and E. R. T. Tiekink Online 10 January 2003

Acta Cryst. (2003). E59, m55-m56  [ doi:10.1107/S1600536803000138 ] 4-Sulfido-bis(2-phenylthiolato)tetrakis(tricarbonyliron) M. Hu, C. Ma, X. Zhang, C. Fang, F. Chen, C. Chen and Q. Liu Online 17 January 2003

Acta Cryst. (2003). E59, m57-m58  [ doi:10.1107/S1600536803000813 ] A potassium crown ether complex with dichloroaurate(I) M. A. Hossain, D. R. Powell and K. Bowman-James Online 17 January 2003

Acta Cryst. (2003). E59, m59-m60  [ doi:10.1107/S1600536803000825 ] catena-Poly[[silver(I)--2,5-bis(4-pyridyl)-1,3,4-oxadiazole] nitrate], a one-dimensional coordination polymer exhibiting a double-chain supramolecular structure through hydrogen bonds Y.-M. Guo, H. Liu and X.-B. Leng Online 17 January 2003

Acta Cryst. (2003). E59, m61-m63  [ doi:10.1107/S1600536803000710 ] (Piperidine-N)[N-(salicylidene)phenylalaninato-3O,N,O']copper(II) R. J. Butcher, G. M. Mockler and O. McKern Online 24 January 2003

Acta Cryst. (2003). E59, m64-m66  [ doi:10.1107/S1600536803001193 ] A triclinic polymorph of octa-tert-butoxytetralithiumtetrasodium W. Clegg, A. M. Drummond, S. T. Liddle and R. E. Mulvey Online 24 January 2003

Acta Cryst. (2003). E59, m67-m68  [ doi:10.1107/S1600536803001077 ] Potassium 4-nitramino-1,2,4-triazolate A. D. Vasiliev, A. M. Astachov, L. A. Kruglyakova and R. S. Stepanov Online 24 January 2003

Acta Cryst. (2003). E59, m69-m71  [ doi:10.1107/S1600536802023024 ] A potassium cryptate-2,2,2 salt of tricarbonyl(4-cyclopentadiene)manganese L. Shao, S. J. Geib and N. J. Cooper Online 24 January 2003

Acta Cryst. (2003). E59, m72-m73  [ doi:10.1107/S1600536803001120 ] Bis[-bis(diphenylphosphino)methane]digold(I) bis(hexafluorophosphate) dichloromethane disolvate M. Wu, L. Zhang and Z. Chen Online 24 January 2003

Acta Cryst. (2003). E59, m74-m76  [ doi:10.1107/S1600536803001533 ] Redetermination of chloro(triethanolaminato)zinc(II) at 150 K M. Lutz and R. Bakker Online 24 January 2003

Acta Cryst. (2003). E59, m77-m79  [ doi:10.1107/S1600536803001600 ] Redetermination of nickel bis(dithiocarbamate) at 100 K S. Santos, S. Guilardi, J. A. L. C. Resende, M. M. M. Rubinger, M. R. L. Oliveira and J. Ellena Online 31 January 2003

Acta Cryst. (2003). E59, m80-m82  [ doi:10.1107/S1600536803001545 ] Undecacarbonyl(4-2-thiodithiobenzoato- 4C,S,S',S'')(triphenylphosphine)tetrafer E. A. Laifa, N. Benali-Cherif and F. Berrah Online 31 janvier 2003

Acta Cryst. (2003). E59, m83-m84  [ doi:10.1107/S1600536803002046 ] Tetrakis(tert-butyl 3-oxobutanoato)zirconium(IV) U. K. Urs, M. S. Dharmaprakash, S. A. Shivashankar and T. N. Guru Row Online 31 January 2003

Acta Cryst. (2003). E59, m85-m86  [ doi:10.1107/S1600536803001673 ] Bis(5-pentamethylcyclopentadienyl)[bis-5-syn-[2.2](4,7)indenophanyl]diruthenium(II) P. G. Jones, H. Hopf, T. Hartig and D. Döring Online 31 January 2003

Acta Cryst. (2003). E59, m87-m90  [ doi:10.1107/S1600536803001922 ] Bis(-8-hydroxy-7-iodoquinoline-5-sulfonato-3N,O:O')bis[triaquazinc(II)] tetrahydrate S. Francis, P. T. Muthiah, G. Bocelli and A. Cantoni Online 31 January 2003

Acta Cryst. (2003). E59, m91-m94  [ doi:10.1107/S1600536803001557 ] N-Phenethylbiguanidium tetrachlorozincate(II) M. Zhu, P. Yang and L. Lu Online 31 January 2003

organic compounds

Acta Cryst. (2003). E59, o106-o107  [ doi:10.1107/S1600536802023504 ] 2a'-Chloro-3,8-dioxo-1',2',2a',8a'-tetrahydrodispiro[cyclopropane-1,1'-cyclobuta[b]napthalene-2',1''-cyclopropane] L. Wang, A. Usman, H.-K. Fun, Y. Zhang and J.-H. Xu Online 10 January 2003

Acta Cryst. (2003). E59, o108-o110  [ doi:10.1107/S1600536802023334 ] Bis(DL-aspartic acid) oxalate M. Alagar, R. V. Krishnakumar, M. Subha Nandhini, T. S. Cameron and S. Natarajan Online 10 January 2003

Acta Cryst. (2003). E59, o111-o113  [ doi:10.1107/S1600536802023310 ] r-2,c-6-Bis(4-chlorophenyl)-3,5-dimethyltetrahydropyran-t-4-ol B. S. Krishnamoorthy, T. R. Sarangarajan, K. Thanikasalam, K. Panchanatheswaran and R. Jeyaraman Online 10 January 2003

Acta Cryst. (2003). E59, o114-o116  [ doi:10.1107/S1600536802023413 ] 5-Butylthevinone: stereochemistry of the Diels-Alder reaction of 5-butylthebaine with 3-buten-2-one W. Chen, M. D. Metcalf, A. Coop, J. L. Flippen-Anderson and J. R. Deschamps Online 10 January 2003

Acta Cryst. (2003). E59, o117-o118  [ doi:10.1107/S1600536802023449 ] 1-O-p-Toluenesulfonyl-2,3:4,5-di-O-isopropylidene-L-arabitol P. G. Jones, P. Kus and R. Celinski Online 10 January 2003

Acta Cryst. (2003). E59, o119-o120  [ doi:10.1107/S1600536802022870 ] 2,7-Dimethyl-4,5-bis(trimethylsilyl)octa-2,3,5,6-tetraene P. G. Jones, P. Bubenitschek, H. Hopf and R. Stamm Online 10 January 2003

Acta Cryst. (2003). E59, o121-o123  [ doi:10.1107/S1600536802023693 ] (1E,3S,4aR,12aR)-3-Isopropenyl-8-methoxy-3,4,4a,5,6,11,12,12a-octahydro-1(2H)-chrysenone oxime H. Kooijman and A. L. Spek Online 10 January 2003

Acta Cryst. (2003). E59, o124-o126  [ doi:10.1107/S1600536802023620 ] N-[N-(Furan-2-carbonyl)hydrazinothiocarbonyl]benzamide B. M. Yamin and M. S. M. Yusof Online 10 January 2003

Acta Cryst. (2003). E59, o127-o128  [ doi:10.1107/S160053680300076X ] Trimesic acid bis(N,N-dimethylformamide) solvate at 150 K S. H. Dale and M. R. J. Elsegood Online 10 January 2003

Acta Cryst. (2003). E59, o129-o131  [ doi:10.1107/S160053680202370X ] Diphenyl (3,3-diphenoxycyclohexyl)phosphonate I. A. Guzei, R. Stockland and T. W. Tennis Online 10 January 2003

Acta Cryst. (2003). E59, o132-o134  [ doi:10.1107/S1600536803000783 ] 4-[2-(4-Pyridyl)ethyl]pyridinium nitrate trihydrate F. A. Almeida Paz, Y. Z. Khimyak and J. Klinowski Online 17 January 2003

Acta Cryst. (2003). E59, o135-o137  [ doi:10.1107/S1600536802023632 ] 3-{3,3-Dimethylspiro[2,3-dihydro-1H-indole-2,3'-(3'H-naphtho[2,1-b][1,4]oxazin)]-1-yl}propionic acid Y. Gao, W. Zou, W. Zhang, J. Li and J. Meng Online 17 January 2003

Acta Cryst. (2003). E59, o138-o140  [ doi:10.1107/S1600536803000126 ] 1-(4-Methacryloyloxyphenyl)-3-(3-bromophenyl)prop-2-en-1-one T. Ravishankar, K. Chinnakali, S. Nanjundan, S. Radhakrishnan, A. Usman and H.-K. Fun Online 17 January 2003

Acta Cryst. (2003). E59, o141-o142  [ doi:10.1107/S1600536803000795 ] L-Valinium hydrogenphosphite L. Bendheif, N. Benali-Cherif, L. Benguedouar, K. Bouchouit and H. Merazig Online 17 January 2003

Acta Cryst. (2003). E59, o143-o144  [ doi:10.1107/S160053680202353X ] (Z)-7-Chloro-3-(diméthylaminométhylène)-1-méthyl-5-phényl-1,3-dihydro-2H-[1,4]benzodiazépin-2-one R. Benelbaghdadi, R. A. Hasnaoui, J. P. Lavergne, M. Ait Itto and M. Pierrot Online 17 janvier 2003

Acta Cryst. (2003). E59, o145-o147  [ doi:10.1107/S1600536802023723 ] An unsymmetrical tetrathiafulvalene with a fused 1,2,5-thiadiazole ring and an ethylenedioxy group M. Tomura and Y. Yamashita Online 17 January 2003

Acta Cryst. (2003). E59, o148-o150  [ doi:10.1107/S160053680300014X ] Hydrazine carbodithioic acid pyridinium-2-yl methyl ester chloride K. A. Crouse, K. T. Chew, B. M. Yamin, S. W. Ng and M. T. H. Tarafder Online 17 January 2003

Acta Cryst. (2003). E59, o151-o152  [ doi:10.1107/S1600536802023711 ] N-Benzoyl-N'-phenylthiourea B. M. Yamin and M. S. M. Yusof Online 17 January 2003

Acta Cryst. (2003). E59, o153-o154  [ doi:10.1107/S1600536803000709 ] 7-Ethylamino-4-(trifluoromethyl)coumarin J. P. Jasinski, J. M. Jasinski, Y. Li and D. J. Crosby Online 17 January 2003

Acta Cryst. (2003). E59, o155-o157  [ doi:10.1107/S1600536803000114 ] 4,4',5,5'-Tetramethyltetrathiafulvalene-1,4-dinitrobenzene (1/1) A. S. Batsanov and S. B. Lyubchik Online 17 January 2003

Acta Cryst. (2003). E59, o158-o160  [ doi:10.1107/S1600536803000692 ] 1'-Deoxy-1'-hydroxymethyl-1,2'-O-isopropylidene--D-arabinofuranose B. Doboszewski and A. Y. Nazarenko Online 17 January 2003

Acta Cryst. (2003). E59, o161-o163  [ doi:10.1107/S1600536803000722 ] N-[3,5-Bis(trifluoromethyl)phenyl]salicylaldimine N. Karadayi, S. Gözüyesil, B. Güzel and O. Büyükgüngör Online 17 January 2003

Acta Cryst. (2003). E59, o164-o166  [ doi:10.1107/S1600536803000965 ] 3-Oxoolean-12-en-20-yl -methylcarboxylate A. C. Doriguetto, L. P. Duarte, J. A. Ellena, G. D. F. Silva, Y. P. Mascarenhas and A. B. Cota Online 17 January 2003

Acta Cryst. (2003). E59, o167-o168  [ doi:10.1107/S160053680300093X ] A dimer of 7-cyanodibenzobarrelene P. G. Jones, P. Bubenitschek, H. Hopf and B. Witulski Online 17 January 2003

Acta Cryst. (2003). E59, o169-o170  [ doi:10.1107/S1600536803000941 ] 9,10-Dicyanodibenzoisobullvalene P. G. Jones, H. Hopf and B. Witulski Online 17 January 2003

Acta Cryst. (2003). E59, o171-o173  [ doi:10.1107/S1600536803000862 ] 6(S)-Methyl-3(S)-(1-methylethyl)piperazin-2-one P. Sawatzki, T. Mikeska, K. Sandhoff, M. Nieger and T. Kolter Online 17 January 2003

Acta Cryst. (2003). E59, o174-o176  [ doi:10.1107/S1600536803000989 ] catena-Poly[[bis(4-cyanobenzoato)copper(II)]--4,4'-bipyridine-2N:N'] H.-Y. He and L.-G. Zhu Online 17 January 2003

Acta Cryst. (2003). E59, o177-o179  [ doi:10.1107/S1600536802023322 ] 2-Bromo-N-[3-bromo-1-(phenylsulfonyl)indol-2-ylmethyl]-4-methylaniline M. M. Govind, J. Govindaraj, V. Rajakannan, D. Velmurugan, M.-J. Kim, P. C. Srinivasan and S. Kannadasan Online 17 January 2003

Acta Cryst. (2003). E59, o180-o182  [ doi:10.1107/S1600536803000953 ] Guaninium sulfate monohydrate A. Cherouana, N. Benali-Cherif and L. Bendjeddou Online 17 January 2003

Acta Cryst. (2003). E59, o183-o185  [ doi:10.1107/S1600536803000850 ] Bis(cinchonidinium) L-tartrate dihydrate H. Zhang, Z.-Y. Lin, Z.-H. Zhou and S. W. Ng Online 17 January 2003

Acta Cryst. (2003). E59, o186-o187  [ doi:10.1107/S1600536803001016 ] 6,6-Dimethyl-2-(1-methylethenyl)-3,4,5-tris(1-methylethylidene)-1-(2-methylpropen-1-yl)cyclohexane P. G. Jones, P. Bubenitschek, H. Hopf and T. Höpfner Online 17 January 2003

Acta Cryst. (2003). E59, o188-o189  [ doi:10.1107/S1600536803001028 ] [2.2](2,5)Furanoparacyclophane-12,13-dicarbaldehyde P. G. Jones, P. Bubenitschek, H. Hopf and B. Witulski Online 17 January 2003

Acta Cryst. (2003). E59, o190-o192  [ doi:10.1107/S1600536803001004 ] Bis(4-dimethylaminopyridinium) 1,2-difluorodiphosphate R. Sluka, M. Necas and M. Cerník Online 24 January 2003

Acta Cryst. (2003). E59, o193-o194  [ doi:10.1107/S1600536803001089 ] 1-Ethyl-2-nitroguanidine A. D. Vasiliev, A. M. Astachov, M. S. Molokeev, L. A. Kruglyakova and R. S. Stepanov Online 24 January 2003

Acta Cryst. (2003). E59, o195-o197  [ doi:10.1107/S1600536803001247 ] Bis(melaminium) hydrogen phosphite tetrahydrate L. E. Gordon and W. T. A. Harrison Online 24 January 2003

Acta Cryst. (2003). E59, o198-o199  [ doi:10.1107/S160053680300120X ] 2-(4-Methoxyphenyl)-5-(4-methylpent-3-enyl)-2,3,3a,4,7,7a-hexahydro-1H-isoindole-1,3-dione D. E. Lynch and I. McClenaghan Online 24 January 2003

Acta Cryst. (2003). E59, o200-o202  [ doi:10.1107/S1600536803001235 ] 5-Amino-4-(4-dimethylaminophenyl)-2-(4-methoxyphenyl)-7-(pyrrolidin-1-yl)-1,6-naphthyridine-8-carbonitrile S. Bhaskaran, M. Yogavel, V. Rajakannan, R. Krishna, D. Velmurugan and V. Raghukumar Online 24 January 2003

Acta Cryst. (2003). E59, o203-o205  [ doi:10.1107/S1600536803001119 ] Phyllanthin from the plant Phyllanthus amarus V. Rajakannan, M. S. Sripathi, S. Selvanayagam, D. Velmurugan, U. D. Murthy, M. Vishwas, S. P. Thyagarajan, S. Shanmuga Sundara Raj and H.-K. Fun Online 24 January 2003

Acta Cryst. (2003). E59, o206-o208  [ doi:10.1107/S1600536803001107 ] -Alaninium trichloroacetate at 105 K K. Rajagopal, R. V. Krishnakumar, M. Subha Nandhini, A. Mostad and S. Natarajan Online 24 January 2003

Acta Cryst. (2003). E59, o209-o211  [ doi:10.1107/S160053680202295X ] DL-Phenylalaninium maleate at 123 K M. Alagar, M. Subha Nandhini, R. V. Krishnakumar, A. Mostad and S. Natarajan Online 24 January 2003

Acta Cryst. (2003). E59, o212-o214  [ doi:10.1107/S1600536803001314 ] (5S,6R)-4,5-Dimethyl-6-phenyl-3-trimethylacetyl-2H-1,3,4-oxadiazinan-2-one G. M. Ferrence, J. M. Esken, J. R. Blackburn and S. R. Hitchcock Online 24 January 2003

Acta Cryst. (2003). E59, o215-o217  [ doi:10.1107/S1600536803001144 ] Dichloro{2-[N-(2-hydroxyethylammonioethyl)iminomethyl]phenolate}zinc(II) A. Usman, H.-K. Fun, S. Chantrapromma, H.-L. Zhu and Q.-X. Liu Online 24 January 2003

Acta Cryst. (2003). E59, o218-o219  [ doi:10.1107/S1600536803001338 ] [2.2](2,7)Oxepinoparacyclophane-4,5-dicarbonitrile P. G. Jones, P. Bubenitschek, H. Hopf and B. Witulski Online 24 January 2003

Acta Cryst. (2003). E59, o220-o221  [ doi:10.1107/S160053680300134X ] 2,3:9,10-Dibenzotricyclo[5.3.0.04,8]deca-2,5,9-triene-6,7-dicarbonitrile P. G. Jones, P. Bubenitschek, H. Hopf and B. Witulski Online 24 January 2003

Acta Cryst. (2003). E59, o222-o224  [ doi:10.1107/S1600536803001405 ] 2-Amino-4-(4-chlorophenylthio)-5-phenyl-6-(1-piperidyl)pyrimidine D. E. Lynch and I. McClenaghan Online 24 January 2003

Acta Cryst. (2003). E59, o225-o226  [ doi:10.1107/S1600536803001363 ] 2-(4-Bromophenyl)-5-methyl-2,3-dihydro-4H-1,2,4-triazol-3-one S. Thamotharan, V. Parthasarathi, R. K. Hunnur, B. Badami and A. Linden Online 24 January 2003

Acta Cryst. (2003). E59, o227-o229  [ doi:10.1107/S1600536803001569 ] --Stacking and nitro--stacking interactions of 1-(4-nitrophenyl)-4-phenyl-2,4-bis(phenylethynyl)butadiene B. R. Kaafarani, B. Wex, A. G. Oliver, J. A. Krause Bauer and D. C. Neckers Online 24 January 2003

Acta Cryst. (2003). E59, o230-o231  [ doi:10.1107/S1600536803001624 ] Ethyl 5-ethoxymethylene-2-methyl-6-oxo-4-phenyl-1,4,5,6-tetrahydropyridine-3-carboxylate H. Novoa de Armas, O. M. Peeters, N. M. Blaton, C. J. De Ranter, M. Suárez Navarro, Y. Verdecia Reyes, E. Ochoa Rodríguez and E. Salfrán Online 31 January 2003

Acta Cryst. (2003). E59, o232-o233  [ doi:10.1107/S1600536803001612 ] Reinvestigation of 5,12-dihydro-5,12-dimethylquino[2,3-b]acridine-7,4-dione J. Mizuguchi and T. Senju Online 31 January 2003

Acta Cryst. (2003). E59, o234-o236  [ doi:10.1107/S1600536803001326 ] N-(3-Chlorophenyl)--(2-hydroxyphenyl)nitrone: supramolecular aggregation through - and C-H interactions E. Mothi Mohamed, S. Chandrasekar and K. Panchanatheswaran Online 31 January 2003

Acta Cryst. (2003). E59, o237-o239  [ doi:10.1107/S1600536803001387 ] Spiro[3,4-bis(4-chlorophenyl)-4,5-dihydroisoxazole-5,3'-flavan-4'-one] A. Jeyabharathi, M. N. Ponnuswamy, S. Manikandan and R. Raghunathan Online 31 January 2003

Acta Cryst. (2003). E59, o240-o241  [ doi:10.1107/S1600536803001399 ] Spiro[3-(4-chlorophenyl)-4-(4-methylphenyl)-4,5-dihydroisoxazole-5,3'-flavan-4'-one] A. Jeyabharathi, M. N. Ponnuswamy, S. Manikandan and R. Raghunathan Online 31 January 2003

Acta Cryst. (2003). E59, o242-o243  [ doi:10.1107/S1600536803001302 ] Diethyl (4-tert-butyl-1,3-thiazol-2-ylaminomethylene)malonate D. E. Lynch and I. McClenaghan Online 31 January 2003

Acta Cryst. (2003). E59, o244-o246  [ doi:10.1107/S1600536803002009 ] 5,6-Dioxo-1,10-phenanthrolin-1-ium bromide at 120 K J. A. S. Bomfim, C. A. L. Filgueiras, R. A. Howie and J. L. Wardell Online 31 January 2003

Acta Cryst. (2003). E59, o247-o249  [ doi:10.1107/S1600536803002034 ] 4,11-Bis(4-chlorophenyl)-3,10-bis(2,6-dichlorophenyl)-1,8-dioxa-2,9-diazadispiro[4.1.4.3]tetradeca-2,9-dien-6-one 0.75-hydrate X.-F. Li, Y.-Q. Feng, J.-P. Zhuang and X.-F. Hu Online 31 January 2003

Acta Cryst. (2003). E59, o250-o252  [ doi:10.1107/S1600536803001909 ] 3-tert-Butyl-5-[(4-methoxybenzylidene)amino]-1-phenylpyrazole J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, E. Rengifo and R. Abonia Online 31 January 2003

Acta Cryst. (2003). E59, o253-o254  [ doi:10.1107/S1600536803002022 ] Dimethylethylammonium bromide M. Scheibitz, H.-W. Lerner and M. Bolte Online 31 January 2003

Acta Cryst. (2003). E59, o255-o257  [ doi:10.1107/S1600536803002137 ] (Benzoylmethyl)triphenylphosphonium iodide: supramolecular zigzag chains via C-HO hydrogen bonding stabilized by C-HI interactions M. Baby Mariyatra, B. Kalyanasundari, K. Panchanatheswaran and A. E. Goeta Online 31 January 2003

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