Acta Cryst. (2003). E59, m69-m71  [ doi:10.1107/S1600536802023024 ]

A potassium cryptate-2,2,2 salt of tricarbonyl(⁴-cyclopentadiene)manganese

L. Shao, S. J. Geib and N. J. Cooper

Online 24 January 2003

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.002 Å
• R factor = 0.036
• wR factor = 0.101
• Data-to-parameter ratio = 26.3

checkCIF results

No syntax errors found



ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           32.47                 
         From the CIF: _reflns_number_total               9907                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns        10733                           
         Completeness (_total/calc)             92.30%                          
          Alert C: < 95% complete                                               


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check

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