Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 59| Part 3

ISSN: 2056-9890

March 2003 issue

Highlighted illustration

Cover illustration: Perhaps as a result of its highly deliquescent nature, the X-ray crystal structure of trichloroacetic acid has not been reported until now. This low-temperature study reveals that the molecules form centrosymmetric pairs, leading to hydrogen-bonded dimers. See Rajagopal, Mostad, Krishnakumar, Subha Nandhini & Natarajan [Acta Cryst. E59, o316-o318].

inorganic compounds

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Dilithium selenate hydrate, Li₂SeO₄·H₂O

M. G. Johnston and W. T. A. Harrison

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The cluster compound PrMo_7.6O₁₄

N. Barrier and P. Gougeon

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Holmium chloride oxoselenate(IV), HoClSeO₃

M. S. Wickleder

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Sodium magnesium tris(dihydrogenphosphite) monohydrate, NaMg(H₂PO₃)₃·H₂O

R. Ouarsal, A. Alaoui Tahiri, M. Lachkar, M. Dusek, K. Fejfarová and B. El Bali

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Sc₂TiO₅, an entropy-stabilized pseudobrookite-type compound

U. Kolitsch and E. Tillmanns

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HgB₄O₇, a member of the isotypic M^IIB₄O₇ family (M^II = Mg, Mn, Zn, Cd)

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Bi₃ScMo₂O₁₂: the difference from Bi₃FeMo₂O₁₂

U. Kolitsch and E. Tillmanns

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metal-organic compounds

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[4](1)(2,3-Diazabuta-1,3-diene)ferrocenophane

B. M. Yamin and N. M. Ali

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Chloro(P-{2-[N-(2,6-diisopropylphenyl)iminomethyl]phenyl}-P,P-diphenylphosphine-κ²N,P)methylpalladium(II)

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Dichloro(2,2′,4,4′,6,6′-hexamethyl-m-terphenyl)bis(N-methylimidazole)(tetrahydrofuran)samarium(III) toluene disolvate

G. W. Rabe, B. Rhatigan, A. L. Golen and A. L. Rheingold

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Tetrakis[4-amino-N-(2-hydroxyethyl)pyridinium] hexacosaoxooctamolybdate

Y. Yan, C.-D. Wu, J.-H. Liu, Q.-Z. Zhang and C.-Z. Lu

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(η³-Allyl)[(S)-(+)-(2-pyrrolidinylmethyl)pyrrolidine]palladium(II) trifluoromethanesulfonate

M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson

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Undecacarbonyl(μ₄-2-thiodithiobenzoato-κ⁴C,S,S′,S′′)(trimethylphosphite)tetrafer

E. A. Laifa, N. Benali-Cherif and H. Merazig

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[1,1′-Bis(diphenylphosphino)ferrocene-κ²P,P′](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate dichloromethane disolvate

M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson

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Poly[[bis(4,4′-bipyridine)bis(μ-oxalato)trizinc(II)]-di-μ-4,4′-bipyridine-μ-oxalato]

K. J. Nordell, K. A. Higgins and M. D. Smith

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Anhydrous octaguanidinium hexatungstoplatinate(IV)

U. Lee, S.-J. Jang, H.-C. Joo and K.-M. Park

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Twinned bis[tris(1,2-ethanediamine-κ²N,N′)manganese(II)] pentaselenodiantimonate(III)

C. Näther, F. Wendland and W. Bensch

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Dichloro(N,N-dimethylethylenediamine)cadmium(II): a novel two-dimensional chloro-bridged coordination polymer

H.-D. Bian, W. Gu, S.-P. Yan, D.-Z. Liao and Z.-H. Jiang

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4-(Tri-tert-butoxysilylthiomercurio)benzoic acid

J. Chojnacki, A. Walaszewska, E. Baum and W. Wojnowski

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Bis{4-[α-(4-acetylphenylimino)benzyl]-3-methyl-1-phenylpyrazol-5-onato}aquacopper(II)

J.-L. Wang, F. Ding and F.-M. Miao

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(1,2-Diaminocyclohexane)silver(I) trifluoromethanesulfonate

A. Usman, H.-K. Fun, H.-L. Zhu and X.-J. Wang

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A dinuclear rhenium complex, {[(C₁₈H₂₄N₂)Re(CO)₃]₂(μ-C₁₂H₁₂N₂)}(PF₆)₂·2CH₂Cl₂

S.-S. Sun, D. T. Tran, P. Y. Zavalij, S. R. J. Oliver and A. J. Lees

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Tetrakis(μ₃-phenoxo-acetonitrilelithium), a tetrameric lithium aryloxide with a cubane core

M. Tombul, R. J. Errington, R. A. Coxall and W. Clegg

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organic compounds

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Bis[(3,5-dimethylpyrazol-1-yl)ethyl] disulfide

A. M. Mills, M.-C. Chalbot, E. Bouwman and A. L. Spek

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2-Hydroxy-4,4-dimethyl-N-(4-methylphenyl-6-oxocyclohexanylacetamide

S. Selvanayagam, M. Yogavel, V. Rajakannan, D. Velmurugan, S. Shanmuga Sundara Raj and H.-K. Fun

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1,2-Bis[bis(4-methoxyphenyl)hydroxymethyl]benzene

K. A. Carey, W. Clegg, M. R. J. Elsegood, B. T. Golding and H. Maskill

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3-Benzoyl-2-hydroxy-2-methylchromene

M. Yogavel, D. Velmurugan, K. Sekar, H. Schenk, J. Fraanje, R. Peschar, S. Srinivasan, P. R. Athappan and Z. A. Rafi

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N,N,N′,N′-Tetrakis(2-pyridiniomethyl)ethylenediamine tetraperchlorate

S. S. Gunatilleke and R. E. Norman

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4-[(2,6-Dichlorophenyl)(hydroxyimino)methyl]-1,5-dimethyl-2-phenyl-1,2-dihydropyrazol-3-one

X.-F. Li, Y.-Q. Feng, J.-P. Zhuang and X.-F. Hu

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1-(4-Methoxypyrimidin-2-yl)-3-(2-nitrophenylsulfonyl)urea

N. Ma, Z.-M. Li, J.-G. Wang and H.-B. Song

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L-Prolinium trichloroacetate at 105 K

K. Rajagopal, R. V. Krishnakumar, A. Mostad and S. Natarajan

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(rac-2SR,3RS,5SR)-Spiro[3-methoxycarbonyl-1-azabicyclo[3.3.0]octane-2,1′-acenaphthylen]-2′-one

T. V. Sundar, V. Parthasarathi, C. Álvarez-Rúa, S. García-Granda, I. Sharma, R. T. Pardasani and R. C. Mehrotra

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Methyl 2,3,6-tri-O-benzoyl-α-D-xylo-hexopyranosid-4-ulose

O. Renaudet, P. Dumy, C. Philouze and M.-T. Averbuch

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5-Ethyl-6-oxo-4-thioxo-1,3,2-oxazaphospholidino[3,2-a][1,3,2]benzodiazaphosphorine

S.-L. Deng, R.-Y. Chen, X.-B. Leng and L.-H. Weng

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4-(2-Isonicotinoylhydrazino)-4-oxobutanoic acid

A. C. Doriguetto, C. H. T. de Paula Silva, D. G. Rando, E. I. Ferreira and J. A. Ellena

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7,14-Dioxatetracyclo[14.2^4,5.2^19,20.2^21,22.2^23,24]tetracosa-1,3,5,9,11,15,17,19,21,23-decaene

T. Ravishankar, K. Chinnakali, P. Rajakumar, V. Murali, A. Usman and H.-K. Fun

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7,16-Dioxatetracyclo[16.2^4,5.2^21,22.2^23,24.0^9,14]tetracosa-1,3,5,9,11,13,17,19,21,23-decaene

T. Ravishankar, K. Chinnakali, P. Rajakumar, V. Murali, A. Usman and H.-K. Fun

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Ladders in the supramolecular structure of 1-(4-bromophenyl)-3-[2-(2-hydroxyethyl)amino-5-nitroanilino]-1-propanone dimethylformamide solvate

J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, B. Insuasty and Y. Caldas

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16α,17α-Epoxy-20-oxopregn-5-ene-3β,21-diyl diacetate

L. C. R. Andrade, J. A. Paixao, M. J. M. de Almeida, R. M. L. M. Martins, H. I. M. Soares, M. J. S. M. Moreno, M. L. Sá e Melo and A. S. Campos Neves

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6-Methyl-11a,12-dihydro-6H-quino[3,2-b][1,4]benzothiazine: an amidine formed under unusual conditions

R. L. Luck, K. Li and D. K. Bates

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2-Amino-5-butyl-4-methyl-1,3-thiazol-3-ium nitrate

B. Zarychta, G. Spaleniak and J. Zaleski

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2,3-Dimethyl 5-isopropyl 1-ethoxymethyl-6-methyl-4-(3-nitrophenyl)-1,4-dihydropyridine-2,3,5-tricarboxylate

V. Vrabel, D. Oktavec and Š. Marchalín

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3,3-Bis(methylthio)-2-oxo-N-phenylpropanamide

J. R. Deschamps, L. S. Suwandi and M. Konaklieva

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2-tert-Butyl-4-piperidino-β-diketimine

M.-S. Zhou, D.-S. Liu, S.-P. Huang and H.-B. Tong

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2,2′-Diamino-4,4′-bi-1,3-thiazole

J.-G. Liu, D.-J. Xu and C.-H. Hung

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2,3-Dithien-2-ylquinoxaline

G. Crundwell, D. Sayers, S. R. Herron and K. A. Kantardjieff

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Trichloroacetic acid at 105 K

K. Rajagopal, A. Mostad, R. V. Krishnakumar, M. Subha Nandhini and S. Natarajan

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(S)-Phenylsuccinic acid

A. Fischer and V. M. Profir

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2,5-Diethoxycarbonyl-6-methyl-4-phenylthieno[2,3-b]pyridine

H. Novoa de Armas, O. M. Peeters, N. M. Blaton, C. J. De Ranter, E. Salfrán, M. Suárez Navarro, E. Ochoa Rodríguez and Y. Verdecia Reyes

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4,4-Dimethyl-2-(2-methyl-1-propenyl)-2,6-diphenyl-2,3,4,5-tetrahydropyrimidine

P. G. Jones, H. Hopf and H. W. Lautenbach

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4-Iodotetrathiafulvalene–1,4-dinitrobenzene (1/1)

A. S. Batsanov and S. B. Lyubchik

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N,N′-Bis(3-hydroxyphenyl)-1,8:4,5-naphthalenetetracarboximide dimethyl sulfoxide disolvate

G. D. Fallon, M.A.-P. Lee and S. J. Langford

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3-(2,6-Dichlorophenyl)-8-ethyl-4-phenyl-1-oxa-6-thia-2,8-diazaspiro[4.4]non-2-ene-7,9-dione

X.-F. Li, Y.-Q. Feng and Y.-F. Gu

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N-(3-Methoxypropyl)-1,8-naphthalimide

B. Zarychta, J. Zaleski, V. Prezhdo and B. Uspenskiy

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Benzotriazol-1-yl 4,6-di-O-acetyl-2,3-dideoxy-α-D-erythro-hex-2-enpyranoside

J. N. Low, J. Cobo, M. D. López, M. Nogueras and A. Sánchez

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3-{2-[2-(3,5-Dinitro-2-oxidophenyl)ethyl]-3,3-dimethyl-3H-indol-1-ium-1-yl}propanoic acid bis(dimethylformamide) solvate

W. Zou, P. Chen, Y. Gao and J. Meng

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N′-Benzoyl-N-p-bromophenylthiourea

B. M. Yamin and M. S. M. Yusof

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Salicylaldehyde 4-nitrophenylhydrazone

S. Shan, D.-J. Xu, J.-Y. Wu and M. Y. Chiang

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2-Hydroxycyclohexene-1-carboxylic acid: the enol isomer of 2-oxocyclohexane-1-carboxylic acid

A. J. Kresge, A. J. Lough and Y. Zhu

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The acetyl derivative of humirianthol

R. A. Burrow, A. F. Morel, I. B. Graebner, D. H. Farrar and A. J. Lough

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Absolute configuration of diacetylated acrenol as its chloroform solvate

R. A. Burrow, A. F. Morel, I. B. Graebner, A. J. Lough and D. H. Farrar

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2-Cyano-3-dimethylamino-N-(2,5-dimethylphenyl)acrylamide

Ompraba, A. Aysha, M. Yogavel, D. Velmurugan, S. Selvi, P. T. Perumal, S. Shanmuga Sundara Raj, H.-K. Fun and Z. A. Rafi

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1,1′-(1,2-Ethanediyl)bis(2,3-dihydro-3-methyl-1H-imidazole-2-thione)

Q. Liu, D. Shi, K. Yu and J. Xu

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N,N′-Bis(benzamidothiocarbonyl)hydrazine dimethyl sulfoxide disolvate

B. M. Yamin and M. S. M. Yusof

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7-Nitro-1,2,3a,4-tetrahydrobenzo[b][1,3]oxazolo[3,2-d]oxazine: a new heterocycle

S. Vishnu Vardhan Reddy, A. Sivalakshmi Devi, K. Vyas, V. Venugopal Rao, Y. Koteswar Rao, A. Venkateswarlu and P. K. Dubey

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2-(5,7-Dihydroxy-4-oxo-4H-chromen-3-yl)-5-methoxy-1,4-benzoquinone (isoflavonequinone)

T. Aree, S. Tip-pyang, S. Seesukphronrarak and N. Chaichit

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N,N′-Bis(tert-butoxycarbonyl)thiourea

C. Li, K. W. Y. Chan and L. Szeto

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Ethyl (Z)-3-bromo-2-[(tert-butoxycarbonyl)amino]-3-phenylacrylate

P. G. Jones and S. Jäger

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1,6-Dibenzoyloxy-2:4,3:5-O²:O⁴,O³:O⁵-bis(phenylboronoyloxy)-D-mannitol

P. J. Duggan, D. G. Humphrey, D. J. Price and E. M. Tyndall

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N-(4-Bromophenyl)pyridine-2-carboxamide

J. Y. Qi, Q. Y. Yang, K. H. Lam, Z. Y. Zhou and A. S. C. Chan

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Diethyl 2-methyl-6-(2-thiazolidinyl)-4-(2-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate

V. Vrábel, J. Kožíšek and Š. Marchalín

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2,4-Dinitrophenyl 4-toluenesulfonate: molecular aggregation through weak C—H⋯O interactions

N. Vembu, M. Nallu, J. Garrison and W. J. Youngs

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3,9-Dimethoxy-6a,11a-dihydro-6H-benzo[4,5]furo[3,2-c]chromene-4,10-diol monohydrate

T. Aree, S. Tip-pyang, S. Paramapojn and N. Chaichit

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4-(4-Bromophenyl)-2,5-diethoxycarbonyl-6-methylthieno[2,3-b]pyridine

H. Novoa de Armas, O. M. Peeters, N. M. Blaton, C. J. De Ranter, M. Suárez Navarro, E. Salfrán Solano, Y. Verdecia Reyes and E. Ochoa Rodríguez

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Per(3-deoxy)-α-cyclomannin: an n-butanol hexahydrate inclusion complex

H. J. Lindner, F. W. Lichtenthaler, K. Fujita, C. Yang, D.-Q. Yuan and Y. Nogami

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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