Acta Cryst. (2003). E59, m119-m121  [ doi:10.1107/S1600536803003386 ]

Twinned bis[tris(1,2-ethanediamine-²N,N')manganese(II)] pentaselenodiantimonate(III)

C. Näther, F. Wendland and W. Bensch

Online 21 February 2003

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.009 Å
• R factor = 0.030
• wR factor = 0.075
• Data-to-parameter ratio = 23.2

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.01                 
         From the CIF: _reflns_number_total               6991                  
         TEST2: Reflns within _diffrn_reflns_theta_max                          
         Count of symmetry unique reflns         7542                           
         Completeness (_total/calc)             92.69%                          
          Alert C: < 95% complete                                               

PLAT_420  Alert C D-H Without Acceptor       N(4)   -   H(7N)             ?

PLAT_420  Alert C D-H Without Acceptor       N(4)   -   H(8N)             ?

PLAT_420  Alert C D-H Without Acceptor       N(5)   -   H(9N)             ?

PLAT_420  Alert C D-H Without Acceptor       N(10)  -   H(20N)            ?

PLAT_420  Alert C D-H Without Acceptor       N(11)  -   H(21N)            ?


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 6 Alert Level C = Please check

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