Acta Cryst. (2003). E59, m105-m107  [ doi:10.1107/S1600536803003507 ]

(³-Allyl)[(S)-(+)-(2-pyrrolidinylmethyl)pyrrolidine]palladium(II) trifluoromethanesulfonate

M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson

Online 21 February 2003

Key indicators

• Single-crystal X-ray study
• T = 180 K
• Mean (C-C) = 0.005 Å
• R factor = 0.032
• wR factor = 0.069
• Data-to-parameter ratio = 18.9

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.46                 
         From the CIF: _reflns_number_total               3927                  
         Count of symmetry unique reflns         2263                           
         Completeness (_total/calc)            173.53%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured      1664                           
         Fraction of Friedel pairs measured     0.735                           
         Are heavy atom types Z>Si present          yes                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.          

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