Acta Crystallographica Section E

Structure Reports Online

Volume 59, Part 3 (March 2003)

	Cover illustration: Perhaps as a result of its highly deliquescent nature, the X-ray crystal structure of trichloroacetic acid has not been reported until now. This low-temperature study reveals that the molecules form centrosymmetric pairs, leading to hydrogen-bonded dimers. See Rajagopal, Mostad, Krishnakumar, Subha Nandhini & Natarajan [Acta Cryst. E59, o316-o318].

• inorganic compounds
• metal-organic compounds
• organic compounds

inorganic compounds

metal-organic compounds

Acta Cryst. (2003). E59, m95-m96  [ doi:10.1107/S1600536803002691 ] [4](1)(2,3-Diazabuta-1,3-diene)ferrocenophane B. M. Yamin and N. M. Ali Online 14 February 2003

Acta Cryst. (2003). E59, m97-m98  [ doi:10.1107/S160053680300299X ] Chloro(P-{2-[N-(2,6-diisopropylphenyl)iminomethyl]phenyl}-P,P-diphenylphosphine-2N,P)methylpalladium(II) A. L. Spek Online 14 February 2003

Acta Cryst. (2003). E59, m99-m101  [ doi:10.1107/S1600536803003076 ] Dichloro(2,2',4,4',6,6'-hexamethyl-m-terphenyl)bis(N-methylimidazole)(tetrahydrofuran)samarium(III) toluene disolvate G. W. Rabe, B. Rhatigan, A. L. Golen and A. L. Rheingold Online 14 February 2003

Acta Cryst. (2003). E59, m102-m104  [ doi:10.1107/S1600536803003155 ] Tetrakis[4-amino-N-(2-hydroxyethyl)pyridinium] hexacosaoxooctamolybdate Y. Yan, C.-D. Wu, J.-H. Liu, Q.-Z. Zhang and C.-Z. Lu Online 14 February 2003

Acta Cryst. (2003). E59, m105-m107  [ doi:10.1107/S1600536803003507 ] (3-Allyl)[(S)-(+)-(2-pyrrolidinylmethyl)pyrrolidine]palladium(II) trifluoromethanesulfonate M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson Online 21 February 2003

Acta Cryst. (2003). E59, m108-m110  [ doi:10.1107/S1600536803003052 ] Undecacarbonyl(4-2-thiodithiobenzoato-4C,S,S',S'')(trimethylphosphite)tetrafer E. A. Laifa, N. Benali-Cherif and H. Merazig Online 21 février 2003

Acta Cryst. (2003). E59, m111-m113  [ doi:10.1107/S1600536803003581 ] [1,1'-Bis(diphenylphosphino)ferrocene-2P,P'](1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate dichloromethane disolvate M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson Online 21 February 2003

Acta Cryst. (2003). E59, m114-m115  [ doi:10.1107/S1600536803003532 ] Poly[[bis(4,4'-bipyridine)bis(-oxalato)trizinc(II)]-di--4,4'-bipyridine--oxalato] K. J. Nordell, K. A. Higgins and M. D. Smith Online 21 February 2003

Acta Cryst. (2003). E59, m116-m118  [ doi:10.1107/S160053680300360X ] Anhydrous octaguanidinium hexatungstoplatinate(IV) U. Lee, S.-J. Jang, H.-C. Joo and K.-M. Park Online 21 February 2003

Acta Cryst. (2003). E59, m119-m121  [ doi:10.1107/S1600536803003386 ] Twinned bis[tris(1,2-ethanediamine-2N,N')manganese(II)] pentaselenodiantimonate(III) C. Näther, F. Wendland and W. Bensch Online 21 February 2003

Acta Cryst. (2003). E59, m122-m124  [ doi:10.1107/S1600536803003556 ] Dichloro(N,N-dimethylethylenediamine)cadmium(II): a novel two-dimensional chloro-bridged coordination polymer H.-D. Bian, W. Gu, S.-P. Yan, D.-Z. Liao and Z.-H. Jiang Online 21 February 2003

Acta Cryst. (2003). E59, m125-m127  [ doi:10.1107/S1600536803004045 ] 4-(Tri-tert-butoxysilylthiomercurio)benzoic acid J. Chojnacki, A. Walaszewska, E. Baum and W. Wojnowski Online 28 February 2003

Acta Cryst. (2003). E59, m128-m130  [ doi:10.1107/S1600536803002496 ] Bis{4-[-(4-acetylphenylimino)benzyl]-3-methyl-1-phenylpyrazol-5-onato}aquacopper(II) J.-L. Wang, F. Ding and F.-M. Miao Online 28 February 2003

Acta Cryst. (2003). E59, m131-m133  [ doi:10.1107/S160053680300240X ] (1,2-Diaminocyclohexane)silver(I) trifluoromethanesulfonate A. Usman, H.-K. Fun, H.-L. Zhu and X.-J. Wang Online 28 February 2003

Acta Cryst. (2003). E59, m134-m136  [ doi:10.1107/S1600536803004094 ] A dinuclear rhenium complex, {[(C18H24N2)Re(CO)3]2(-C12H12N2)}(PF6)2·2CH2Cl2 S.-S. Sun, D. T. Tran, P. Y. Zavalij, S. R. J. Oliver and A. J. Lees Online 28 February 2003

Acta Cryst. (2003). E59, m137-m139  [ doi:10.1107/S1600536803004318 ] Tetrakis(3-phenoxo-acetonitrilelithium), a tetrameric lithium aryloxide with a cubane core M. Tombul, R. J. Errington, R. A. Coxall and W. Clegg Online 28 February 2003

organic compounds

Acta Cryst. (2003). E59, o258-o260  [ doi:10.1107/S1600536803002289 ] Bis[(3,5-dimethylpyrazol-1-yl)ethyl] disulfide A. M. Mills, M.-C. Chalbot, E. Bouwman and A. L. Spek Online 7 February 2003

Acta Cryst. (2003). E59, o261-o262  [ doi:10.1107/S1600536803001442 ] 2-Hydroxy-4,4-dimethyl-N-(4-methylphenyl-6-oxocyclohexanylacetamide S. Selvanayagam, M. Yogavel, V. Rajakannan, D. Velmurugan, S. Shanmuga Sundara Raj and H.-K. Fun Online 7 February 2003

Acta Cryst. (2003). E59, o263-o265  [ doi:10.1107/S1600536803002514 ] 1,2-Bis[bis(4-methoxyphenyl)hydroxymethyl]benzene K. A. Carey, W. Clegg, M. R. J. Elsegood, B. T. Golding and H. Maskill Online 7 February 2003

Acta Cryst. (2003). E59, o266-o268  [ doi:10.1107/S1600536803002411 ] 3-Benzoyl-2-hydroxy-2-methylchromene M. Yogavel, D. Velmurugan, K. Sekar, H. Schenk, J. Fraanje, R. Peschar, S. Srinivasan, P. R. Athappan and Z. A. Rafi Online 7 February 2003

Acta Cryst. (2003). E59, o269-o271  [ doi:10.1107/S1600536803002447 ] N,N,N',N'-Tetrakis(2-pyridiniomethyl)ethylenediamine tetraperchlorate S. S. Gunatilleke and R. E. Norman Online 7 February 2003

Acta Cryst. (2003). E59, o272-o274  [ doi:10.1107/S1600536803002423 ] 4-[(2,6-Dichlorophenyl)(hydroxyimino)methyl]-1,5-dimethyl-2-phenyl-1,2-dihydropyrazol-3-one X.-F. Li, Y.-Q. Feng, J.-P. Zhuang and X.-F. Hu Online 7 February 2003

Acta Cryst. (2003). E59, o275-o276  [ doi:10.1107/S1600536803001181 ] 1-(4-Methoxypyrimidin-2-yl)-3-(2-nitrophenylsulfonyl)urea N. Ma, Z.-M. Li, J.-G. Wang and H.-B. Song Online 7 February 2003

Acta Cryst. (2003). E59, o277-o279  [ doi:10.1107/S1600536803002332 ] L-Prolinium trichloroacetate at 105 K K. Rajagopal, R. V. Krishnakumar, A. Mostad and S. Natarajan Online 7 February 2003

Acta Cryst. (2003). E59, o280-o282  [ doi:10.1107/S1600536803002344 ] (rac-2SR,3RS,5SR)-Spiro[3-methoxycarbonyl-1-azabicyclo[3.3.0]octane-2,1'-acenaphthylen]-2'-one T. V. Sundar, V. Parthasarathi, C. Álvarez-Rúa, S. García-Granda, I. Sharma, R. T. Pardasani and R. C. Mehrotra Online 7 February 2003

Acta Cryst. (2003). E59, o283-o284  [ doi:10.1107/S1600536803002265 ] Methyl 2,3,6-tri-O-benzoyl--D-xylo-hexopyranosid-4-ulose O. Renaudet, P. Dumy, C. Philouze and M.-T. Averbuch Online 7 February 2003

Acta Cryst. (2003). E59, o285-o287  [ doi:10.1107/S1600536803002290 ] 5-Ethyl-6-oxo-4-thioxo-1,3,2-oxazaphospholidino[3,2-a][1,3,2]benzodiazaphosphorine S.-L. Deng, R.-Y. Chen, X.-B. Leng and L.-H. Weng Online 7 February 2003

Acta Cryst. (2003). E59, o288-o289  [ doi:10.1107/S1600536803002435 ] 4-(2-Isonicotinoylhydrazino)-4-oxobutanoic acid A. C. Doriguetto, C. H. T. de Paula Silva, D. G. Rando, E. I. Ferreira and J. A. Ellena Online 7 February 2003

Acta Cryst. (2003). E59, o290-o292  [ doi:10.1107/S1600536803002733 ] 7,14-Dioxatetracyclo[14.24,5.219,20.221,22.223,24]tetracosa-1,3,5,9,11,15,17,19,21,23-decaene T. Ravishankar, K. Chinnakali, P. Rajakumar, V. Murali, A. Usman and H.-K. Fun Online 7 February 2003

Acta Cryst. (2003). E59, o293-o295  [ doi:10.1107/S1600536803002745 ] 7,16-Dioxatetracyclo[16.24,5.221,22.223,24.09,14]tetracosa-1,3,5,9,11,13,17,19,21,23-decaene T. Ravishankar, K. Chinnakali, P. Rajakumar, V. Murali, A. Usman and H.-K. Fun Online 7 February 2003

Acta Cryst. (2003). E59, o296-o298  [ doi:10.1107/S1600536803002538 ] Ladders in the supramolecular structure of 1-(4-bromophenyl)-3-[2-(2-hydroxyethyl)amino-5-nitroanilino]-1-propanone dimethylformamide solvate J. N. Low, J. Cobo, M. Nogueras, A. Sánchez, B. Insuasty and Y. Caldas Online 7 February 2003

Acta Cryst. (2003). E59, o299-o301  [ doi:10.1107/S1600536803002721 ] 16,17-Epoxy-20-oxopregn-5-ene-3,21-diyl diacetate L. C. R. Andrade, J. A. Paixao, M. J. M. de Almeida, R. M. L. M. Martins, H. I. M. Soares, M. J. S. M. Moreno, M. L. Sá e Melo and A. S. Campos Neves Online 14 February 2003

Acta Cryst. (2003). E59, o302-o303  [ doi:10.1107/S1600536803002988 ] 6-Methyl-11a,12-dihydro-6H-quino[3,2-b][1,4]benzothiazine: an amidine formed under unusual conditions R. L. Luck, K. Li and D. K. Bates Online 14 February 2003

Acta Cryst. (2003). E59, o304-o305  [ doi:10.1107/S1600536803003027 ] 2-Amino-5-butyl-4-methyl-1,3-thiazol-3-ium nitrate B. Zarychta, G. Spaleniak and J. Zaleski Online 14 February 2003

Acta Cryst. (2003). E59, o306-o307  [ doi:10.1107/S1600536803003015 ] 2,3-Dimethyl 5-isopropyl 1-ethoxymethyl-6-methyl-4-(3-nitrophenyl)-1,4-dihydropyridine-2,3,5-tricarboxylate V. Vrabel, D. Oktavec and S. Marchalín Online 14 February 2003

Acta Cryst. (2003). E59, o308-o309  [ doi:10.1107/S1600536803002769 ] 3,3-Bis(methylthio)-2-oxo-N-phenylpropanamide J. R. Deschamps, L. S. Suwandi and M. Konaklieva Online 14 February 2003

Acta Cryst. (2003). E59, o310-o311  [ doi:10.1107/S1600536803002605 ] 2-tert-Butyl-4-piperidino--diketimine M.-S. Zhou, D.-S. Liu, S.-P. Huang and H.-B. Tong Online 14 February 2003

Acta Cryst. (2003). E59, o312-o313  [ doi:10.1107/S1600536803002940 ] 2,2'-Diamino-4,4'-bi-1,3-thiazole J.-G. Liu, D.-J. Xu and C.-H. Hung Online 14 February 2003

Acta Cryst. (2003). E59, o314-o315  [ doi:10.1107/S1600536803002976 ] 2,3-Dithien-2-ylquinoxaline G. Crundwell, D. Sayers, S. R. Herron and K. A. Kantardjieff Online 14 February 2003

Acta Cryst. (2003). E59, o316-o318  [ doi:10.1107/S1600536803002903 ] Trichloroacetic acid at 105 K K. Rajagopal, A. Mostad, R. V. Krishnakumar, M. Subha Nandhini and S. Natarajan Online 14 February 2003

Acta Cryst. (2003). E59, o319-o320  [ doi:10.1107/S1600536803002836 ] (S)-Phenylsuccinic acid A. Fischer and V. M. Profir Online 14 February 2003

Acta Cryst. (2003). E59, o321-o323  [ doi:10.1107/S1600536803003222 ] 2,5-Diethoxycarbonyl-6-methyl-4-phenylthieno[2,3-b]pyridine H. Novoa de Armas, O. M. Peeters, N. M. Blaton, C. J. De Ranter, E. Salfrán, M. Suárez Navarro, E. Ochoa Rodríguez and Y. Verdecia Reyes Online 14 February 2003

Acta Cryst. (2003). E59, o324-o325  [ doi:10.1107/S1600536803003209 ] 4,4-Dimethyl-2-(2-methyl-1-propenyl)-2,6-diphenyl-2,3,4,5-tetrahydropyrimidine P. G. Jones, H. Hopf and H. W. Lautenbach Online 14 February 2003

Acta Cryst. (2003). E59, o326-o327  [ doi:10.1107/S1600536803003064 ] 4-Iodotetrathiafulvalene-1,4-dinitrobenzene (1/1) A. S. Batsanov and S. B. Lyubchik Online 14 February 2003

Acta Cryst. (2003). E59, o328-o329  [ doi:10.1107/S1600536803003088 ] N,N'-Bis(3-hydroxyphenyl)-1,8:4,5-naphthalenetetracarboximide dimethyl sulfoxide disolvate G. D. Fallon, M.A.-P. Lee and S. J. Langford Online 21 February 2003

Acta Cryst. (2003). E59, o330-o331  [ doi:10.1107/S1600536803003003 ] 3-(2,6-Dichlorophenyl)-8-ethyl-4-phenyl-1-oxa-6-thia-2,8-diazaspiro[4.4]non-2-ene-7,9-dione X.-F. Li, Y.-Q. Feng and Y.-F. Gu Online 21 February 2003

Acta Cryst. (2003). E59, o332-o333  [ doi:10.1107/S1600536803003428 ] N-(3-Methoxypropyl)-1,8-naphthalimide B. Zarychta, J. Zaleski, V. Prezhdo and B. Uspenskiy Online 21 February 2003

Acta Cryst. (2003). E59, o334-o336  [ doi:10.1107/S1600536803003362 ] Benzotriazol-1-yl 4,6-di-O-acetyl-2,3-dideoxy--D-erythro-hex-2-enpyranoside J. N. Low, J. Cobo, M. D. López, M. Nogueras and A. Sánchez Online 21 February 2003

Acta Cryst. (2003). E59, o337-o339  [ doi:10.1107/S1600536803003337 ] 3-{2-[2-(3,5-Dinitro-2-oxidophenyl)ethyl]-3,3-dimethyl-3H-indol-1-ium-1-yl}propanoic acid bis(dimethylformamide) solvate W. Zou, P. Chen, Y. Gao and J. Meng Online 21 February 2003

Acta Cryst. (2003). E59, o340-o341  [ doi:10.1107/S1600536803003453 ] N'-Benzoyl-N-p-bromophenylthiourea B. M. Yamin and M. S. M. Yusof Online 21 February 2003

Acta Cryst. (2003). E59, o342-o343  [ doi:10.1107/S1600536803003350 ] Salicylaldehyde 4-nitrophenylhydrazone S. Shan, D.-J. Xu, J.-Y. Wu and M. Y. Chiang Online 21 February 2003

Acta Cryst. (2003). E59, o344-o346  [ doi:10.1107/S1600536803003568 ] 2-Hydroxycyclohexene-1-carboxylic acid: the enol isomer of 2-oxocyclohexane-1-carboxylic acid A. J. Kresge, A. J. Lough and Y. Zhu Online 21 February 2003

Acta Cryst. (2003). E59, o347-o349  [ doi:10.1107/S1600536803003374 ] The acetyl derivative of humirianthol R. A. Burrow, A. F. Morel, I. B. Graebner, D. H. Farrar and A. J. Lough Online 21 February 2003

Acta Cryst. (2003). E59, o350-o352  [ doi:10.1107/S1600536803003349 ] Absolute configuration of diacetylated acrenol as its chloroform solvate R. A. Burrow, A. F. Morel, I. B. Graebner, A. J. Lough and D. H. Farrar Online 21 February 2003

Acta Cryst. (2003). E59, o353-o355  [ doi:10.1107/S1600536803002848 ] 2-Cyano-3-dimethylamino-N-(2,5-dimethylphenyl)acrylamide Ompraba, A. Aysha, M. Yogavel, D. Velmurugan, S. Selvi, P. T. Perumal, S. Shanmuga Sundara Raj, H.-K. Fun and Z. A. Rafi Online 21 February 2003

Acta Cryst. (2003). E59, o356-o357  [ doi:10.1107/S1600536803003623 ] 1,1'-(1,2-Ethanediyl)bis(2,3-dihydro-3-methyl-1H-imidazole-2-thione) Q. Liu, D. Shi, K. Yu and J. Xu Online 21 February 2003

Acta Cryst. (2003). E59, o358-o359  [ doi:10.1107/S1600536803003635 ] N,N'-Bis(benzamidothiocarbonyl)hydrazine dimethyl sulfoxide disolvate B. M. Yamin and M. S. M. Yusof Online 28 February 2003

Acta Cryst. (2003). E59, o360-o362  [ doi:10.1107/S160053680300401X ] 7-Nitro-1,2,3a,4-tetrahydrobenzo[b][1,3]oxazolo[3,2-d]oxazine: a new heterocycle S. Vishnu Vardhan Reddy, A. Sivalakshmi Devi, K. Vyas, V. Venugopal Rao, Y. Koteswar Rao, A. Venkateswarlu and P. K. Dubey Online 28 February 2003

Acta Cryst. (2003). E59, o363-o365  [ doi:10.1107/S1600536803003684 ] 2-(5,7-Dihydroxy-4-oxo-4H-chromen-3-yl)-5-methoxy-1,4-benzoquinone (isoflavonequinone) T. Aree, S. Tip-pyang, S. Seesukphronrarak and N. Chaichit Online 28 February 2003

Acta Cryst. (2003). E59, o366-o368  [ doi:10.1107/S1600536803003647 ] N,N'-Bis(tert-butoxycarbonyl)thiourea C. Li, K. W. Y. Chan and L. Szeto Online 28 February 2003

Acta Cryst. (2003). E59, o369-o371  [ doi:10.1107/S160053680300357X ] Ethyl (Z)-3-bromo-2-[(tert-butoxycarbonyl)amino]-3-phenylacrylate P. G. Jones and S. Jäger Online 28 February 2003

Acta Cryst. (2003). E59, o372-o373  [ doi:10.1107/S1600536803004069 ] 1,6-Dibenzoyloxy-2:4,3:5-O2:O4,O3:O5-bis(phenylboronoyloxy)-D-mannitol P. J. Duggan, D. G. Humphrey, D. J. Price and E. M. Tyndall Online 28 February 2003

Acta Cryst. (2003). E59, o374-o375  [ doi:10.1107/S1600536803004057 ] N-(4-Bromophenyl)pyridine-2-carboxamide J. Y. Qi, Q. Y. Yang, K. H. Lam, Z. Y. Zhou and A. S. C. Chan Online 28 February 2003

Acta Cryst. (2003). E59, o376-o377  [ doi:10.1107/S1600536803004124 ] Diethyl 2-methyl-6-(2-thiazolidinyl)-4-(2-thienyl)-1,4-dihydropyridine-3,5-dicarboxylate V. Vrábel, J. Kozísek and S. Marchalín Online 28 February 2003

Acta Cryst. (2003). E59, o378-o380  [ doi:10.1107/S1600536803004197 ] 2,4-Dinitrophenyl 4-toluenesulfonate: molecular aggregation through weak C-HO interactions N. Vembu, M. Nallu, J. Garrison and W. J. Youngs Online 28 February 2003

Acta Cryst. (2003). E59, o381-o383  [ doi:10.1107/S1600536803004227 ] 3,9-Dimethoxy-6a,11a-dihydro-6H-benzo[4,5]furo[3,2-c]chromene-4,10-diol monohydrate T. Aree, S. Tip-pyang, S. Paramapojn and N. Chaichit Online 28 February 2003

Acta Cryst. (2003). E59, o384-o386  [ doi:10.1107/S1600536803004100 ] 4-(4-Bromophenyl)-2,5-diethoxycarbonyl-6-methylthieno[2,3-b]pyridine H. Novoa de Armas, O. M. Peeters, N. M. Blaton, C. J. De Ranter, M. Suárez Navarro, E. Salfrán Solano, Y. Verdecia Reyes and E. Ochoa Rodríguez Online 28 February 2003

Acta Cryst. (2003). E59, o387-o389  [ doi:10.1107/S1600536803003763 ] Per(3-deoxy)--cyclomannin: an n-butanol hexahydrate inclusion complex H. J. Lindner, F. W. Lichtenthaler, K. Fujita, C. Yang, D.-Q. Yuan and Y. Nogami Online 28 February 2003

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