Acta Cryst. (2003). E59, m97-m98  [ doi:10.1107/S160053680300299X ]

Chloro(P-{2-[N-(2,6-diisopropylphenyl)iminomethyl]phenyl}-P,P-diphenylphosphine-²N,P)methylpalladium(II)

A. L. Spek

Online 14 February 2003

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (C-C) = 0.003 Å
• R factor = 0.023
• wR factor = 0.053
• Data-to-parameter ratio = 19.5

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



ABSTM_02  Alert C The ratio of Tmax/Tmin expected RT(exp) is > 1.10             
          Absorption corrections should be applied.                             
          Tmin and Tmax expected:      0.690     0.812                          
          RT(exp) =      1.176                                                  

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           27.44                 
         From the CIF: _reflns_number_total               6433                  
         Count of symmetry unique reflns         3601                           
         Completeness (_total/calc)            178.64%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured      2832                           
         Fraction of Friedel pairs measured     0.786                           
         Are heavy atom types Z>Si present          yes                         
          Please check that the estimate of the number of Friedel pairs is      
          correct. If it is not, please give the correct count in the           
          _publ_section_exptl_refinement section of the submitted CIF.          


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 1 Alert Level C = Please check

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