Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 59| Part 4

ISSN: 2056-9890

April 2003 issue

Highlighted illustration

Cover illustration: This biphenyl derivative is chiral by virtue of hindered rotation about the central C-C bond of the biphenyl unit, and has approximate molecular twofold rotation symmetry. The absolute configuration has been determined and correlated with circular dichroism spectra of this and related compounds. See Linden & Rippert [Acta Cryst. E59, o390-o392].

inorganic compounds

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KPrF₄

F. Werner, M. Weil and F. Kubel

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Dipotassium zinc bis(dihydrogendiphosphate) dihydrate, K₂Zn(H₂P₂O₇)₂·2H₂O

A. A. Tahiri, R. Ouarsal, M. Lachkar, P. Y. Zavalij and B. El Bali

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Di-μ-iodo-bis[dicarbonylrhodium(I)]

S. Burger, B. Therrien and G. Süss-Fink

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Li₃Sc(MoO₄)₃: substitutional disorder on three (Li,Sc) sites

U. Kolitsch and E. Tillmanns

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Tetragonal form of barium cobalt disilicate, Ba₂CoSi₂O₇

B. El Bali and P. Y. Zavalij

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Cobalt hydrogen selenite chloride dihydrate, Co(HSeO₃)Cl·2H₂O

M. G. Johnston and W. T. A. Harrison

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K₂MoO₂P₂O₇

M. F. Zid, A. Driss and T. Jouini

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metal-organic compounds

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Bis[N,N′-bis(2-fluorobenzylidene)ethylenediamine-κ²N,N′]silver(I) nitrate

A. Usman, H.-K. Fun, H.-L. Zhu and Q.-X. Liu

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Di-μ-acetato-κ³O,O′:O′-di-μ-trichloroacetato-κ²O:O′-bis[aqua(trichloroacetato)(1,10-phenanthroline-κ²N,N′)praseodymium(III)] dimethylformamide disolvate

S.-Y. Zhang, Z. Shi, Z. Long-Guan, R.-R. Xu and W.-Q. Pang

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[Dicarbonyl(η⁵-cyclopentadienyl)iron(II)]-μ₂-1,3-propanediyl-[dicarbonyl(η⁵-cyclopentadienyl)ruthenium(II)]

H. B. Friedrich, R. A. Howie and M. O. Onani

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Tetraaquatetrakis[2-(2-hydroxyethylamino)ethanolato]tetracopper(II) tetranitrate 14/3-hydrate

E. A. Vinogradova, V. N. Kokozay, O. Y. Vassilyeva and B. W. Skelton

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catena-Poly[[bis(3-aminobenzoic acid-κN)cadmium(II)]-di-μ-thiocyanato-κ⁴N:S;S:N]

R. Wang, M. Hong, J. Luo, L. Han, Z.-Z. Lin and R. Cao

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cis-Dichlorobis(4,4′-dimethyl-2,2′-bipyridine)iridium(III) hexafluorophosphate

N. Yoshikawa, J. Sakamoto, N. Kanehisa, Y. Kai and T. Matsumura-Inoue

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The 1:2 bis(maleonitriledithiolato)palladium(II) complex of the N-(2-fluoro-4-bromobenzyl)pyridinium cation

Y. Chen, J. Xie, X. Ren and G. Liu

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(18-Crown-6-κ⁶O)potassium 2,4-dinitrophenolate 2,4-dinitrophenol

J. C. Barnes and T. J. R. Weakley

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Dianilinium tetradecachlorohexamolybdate dihydrate, (PhNH₃)₂[(Mo₆Cl₈)Cl₆]·2H₂O

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catena-Poly[disodium [[tris(formato-κO)copper(II)]-μ₂-formato-κ²O:O′]], with partial substitution of formate by acetate, Na_2n[Cu(O₂CH)_4−x(O₂CCH₃)_x]_n (x = 0.28)

A. Golobič, K. Klančar and P. Šegedin

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A cationic zinc(II) complex of a new ligand based on N,N,N′,N′-tetramethylstreptamine 2,4,6-orthoformate as the chloride salt

P. G. Jones, A. J. Kirby and C. Beckmann

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A cationic zinc(II) complex of a new ligand based on N,N,N′,N′-tetramethylstreptamine 2,4,6-orthoformate as the trichloro(pyridine)zincate(II) salt

P. G. Jones, I. Dix, A. J. Kirby and C. Beckmann

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Aquatriphenyl(trifluoroacetato)tin–2,2′:6′,2′′-terpyridine (1/1)

C. F. Chee, K. M. Lo and S. W. Ng

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Di-μ₃-bromo-dibromotetrakis[μ-diphenyl(2-pyridyl)phosphine)]tetracopper(I) dichloromethane hexasolvate

J.-L. Zhou, Y.-Z. Li, H.-G. Zheng, X.-Q. Xin and L.-L. Xu

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catena-[1,3-Diammoniopropane di-μ₂-hydroxo-di-μ₄-phosphato-trioxotrivanadium dihydrate]: a redetermination at 180 (2) K

F. A. Almeida Paz, F.-N. Shi, T. Trindade, J. Rocha and J. Klinowski

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Tetrachloro(N,N,N′,N′-tetramethylethylenediamine)zirconium(IV)

C. E. F. Rickard, M. W. Glenny and A. J. Nielson

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Bis(diethylenetriamine-κ³N)nickel hexafluorogermanate

H.-X. Zhang, G.-Y. Yang and Y.-Q. Sun

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Tris(N,N-diethyldithiocarbamato-κ²S,S′)nickel(II)

A. K. Mohamed, N. Auner and M. Bolte

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Redetermination of bis(N,N-diethyldithiocarbamato-κS)dimethyltin(IV) at low temperature

A. K. Mohamed, N. Auner and M. Bolte

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Bis(triphenylphosphine)iminium μ-acetato-di-μ-acetylacetonato-bis[acetylacetonatomagnesate(II)] monohydrate

P. G. Jones and M. M. Álvarez-Falcón

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Bis[μ-bis(diphenylphosphino)methane-κ²P:P′]bis[diacetonitrilecopper(I)] bis(hexafluorophosphate)

M.-M. Wu, L.-Y. Zhang, Y.-H. Qin and Z.-N. Chen

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Ethylenediammonium tetraaquabis(sulfato)iron(II)

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Bis(thiosemicarbazido-κ²N,S)nickel(II)–succinate–succinic acid (1/1/1)

S.-L. Li, A. Usman, I. A. Razak, A. A. Rahman, H.-K. Fun, J.-Y. Wu, Y.-P. Tian, M.-H. Jiang and Z.-Y. Chen

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Aqua(trifluoroacetato)triphenyltin–15-crown-5 (2/1)

C. F. Chee, K. M. Lo and S. W. Ng

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Aqua(trifluoroacetato)triphenyltin–2,2′-bipyridine (2/2)

C. F. Chee, K. M. Lo and S. W. Ng

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Hexacarbonyldicobalt addition across the C C bond of the alkynethiolate ligand in the cluster [Ru₃(μ₃,η²-C CSiMe₃)(μ-SC CSiMe₃)(CO)₉]

E. Delgado, M. I. Alcalde, B. Donnadieu, E. Hernandez and J. Sanchez-Nieves

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(4,4′-Dimethyl-2,2′-bipyridine)(ethynylbenzene)(triphenylphosphine)platinum(II) hexafluoroantimonate

M.-M. Wu, L.-Y. Zhang, Y.-H. Qin and Z.-N. Chen

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Dipotassium disodium trans-bis(pyrazine-2,3-dicarboxylato)copper(II) dithiocyanate dihydrate

M.-S. Wang, L.-Z. Cai, G.-W. Zhou, G.-C. Guo, J.-G. Mao and J.-S. Huang

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catena-Poly[[[μ-N,N′-bis(2-aminoethyl)oxamido]dicopper(II)]-di-μ-dicyanoamido]

S. Chu, X.-Q. Wang, R.-J. Wang and G.-Q. Shen

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A synchrotron study of μ₃-chloro-tri-μ-chloro-μ₃-sulfido-hexakis(triphenylphospine)triruthenium(II)–tetrahydrofuran–water (1/1.25/0.75)

V.-A. Tolhurst, D. Cookson and P. Turner

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organic compounds

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(−)-(P)-N,N′-Bis[(5-bromo-2-hydroxyphenyl)methylidene]-6,6′-dimethyl-1,1′-biphenyl-2,2′-dimethanamine

A. Linden and A. J. Rippert

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1,2-Bis(benzothiazol-2-ylsulfanyl)ethane

R.-Q. Zou, J.-R. Li, Y. Zheng, R.-H. Zhang and X.-H. Bu

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2-Acetylbenzo[b]furan

A. Thiruvalluvar, S. Silvarani, A. Vadivelu, K. Sithik Ali and V. R. Venkataraman

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Quinolinium fumarate

N. Shan, E. Batchelor and W. Jones

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N-p-Bromophenyl-N′-(2-chlorobenzoyl)urea

B. M. Yamin and A. S. Mardi

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8,10-Dibenzylimidazonorbornylene

S. G. Gouin, J.-F. Gestin, J. C. Meslin, D. Deniaud and M. Evain

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( $\pm$ )-anti-7-Ethyl-1-(4-methoxyphenyl)-5,5,syn-8-trimethyl-2-oxabicyclo[2.2.2]octan-3-one, a bicyclic δ-lactone

S. Xie, Y. Hou, C. Y. Meyers and P. D. Robinson

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( $\pm$ )-5-Ethyl-endo-4-(4-methoxyphenyl)-2,2,anti-8-trimethyl-6-oxabicyclo[3.2.1]octan-7-one, a bicyclic γ-lactone

S. Xie, Y. Hou, C. Y. Meyers and P. D. Robinson

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Guest differentiation in a 6^I,6^II-disubstituted β-cyclodextrin

F. W. Lichtenthaler, H. J. Lindner, K. Fujita, D.-Q. Yuan and Y. Ren

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Methyl 4-amino-2-oxo-1,2-dihydroquinoline-3-carboxylate

V. B. Rybakov, V. V. Chernyshev, I. V. Ukrainets, P. A. Bezugly, L. V. Sidorenko and N. Skaif

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N,N′-Bis(4-methylphenyl)pyridine-2,6-dicarboxamide

J. Y. Qi, Q. Y. Yang, K. H. Lam, Z. Y. Zhou and A. S. C. Chan

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Dimethyl{3-[1-methyl-4-(1-methyl-4-nitropyrrole-2-carboxamido)pyrrole-2-carboxamido]propyl}ammonium chloride methanol solvate

L. Lu, M. Zhu, J. Li and P. Yang

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3-Hydroxypyridinium 2,5-dihydroxybenzoate

T. Fukunaga, S. Kashino and H. Ishida

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2-Amino-4-phenyl-5,6-dihydrobenzo[h]quinazoline

X. Wang, D. Shi, S. Tu and K. Yu

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(5-Bromopyrrol-3-yl)cyclohexylmethanone

T. J. Emge, M. J. Clements, D. S. Myers and S. Knapp

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5,17-Bis(diphenylphosphinoyl)-25,26,27,28-tetrapropoxycalix[4]arene

C. Jeunesse, D. Matt, P. G. Jones and H. Thönnessen

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4-{[3,4-Dihydro-5-methyl-3-oxo-2-phenyl-2H-pyrazol-4-ylidene](phenyl)methylamino}-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

J.-L. Wang, Y. Yang, X. Zhang and F.-M. Miao

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3,4-Dimethoxyphenylacetic acid

D. Chopra, A. R. Choudhury and T. N. Guru Row

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N-(4-Ethoxyphenyl)-2-[(4-ethoxyphenylcarbamoyl)methoxy]acetamide monohydrate, a supramolecular chain structure formed by hydrogen bonds

X.-F. Li, W.-S. Liu and M.-Y. Tan

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Methyl 2-(4-methoxypyrimidin-2-ylcarbamoylsulfamoyl)benzoate

N. Ma, B. Wang, J. Wang, H. Song, S. Wang and Z. Li

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1H-Nicotinamidium 3,5-dinitrosalicylate

M. Koman, L. Martiška, D. Valigura and T. Glowiak

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2-[(4-Bromophenyl)amino]-1-phenylethanone

I. Saraogi, B. H. M. Mruthyunjayaswamy, O. B. Ijare, Y. Jadegoud and T. N. Guru Row

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2,2,6,6-Tetramethyl-4-oxopiperidinium trifluoroacetate

S. Breitung, H.-W. Lerner and M. Bolte

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Zwitterionic 2-guanidinium-1-aminocarboxylate monohydrate

T. Kolev and R. Petrova

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6-Methyl-4-phenylthieno[2,3-b]pyridine-2,5-dicarboxylic acid

H. Novoa de Armas, O. M. Peeters, N. M. Blaton, C. J. De Ranter, M. Suárez Navarro, E. Salfrán Solano, Y. Verdecia Reyes and E. Ochoa Rodríguez

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1,4-Bis(2-mercaptobenzothiazolyl)butane

C. Chen, C. Su, H. Zhang, A. Xu and B. Kang

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(1R,2R)-(+)-1,2-Diphenylethylenediamine

M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson

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4,5-Dibromo-1-methyl-1H-imidazole

W. E. Noland, K. P. Cole and D. Britton

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r-2,c-6-Bis(p-tolyl)-t-3,t-5-dimethyltetrahydropyran-4-one

B. S. Krishnamoorthy, T. R. Sarangarajan, K. Thanikasalam, K. Panchanatheswaran and R. Jeyaraman

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r-2,c-6-Bis(4-chlorophenyl)-t-3,t-5-dimethyltetrahydropyran-4-one

S. Jose Kavitha, T. R. Sarangarajan, K. Thanikasalam, K. Panchanatheswaran and R. Jeyaraman

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1,4-Diphenyl-2,3-dithien-3-ylcyclopentadien-1-one

J. Linehan, G. Crundwell, S. R. Herron and K. A. Kantardjieff

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The β-form of di-tert-butyl 1,4-dioxo-3,6-diphenyl-1,2,4,5-tetrahydropyrrolo[3,4-c]pyrrole-2,5-dicarboxylate

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Di-tert-butyl 3,6-bis(2-methylphenyl)-1,4-dioxo-1,2,4,5-tetrahydropyrrolo[3,4-c]pyrrole-2,5-dicarboxylate

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Di-tert-butyl 7,14-dihydro-7,14-dioxoquino[2,3-b]acridine-5,12-dicarboxylate

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Redetermination of 4,4′-dibromobiphenyl

A. K. Mohamed, N. Auner and M. Bolte

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1-Methyl-4-nitro-2-(trichloroacetyl)pyrrole

L.-P. Lu, C.-Y. Zhou, G.-C. Zhang, M.-L. Zhu and P. Yang

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n-Undecylammonium bromide monohydrate

G. J. Kruger, M. Rademeyer and D. G. Billing

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1,3-Bis(2,2′:6′,2′′-terpyridin-4′-yl)benzene, a new dinucleating bis(tridentate) ligand, as its dichloromethane solvate

S. Vaduvescu and P. G. Potvin

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(RS)-Phenylsuccinic acid

A. Fischer and V. M. Profir

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N-(4-Bromo-2-nitrophenyl)-N-methyl-N'-(quinolin-4-ylmethylene)hydrazine

S. Öztürk, M. Akkurt, E. Aydemír and H.-K. Fun

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N,N-Dimethyl-N′-(o-fluorobenzoyl)hydrazide

K. W. Muir and D. G. Morris

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3-Bromo-4-(dicyclohexylphosphinoyl)-2,6-dimethoxypyridine

J. Wu, R. Guo, Z. Zhou, H. Chen and C. Yeung

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The 2:1 complex of 4-aminobenzoic acid and 4,4′-bipyridyl N,N′-dioxide

R. Moreno-Fuquen, M. Font i Carot, M. Garriga, F. Cano, M. Martinez-Ripoll, J. Valderrama-Naranjo and L. M. Serratto

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(6R,9S,13R,14S)-7,8-Didehydro-3,7-dimethoxy-17-methyl-6-phenylmorphinan-4,6-diol

C.-B. Li, W.-Q. Zhang and C. Wang

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Ethyl (2S)-2-[(2R,2′R,5S)-2′,5-dimethyl-5′-oxoperhydro-[2,2′]]bifuranyl-5-yl]-2-hydroxyethanoate

S. J. Coles and M. B. Hursthouse

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2-Chlorophenyl 4-toluenesulfonate: molecular aggregration through weak C—H⋯O interactions

N. Vembu, M. Nallu, J. Garrison and W. J. Youngs

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Tetrabutylammonium 2,6-dihydroxybenzoate 2,6-dihydroxybenzoic acid solvate

F. A. Almeida Paz, P. C. R. Soares-Santos, H. I. S. Nogueira, T. Trindade and J. Klinowski

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Ethyl 3-(1-benzoyl-3-phenylaziridin-2-yl)propenoate

A. S. Batsanov, W. M. Dutton, P. G. Steel and D. J. Aldous

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4-(2-Pyridyl)-1H,2H-pyrido[1,2-c]pyrimidine-1,3-dione

I. Wolska, F. Herold and M. Maj

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14-n-Butyldibenz[a,h]acridine

J. K. Ray, B. C. Roy, D. Pan, M. Canle L., J. A. Santaballa and J. Mahía

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1-(Benzotriazol-1-ylmethyl)-5-(4-dimethylaminophenyl)-3-phenyl-4,5-dihydro-1H-pyrazole

J. N. Low, J. Cobo, F. Arroyabe, H. Torres, R. Abonia and M. Nogueras

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trans-(3R,2aS)-(−)-3-Phenyl-2,3,5,6,7,8-hexahydro-oxazolo[3,2-a]pyridine-5-thione

L.-F. Roa, D. Gnecco, A. Galindo, J. Juárez, J. L. Terán and S. Bernès

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(3,4),(6,7)Dibenzo-9,10-dicyanotriquinacene

P. G. Jones, P. Bubenitschek, H. Hopf and B. Witulski

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5-(1H-Indol-3-yl)-1-phenylpent-4-ene-1,3-dione

A. F. Arrieta and A. Mostad

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8-[N-(tert-Butoxycarbonyl)-L-glycyl]quinolin-8-amine

Y. Shao, C. Tu, J. Zhang and Z. Guo

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1-Acetyl-4-(p-chlorobenzylideneamino)-3-methyl-4,5-dihydro-1H-1,2,4-triazol-5-one

U. Çoruh, B. Kahveci, S. Şaşmaz, E. Ag~ar and Y. Kim

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Redetermination of 5,11,17,23-tetra-tert-butyl-25,27-di(ethoxycarbonylmethoxy)-26,28-dihydroxycalix[4]arene chloroform disolvate at low temperature

M. Bolte, C. Danila and V. Böhmer

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(S)-(−)-2,2′-Bis(diphenylphosphino)-1,1′-binaphthyl, a versatile chelating ligand

M. D. Jones, F. A. Almeida Paz, J. E. Davies and B. F. G. Johnson

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(2,6-Diisopropylphenyl)isopropylideneammonium iodide

R. J. Baker, H. Bettentrup and C. Jones

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Ammonium 2-mercaptopyridine-3-carboxylate hydrate

G. Smith and D. S. Sagatys

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1-(4-Chloro-2-nitrophenyl)-4,4′-bipyridinium triiodide

Y.-Q. Sun, J. Zhang and G.-Y. Yang

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A dithietane of 2-methylpropanedithioic acid

A. Mahjoub, H. Zantour, S. Masson, M. Saquet and M.-T. Averbuch-Pouchot

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Monoclinic form of 7-nitro-2-phenyl-1,2-benzisoselenazol-3(2H)-one

L. Dupont, M. Messali and L. Christiaens

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3,5-Dinitroxytricyclo[2.2.1.0^2,6]heptane

S. Öztürk, B. Büyükkıdan, M. Akkurt, O. Çakmak and H.-K. Fun

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Methyl (E)-2-acetyl-3-amino-2-pentenoate

X. Chen and T. Chen

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Mersinine A from Kopsia fruticosa

G. Subramaniam, T. S. Kam and S. W. Ng

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4-Hydroxy-3,6,9-trimethyl-2,3-dihydrobenzo[de]chromene-7,8-dione

X.-D. Guo, C.-Z. Liao, L. Ma and L.-Q. Gu

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1-Ethynyl-2-isopropoxy-3-methoxybenzene

C. M. Williams, L. N. Mander and P. V. Bernhardt

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N,N,N′,N′-Tetramethylstreptamine 2,4,6-orthoformate

C. Beckmann, P. G. Jones and A. J. Kirby

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N,N,N′,N′-Tetramethylstreptamine 2,4,6-orthoformate hydrochloride

C. Beckmann, P. G. Jones and A. J. Kirby

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(3E)-3-[(4-Hexylphenyl)imino]1H-indol-2(3H)-one

S. Öztürk, M. Akkurt, M. Ü. Özgür, A. Erçağ and F. W. Heinemann

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Methyl ( $\pm$ )-(1α,2β,8α,9α,10β)-2-chloro-4-aza-3-oxatetracyclo[8.4.0.0^2,9.0^4,8]tetradecane-9-carboxylate oxalic acid monohydrate

D. S. Yufit, J. A. K. Howard, S. I. Kozhushkov, S. Masini, A. Brandi and A. Meijere

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(m-Carboxyphenyl)ammonium perchlorate at 223 K

L. Bendjeddou, A. Cherouana, F. Berrah and N. Benali-Cherif

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N—H⋯O hydrogen bonding in the adduct of N-(2-aminoethyl)-2-hydroxybenzamide with picric acid

Q. Yu, Y. Tang, Y.-H. Feng, M.-Y. Tan and K.-B. Yu

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4′-Hydroxy-3′-methoxyacetophenone (acetovanillone)

G.-B. Ma, B. O. Patrick, T. Q. Hu and B. R. James

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5-[(2-Hydroxyphenyl)methyleneamino]-1,3,4-thiadiazole-2(3H)-thione

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(Z)-α-Chloromethyl-3,3′,4,4′-tetramethoxystilbene

R. Stomberg, V. Langer, S. Li and K. Lundquist

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N,N-Dimethylbiguanidium nitrate

M. Zhu, L. Lu and P. Yang

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1-(2-Hydroxyethyl)-4-{4,5,6,7-tetrahydro-1-[1-(2-hydroxyethyl)-pyridin-4(1H)-ylidene]-1H-inden-3-yl}pyridinium iodide

G. J. Gainsford, A. J. Kay and A. D. Woolhouse

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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