(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2003). E59, m192-m194 [ doi:10.1107/S1600536803005713 ]

Bis(triphenylphosphine)iminium -acetato-di--acetylacetonato-bis[acetylacetonatomagnesate(II)] monohydrate

P. G. Jones and M. M. Álvarez-Falcón

Online 31 March 2003

Key indicators

Single-crystal X-ray study
T = 133 K
Mean (C-C) = 0.004 Å
R factor = 0.045
wR factor = 0.105
Data-to-parameter ratio = 14.4

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



PLAT_601  Alert B Structure Contains Solvent Accessible VOIDS of     123.00 A   3

Author response: There is no evidence that these voids are occupied (see residual electron density) and I do not believe that they have a deeper structural significance.


 0 Alert Level A = Potentially serious problem

 1 Alert Level B = Potential problem

 0 Alert Level C = Please check