# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_qjy33 _shelx_title ' QJY33 in C2/c C21H19N3O2' _shelx_refln_list_code 4 _shelx_F_calc_maximum 259.85 _exptl_crystal_F_000 728.00 _reflns_d_resolution_high 0.7672 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 25.1403 _cell_length_b 8.5779 _cell_length_c 8.5295 _cell_angle_alpha 90.000 _cell_angle_beta 94.456 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2418.17 2102.29 214.46 o 6 0 0 150.84 145.13 11.23 o 8 0 0 1079.77 1073.23 32.13 o 10 0 0 0.14 28.76 11.34 o 12 0 0 563.03 566.50 106.46 o 14 0 0 381.78 895.09 211.75 o 16 0 0 150.12 228.36 73.94 o 18 0 0 45.11 -6.97 26.32 o 20 0 0 163.46 228.40 45.68 o 22 0 0 13.43 -19.36 26.32 o 24 0 0 464.76 397.18 62.71 o 26 0 0 7.81 27.10 39.49 o 30 0 0 2.97 -3.10 54.20 o 32 0 0 15.47 17.81 45.68 o 1 1 0 5854.64 5817.27 406.32 o 3 1 0 1922.16 1976.18 108.27 o 5 1 0 13590.78 13426.36 452.79 o 9 1 0 3073.19 2688.79 213.55 o 11 1 0 281.40 260.62 17.88 o 13 1 0 689.38 638.53 89.79 o 15 1 0 994.74 755.62 136.33 o 17 1 0 113.34 230.56 70.22 o 19 1 0 17.00 6.37 21.33 o 21 1 0 0.91 -3.87 16.47 o 23 1 0 181.84 177.37 34.28 o 25 1 0 3.36 -0.37 21.21 o 27 1 0 30.84 10.85 26.41 o 29 1 0 12.25 21.06 32.18 o 31 1 0 0.05 -10.71 33.64 o 0 2 0 7.37 0.36 5.66 o 2 2 0 964.97 1037.98 71.97 o 4 2 0 574.95 601.29 71.97 o 6 2 0 300.29 249.35 14.69 o 8 2 0 190.03 200.97 14.06 o 12 2 0 0.19 -1.41 7.22 o 14 2 0 4060.40 3500.46 148.17 o 16 2 0 34.56 19.33 8.91 o 18 2 0 0.39 -1.94 12.53 o 20 2 0 36.33 36.65 17.55 o 22 2 0 17.20 1.52 16.37 o 24 2 0 26.40 8.93 16.76 o 26 2 0 4.40 4.34 31.39 o 28 2 0 1.47 -29.39 29.39 o 30 2 0 0.03 -17.76 32.63 o 32 2 0 0.08 33.87 47.78 o 1 3 0 1731.58 1653.13 124.31 o 3 3 0 252.55 231.58 15.42 o 5 3 0 369.14 391.21 14.19 o 7 3 0 315.61 285.68 16.72 o 9 3 0 372.10 425.53 29.68 o 11 3 0 11.99 25.08 8.68 o 13 3 0 48.19 45.58 11.22 o 15 3 0 88.05 74.02 17.99 o 17 3 0 52.43 57.92 16.26 o 19 3 0 149.41 222.70 53.45 o 21 3 0 0.04 -1.13 17.24 o 23 3 0 0.24 -17.75 17.75 o 25 3 0 1.77 -19.60 30.05 o 27 3 0 0.35 -4.37 32.49 o 29 3 0 0.26 4.22 35.47 o 31 3 0 1.21 11.76 36.40 o 0 4 0 4838.74 4585.03 617.83 o 2 4 0 1371.51 1393.33 120.87 o 4 4 0 119.94 130.99 17.48 o 6 4 0 661.76 702.32 17.90 o 8 4 0 106.19 122.51 15.00 o 10 4 0 202.45 246.70 17.30 o 12 4 0 0.31 -6.66 9.10 o 14 4 0 0.05 0.31 9.47 o 16 4 0 53.19 49.81 12.41 o 18 4 0 20.24 24.39 17.91 o 20 4 0 114.10 123.49 23.78 o 22 4 0 31.11 30.03 23.63 o 24 4 0 45.85 73.72 36.12 o 26 4 0 4.82 4.96 33.09 o 28 4 0 16.54 17.26 34.19 o 30 4 0 1.64 -16.39 40.38 o 1 5 0 236.42 350.09 55.99 o 5 5 0 288.84 351.04 15.84 o 7 5 0 5.01 -8.34 10.03 o 9 5 0 651.68 572.64 35.57 o 11 5 0 1.75 5.92 11.54 o 13 5 0 7.80 7.64 11.10 o 15 5 0 35.38 20.19 12.21 o 17 5 0 141.53 189.04 39.26 o 19 5 0 680.80 644.87 80.57 o 21 5 0 128.68 121.14 29.44 o 23 5 0 7.09 3.87 32.30 o 25 5 0 2.27 -8.88 35.16 o 27 5 0 2.48 2.81 37.48 o 29 5 0 0.00 9.84 38.03 o 0 6 0 282.38 591.51 81.29 o 2 6 0 110.15 88.13 22.05 o 4 6 0 5.58 10.49 11.21 o 6 6 0 378.82 310.20 63.44 o 8 6 0 338.00 348.77 22.65 o 10 6 0 115.71 132.43 19.36 o 12 6 0 8.63 7.08 12.49 o 14 6 0 100.22 126.76 22.74 o 16 6 0 30.57 31.67 19.56 o 18 6 0 10.25 0.27 19.94 o 20 6 0 81.38 124.56 28.83 o 22 6 0 31.02 34.94 31.28 o 24 6 0 1.38 22.10 40.45 o 26 6 0 3.79 -2.04 36.26 o 1 7 0 10.43 -4.91 32.85 o 3 7 0 20.62 0.16 21.39 o 5 7 0 531.08 580.50 50.87 o 7 7 0 11.33 6.93 22.68 o 9 7 0 299.09 499.89 60.89 o 11 7 0 73.63 65.37 22.18 o 13 7 0 24.43 -0.03 19.66 o 15 7 0 42.35 48.10 27.71 o 17 7 0 136.92 207.00 53.42 o 19 7 0 199.19 221.87 44.67 o 21 7 0 35.08 24.78 53.42 o 0 8 0 5.62 11.61 43.36 o 2 8 0 3.25 -7.33 37.12 o 4 8 0 6.22 11.61 32.18 o 6 8 0 15.44 7.52 28.75 o 8 8 0 4.48 0.99 25.54 o 10 8 0 4.12 38.49 25.60 o 12 8 0 7.34 -10.99 21.54 o 14 8 0 0.56 -13.30 18.39 o 16 8 0 4.32 3.35 30.10 o 18 8 0 26.75 28.58 34.90 o 20 8 0 18.47 33.52 39.09 o 1 9 0 20.40 12.19 39.00 o 3 9 0 108.80 117.23 46.79 o 5 9 0 147.00 157.48 47.97 o 7 9 0 38.65 31.82 41.88 o 9 9 0 2.92 17.57 33.14 o 11 9 0 1.01 3.77 29.89 o 13 9 0 0.91 -1.74 23.88 o 15 9 0 6.00 21.55 42.68 o 17 9 0 16.21 16.24 43.21 o 19 9 0 7.22 3.07 39.66 o 0 10 0 1.89 -19.36 70.45 o 2 10 0 1.65 -1.33 51.37 o 4 10 0 8.59 21.40 46.69 o 6 10 0 0.17 15.88 41.39 o 8 10 0 0.23 -28.37 39.41 o 10 10 0 22.47 2.07 37.25 o 12 10 0 9.21 -6.66 27.87 o 14 10 0 0.61 23.42 47.47 o 1 11 0 21.06 31.29 61.83 o 3 11 0 26.26 46.51 64.31 o 5 11 0 22.52 41.41 56.85 o -31 1 1 40.84 36.94 37.43 o -29 1 1 174.55 98.34 37.14 o -27 1 1 23.12 21.04 28.47 o -25 1 1 96.97 86.46 29.74 o -23 1 1 327.36 392.88 46.93 o -21 1 1 12.06 1.41 19.29 o -19 1 1 187.72 270.01 34.08 o -17 1 1 255.81 360.37 22.91 o -15 1 1 1210.27 1418.46 174.13 o -13 1 1 156.92 223.54 24.50 o -11 1 1 679.96 775.66 72.63 o -9 1 1 302.25 284.89 33.68 o -7 1 1 0.35 3.86 5.00 o -5 1 1 469.71 509.52 29.58 o -1 1 1 26043.55 24185.81 592.31 o 1 1 1 698.85 789.50 42.58 o 3 1 1 640.44 604.00 10.63 o 5 1 1 67522.34 67075.91 483.21 o 7 1 1 11210.83 9962.70 517.71 o 9 1 1 1.10 -0.37 7.79 o 11 1 1 167.27 163.16 17.28 o 13 1 1 1059.29 1219.11 182.42 o 15 1 1 42.70 41.06 17.45 o 17 1 1 233.18 228.65 29.07 o 19 1 1 119.21 88.32 28.22 o 21 1 1 3.59 0.65 23.91 o 23 1 1 27.88 24.09 23.52 o 25 1 1 3.21 0.95 25.16 o 27 1 1 31.66 37.24 36.26 o 29 1 1 63.93 14.22 32.71 o 31 1 1 28.47 10.15 43.70 o -32 2 1 6.39 -7.96 33.27 o -30 2 1 30.88 0.98 31.05 o -28 2 1 34.10 1.67 32.71 o -26 2 1 3.37 -3.96 28.20 o -24 2 1 62.03 38.58 36.78 o -22 2 1 49.97 16.94 21.82 o -20 2 1 201.75 266.77 81.59 o -18 2 1 129.06 133.48 28.29 o -16 2 1 4.60 -0.19 11.64 o -14 2 1 184.31 204.28 16.43 o -12 2 1 654.97 644.46 17.67 o -10 2 1 1846.51 1987.67 27.84 o -6 2 1 40.53 52.16 8.60 o -4 2 1 1069.40 935.44 43.88 o -2 2 1 1889.10 1871.22 144.40 o 0 2 1 146.97 175.11 14.11 o 2 2 1 760.50 799.00 24.03 o 6 2 1 4070.28 4004.74 186.08 o 8 2 1 856.52 794.67 33.34 o 10 2 1 740.03 654.04 14.68 o 12 2 1 808.19 804.07 21.08 o 14 2 1 0.00 -1.52 11.85 o 16 2 1 23.33 28.23 13.95 o 18 2 1 205.00 144.24 23.60 o 20 2 1 163.90 206.08 28.82 o 22 2 1 4.40 -1.76 19.35 o 24 2 1 60.66 43.08 24.14 o 26 2 1 7.39 -13.72 25.77 o 28 2 1 5.35 0.07 23.75 o 30 2 1 8.97 -11.29 40.24 o -31 3 1 14.08 43.08 33.89 o -29 3 1 30.50 34.30 35.53 o -27 3 1 0.20 -18.94 30.58 o -25 3 1 22.22 17.65 32.74 o -23 3 1 9.39 11.11 31.35 o -21 3 1 3.52 -4.46 19.24 o -19 3 1 9.64 16.97 20.27 o -17 3 1 267.84 289.84 35.12 o -15 3 1 825.75 803.65 76.57 o -13 3 1 22.03 34.42 10.96 o -11 3 1 297.11 246.59 17.85 o -9 3 1 2451.01 2549.31 162.26 o -7 3 1 202.81 209.61 14.84 o -5 3 1 489.96 456.63 20.49 o -3 3 1 658.95 605.97 60.51 o -1 3 1 3908.13 4137.84 121.63 o 1 3 1 55.23 42.58 11.57 o 3 3 1 4.67 8.39 7.49 o 5 3 1 2655.82 2874.61 183.17 o 7 3 1 1080.05 1147.60 86.81 o 9 3 1 10.42 12.96 8.56 o 11 3 1 79.22 92.70 11.38 o 13 3 1 393.84 321.76 13.05 o 15 3 1 244.89 270.23 27.05 o 17 3 1 7.55 13.35 13.04 o 19 3 1 294.21 295.68 47.10 o 21 3 1 183.94 207.36 28.34 o 23 3 1 3.77 2.96 19.32 o 25 3 1 21.63 14.61 24.48 o 27 3 1 26.74 27.51 31.19 o 29 3 1 8.28 0.26 34.56 o 31 3 1 6.38 17.81 76.65 o -30 4 1 1.23 -1.48 41.56 o -28 4 1 0.01 6.58 37.75 o -26 4 1 14.49 8.07 37.22 o -24 4 1 37.50 47.33 37.81 o -22 4 1 0.23 21.68 24.24 o -20 4 1 44.56 72.88 20.93 o -18 4 1 0.07 -7.52 16.67 o -16 4 1 260.48 329.82 47.00 o -14 4 1 191.55 229.15 22.53 o -12 4 1 21.63 44.86 12.41 o -10 4 1 865.62 714.50 30.77 o -8 4 1 313.67 271.67 13.87 o -6 4 1 31.48 60.40 9.31 o -4 4 1 679.06 655.20 53.94 o -2 4 1 869.14 1116.86 113.77 o 0 4 1 887.51 964.72 29.48 o 2 4 1 1945.72 2322.89 88.19 o 4 4 1 4215.53 4483.43 105.49 o 6 4 1 238.24 233.29 25.47 o 8 4 1 39.53 40.44 11.69 o 10 4 1 39.42 28.58 10.04 o 12 4 1 5.07 -1.05 10.10 o 14 4 1 6.71 -7.44 9.46 o 16 4 1 35.85 40.71 15.15 o 18 4 1 22.18 36.95 18.23 o 20 4 1 37.26 44.46 20.44 o 22 4 1 11.75 10.43 20.59 o 24 4 1 41.32 59.96 24.71 o 26 4 1 12.25 -5.61 37.48 o 28 4 1 0.99 24.87 38.46 o 30 4 1 4.46 27.10 58.84 o -29 5 1 15.03 20.16 42.53 o -27 5 1 0.01 -1.29 42.11 o -25 5 1 2.64 -17.26 36.02 o -23 5 1 14.53 -0.16 34.73 o -21 5 1 4.34 11.72 23.82 o -19 5 1 47.48 88.44 24.26 o -17 5 1 142.92 234.29 37.10 o -15 5 1 171.95 232.95 29.74 o -13 5 1 22.23 30.74 14.58 o -11 5 1 359.27 363.97 23.53 o -9 5 1 12.45 7.88 11.41 o -7 5 1 28.76 32.16 10.61 o -5 5 1 933.71 842.06 42.94 o -3 5 1 453.66 374.20 32.61 o -1 5 1 20.03 37.33 15.59 o 1 5 1 372.93 363.93 33.77 o 3 5 1 1074.48 1129.49 52.40 o 5 5 1 1751.34 1839.54 86.61 o 7 5 1 165.75 189.43 16.78 o 9 5 1 145.05 179.41 18.64 o 11 5 1 247.36 308.38 29.75 o 13 5 1 307.24 308.13 30.04 o 15 5 1 100.82 144.97 32.46 o 17 5 1 92.63 124.06 21.48 o 19 5 1 0.79 8.34 22.03 o 21 5 1 19.38 13.34 20.36 o 23 5 1 15.71 32.88 23.75 o 25 5 1 0.06 -0.49 23.40 o 27 5 1 3.44 19.27 37.97 o -26 6 1 0.47 -39.91 46.45 o -24 6 1 4.07 -14.17 35.52 o -22 6 1 46.33 54.55 35.79 o -20 6 1 84.80 100.72 27.75 o -18 6 1 1.28 -8.11 21.43 o -16 6 1 37.79 59.60 16.02 o -14 6 1 1148.66 912.23 134.49 o -12 6 1 1294.47 1137.59 232.66 o -10 6 1 1000.26 801.69 37.20 o -8 6 1 7.25 -9.09 12.35 o -6 6 1 338.26 344.99 36.32 o -4 6 1 70.00 71.55 25.66 o -2 6 1 5.04 11.37 26.32 o 0 6 1 0.67 -7.96 19.53 o 2 6 1 10.96 -10.12 17.64 o 4 6 1 3.42 -2.46 18.72 o 6 6 1 9.48 -8.18 10.31 o 8 6 1 32.13 28.05 13.53 o 10 6 1 716.97 603.58 43.17 o 12 6 1 163.18 208.68 27.99 o 14 6 1 249.12 298.05 51.95 o 16 6 1 333.11 426.79 34.36 o 18 6 1 296.09 345.50 31.96 o 20 6 1 36.89 17.40 25.96 o 22 6 1 10.08 9.53 32.49 o 24 6 1 77.00 60.89 37.67 o 26 6 1 48.98 66.58 62.71 o -23 7 1 0.63 -24.00 65.03 o -21 7 1 5.44 12.43 34.90 o -19 7 1 23.76 28.15 39.87 o -17 7 1 14.39 7.52 24.64 o -15 7 1 199.86 271.51 49.73 o -13 7 1 139.04 152.84 23.70 o -11 7 1 53.48 57.40 18.83 o -9 7 1 41.66 52.66 28.33 o -7 7 1 50.86 49.02 23.28 o -5 7 1 618.01 621.83 55.74 o -3 7 1 0.50 3.43 26.26 o -1 7 1 246.09 425.97 56.52 o 1 7 1 57.78 98.30 27.86 o 3 7 1 11.05 10.66 23.41 o 5 7 1 26.70 21.89 15.44 o 7 7 1 25.88 12.92 21.49 o 9 7 1 232.51 291.00 28.05 o 11 7 1 0.69 -10.05 16.96 o 13 7 1 37.48 41.23 15.34 o 15 7 1 8.73 7.09 21.72 o 17 7 1 12.32 15.79 22.10 o 19 7 1 64.63 78.65 27.89 o 21 7 1 15.66 -22.10 30.21 o 23 7 1 0.02 8.25 36.08 o -20 8 1 64.65 43.36 48.78 o -18 8 1 12.77 25.55 41.81 o -16 8 1 0.13 -8.48 35.80 o -14 8 1 3.45 3.65 20.54 o -12 8 1 0.28 -16.21 22.03 o -10 8 1 16.58 21.24 24.95 o -8 8 1 1.42 23.44 33.73 o -6 8 1 0.08 -13.87 29.65 o -4 8 1 119.65 127.59 38.68 o -2 8 1 0.37 13.20 34.22 o 0 8 1 505.75 722.76 129.30 o 2 8 1 540.49 658.46 51.08 o 4 8 1 219.42 301.42 42.85 o 6 8 1 1.33 3.52 26.48 o 8 8 1 2.18 5.53 23.45 o 10 8 1 22.62 12.78 23.49 o 12 8 1 15.03 23.93 20.59 o 14 8 1 0.00 -3.98 34.57 o 16 8 1 1.10 -31.48 36.75 o 18 8 1 0.46 19.36 33.45 o 20 8 1 0.72 17.03 64.26 o 22 8 1 0.49 -19.36 65.81 o -19 9 1 35.00 54.97 52.65 o -17 9 1 8.38 20.11 51.49 o -15 9 1 1.04 3.45 22.83 o -13 9 1 0.17 -9.30 25.25 o -11 9 1 7.31 -19.06 30.62 o -9 9 1 23.26 9.10 34.21 o -7 9 1 0.63 -23.35 36.36 o -5 9 1 56.07 48.20 40.56 o -3 9 1 34.93 20.73 42.88 o -1 9 1 5.33 -16.31 38.50 o 1 9 1 5.63 12.32 42.11 o 3 9 1 19.38 -6.54 43.34 o 5 9 1 7.34 25.42 35.16 o 7 9 1 11.70 10.81 33.69 o 9 9 1 69.74 94.77 34.06 o 11 9 1 8.86 -8.41 25.62 o 13 9 1 3.33 -4.74 38.50 o 15 9 1 0.08 -4.63 44.89 o 17 9 1 0.02 16.40 35.32 o -14 10 1 21.71 22.96 31.71 o -12 10 1 11.49 11.14 31.76 o -10 10 1 0.78 4.65 41.03 o -8 10 1 0.14 -23.12 39.42 o -6 10 1 8.63 -6.97 50.40 o -4 10 1 47.42 71.82 48.26 o -2 10 1 29.94 67.56 59.68 o 0 10 1 2.72 -10.62 47.79 o 2 10 1 1.71 -11.64 46.87 o 4 10 1 8.92 -6.46 56.13 o 6 10 1 0.46 -33.40 42.74 o 8 10 1 26.28 21.90 37.65 o 10 10 1 22.33 26.37 33.75 o 12 10 1 2.63 37.50 58.25 o -3 11 1 6.73 40.32 66.03 o -1 11 1 9.01 36.11 57.05 o 1 11 1 0.01 25.88 62.15 o 3 11 1 0.08 -1.31 57.96 o -32 0 2 9.80 8.52 61.16 o -30 0 2 40.74 8.52 48.00 o -28 0 2 10.60 -17.03 45.68 o -26 0 2 13.35 6.97 37.16 o -22 0 2 42.74 18.58 37.94 o -20 0 2 299.02 404.73 193.17 o -18 0 2 40.31 55.76 24.93 o -16 0 2 68.13 204.39 39.87 o -12 0 2 537.62 527.93 27.52 o -10 0 2 222.57 253.64 26.60 o -8 0 2 333.36 324.33 23.61 o -6 0 2 6843.67 6904.61 399.89 o -4 0 2 94.85 77.93 12.56 o -2 0 2 287.91 345.45 37.55 o 0 0 2 14369.91 13513.32 139.36 o 6 0 2 8647.31 9309.23 615.12 o 8 0 2 1918.14 1956.47 68.13 o 10 0 2 7887.09 7639.27 142.46 o 12 0 2 1528.57 1750.52 82.84 o 14 0 2 22.37 54.97 41.81 o 16 0 2 2.73 0.77 36.39 o 18 0 2 121.73 63.49 42.58 o 20 0 2 20.11 11.61 37.16 o 22 0 2 112.98 170.33 54.20 o 24 0 2 6.21 8.52 42.58 o 26 0 2 2.45 -20.90 38.71 o 28 0 2 110.17 161.81 86.71 o 30 0 2 16.99 63.49 63.49 o -31 1 2 0.94 -5.95 31.70 o -29 1 2 1.21 10.24 33.34 o -27 1 2 2.00 4.78 30.20 o -25 1 2 0.83 -10.25 28.08 o -23 1 2 272.23 361.12 45.16 o -21 1 2 106.28 152.61 33.05 o -19 1 2 611.98 725.82 115.21 o -17 1 2 7.82 10.46 12.89 o -15 1 2 3.41 -10.00 10.00 o -13 1 2 10.08 8.14 8.77 o -11 1 2 41.33 29.55 8.64 o -9 1 2 2248.39 2504.84 92.75 o -7 1 2 3326.54 3126.32 72.97 o -5 1 2 671.92 703.54 84.60 o -3 1 2 6.35 1.23 4.60 o -1 1 2 5102.95 4808.03 188.67 o 1 1 2 554.82 581.95 62.16 o 3 1 2 2815.79 2960.92 390.04 o 5 1 2 6734.51 7789.94 655.86 o 7 1 2 2823.20 3063.03 206.18 o 9 1 2 1681.54 1709.06 171.46 o 11 1 2 30.58 15.64 10.26 o 13 1 2 106.58 108.34 24.90 o 15 1 2 78.75 54.85 23.81 o 17 1 2 37.94 58.88 28.88 o 19 1 2 138.77 126.31 36.79 o 21 1 2 24.36 35.29 30.38 o 23 1 2 35.10 20.27 24.78 o 25 1 2 11.40 -2.00 35.16 o 27 1 2 5.86 -13.55 37.77 o 29 1 2 0.02 -2.40 35.36 o 31 1 2 0.49 -3.43 59.46 o -30 2 2 7.99 23.89 31.18 o -28 2 2 1.09 25.14 33.09 o -26 2 2 0.34 -5.08 25.67 o -24 2 2 4.14 -14.02 26.26 o -22 2 2 16.61 15.89 27.23 o -20 2 2 94.56 133.11 59.11 o -18 2 2 123.97 268.65 55.87 o -16 2 2 28.50 20.31 13.70 o -14 2 2 11.10 23.48 11.45 o -12 2 2 547.30 549.04 39.26 o -10 2 2 12816.15 13008.90 213.10 o -8 2 2 459.39 382.17 30.90 o -4 2 2 171.42 161.03 8.57 o -2 2 2 113.20 155.07 16.11 o 0 2 2 3.66 29.30 14.63 o 2 2 2 521.79 535.57 16.15 o 4 2 2 672.42 743.28 23.80 o 6 2 2 0.67 -2.93 6.84 o 8 2 2 96.96 94.48 10.48 o 10 2 2 2158.48 2117.82 72.59 o 12 2 2 303.07 242.82 27.80 o 14 2 2 299.88 287.87 21.63 o 16 2 2 10.14 11.48 25.35 o 18 2 2 987.66 749.15 80.13 o 20 2 2 17.33 6.87 22.08 o 22 2 2 6.14 8.81 22.81 o 24 2 2 6.88 -24.50 25.84 o 26 2 2 15.82 -5.57 31.44 o 28 2 2 5.93 25.67 37.72 o 30 2 2 4.24 -38.24 51.73 o -31 3 2 11.54 -22.40 36.02 o -29 3 2 25.65 24.54 35.17 o -27 3 2 0.75 -11.65 36.26 o -25 3 2 5.00 -0.57 30.69 o -23 3 2 3.77 -14.26 30.05 o -21 3 2 2.73 29.20 27.68 o -19 3 2 7.63 54.67 22.54 o -17 3 2 55.52 83.96 15.81 o -15 3 2 454.99 438.90 44.68 o -13 3 2 1.75 1.41 10.24 o -11 3 2 24.95 13.55 9.80 o -9 3 2 612.63 608.92 66.55 o -7 3 2 86.53 74.12 9.08 o -5 3 2 7082.89 7393.96 481.73 o -3 3 2 1818.23 1792.95 35.07 o -1 3 2 1776.36 1786.42 61.98 o 1 3 2 1554.82 1621.15 110.57 o 3 3 2 1737.05 1853.14 59.94 o 5 3 2 2.30 -5.90 7.70 o 7 3 2 1245.59 1134.39 51.94 o 9 3 2 1382.43 1218.07 31.53 o 11 3 2 719.34 669.02 38.80 o 13 3 2 356.06 316.02 23.80 o 15 3 2 120.16 145.71 18.28 o 17 3 2 62.53 57.79 18.02 o 19 3 2 86.42 95.13 22.38 o 21 3 2 1.38 -13.67 19.09 o 23 3 2 106.19 83.25 26.03 o 25 3 2 16.95 34.71 28.39 o 27 3 2 0.60 6.29 31.49 o 29 3 2 1.37 -44.87 45.35 o -30 4 2 32.20 34.89 43.16 o -28 4 2 0.01 -20.22 37.03 o -26 4 2 13.14 23.46 38.80 o -24 4 2 47.60 66.41 46.84 o -22 4 2 1.50 -17.73 25.67 o -20 4 2 52.92 89.46 36.96 o -18 4 2 23.17 34.30 16.92 o -16 4 2 69.25 83.21 17.12 o -14 4 2 52.15 28.20 12.76 o -12 4 2 19.27 17.78 10.02 o -10 4 2 38.05 50.01 12.52 o -8 4 2 1.57 14.21 9.68 o -6 4 2 203.27 230.27 16.28 o -4 4 2 1456.47 1487.43 72.05 o -2 4 2 698.76 753.31 92.16 o 0 4 2 931.47 932.63 28.08 o 2 4 2 144.99 210.89 24.93 o 4 4 2 829.05 855.79 28.28 o 6 4 2 668.57 730.62 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