Acta Cryst. (2003). E59, o713-o715  [ doi:10.1107/S1600536803008882 ]

1,1-Dichloro-3-méthylthio-1a-phényl-1,1a,2,9-tétrahydroaziridino[2,1-d][1,5]benzodiazépine

S. El Hazazi, S. Baouid, A. Hasnaoui and M. Pierrot

Online 30 avril 2003

Key indicators

• Single-crystal X-ray study
• T = 293 K
• Mean (C-C) = 0.004 Å
• R factor = 0.023
• wR factor = 0.058
• Data-to-parameter ratio = 8.3

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           26.37                 
         From the CIF: _reflns_number_total               1666                  
         Count of symmetry unique reflns         1700                           
         Completeness (_total/calc)             98.00%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured         0                           
         Fraction of Friedel pairs measured     0.000                           
         Are heavy atom types Z>Si present          yes                         
          WARNING: Large fraction of Friedel related reflns may                 
                   be needed to determine absolute structure                    

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