Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 59| Part 6

ISSN: 2056-9890

June 2003 issue

Highlighted illustration

Cover illustration: This lithium compound contains an unusual non-planar four-membered Li-N-Si-N ring with both three- and four-coordinate N atoms. It may serve as an intermediate in the synthesis of other novel compounds. See Shi, Liu & Huang [Acta Cryst. E59, m339-m341].

inorganic compounds

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Monoclinic modification of polymorphic TbB₃O₆

A. Goriounova, P. Held, P. Becker and L. Bohatý

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A reinvestigation of the structure of Cs₃Ta₅O₁₄

D. du Boulay, A. Oono and N. Ishizawa

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A new polymorph of hexaaquamagnesium(II) bis(hypophosphite)

N. V. Kuratieva, M. I. Naumova, D. Y. Naumov and N. V. Podberezskaya

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Na_0.6601Ce_0.1133(H₂PO₄)·H₂O

E. B. Zarkouna, M. F. Zid and A. Driss

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metal-organic compounds

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Tris(quinolin-8-olato)indium(III)

M. Rajeswaran and V. V. Jarikov

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trans(Cl,N_amino)-Chloro(dimethyl sulfoxide-κS)[tris(2-pyridylmethyl)amine-κ⁴N]ruthenium(II) trichlorotris(dimethyl sulfoxide-κS)ruthenate(II)

D. Masui, M. Yamaguchi and T. Yamagishi

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Δ-Aqua-S-citrato(2–)manganese(II)

Y.-F. Deng, Z.-H. Zhou, H.-L. Wan and S. W. Ng

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[1,2-Bis(methylthio)ethane-κ²S,S′]dichlorozinc(II)

M. Parvez, P. D. Clark and H. Yao

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trans,trans,trans-Diethanoldiquinaldinatoiron(II)

K. Osawa, H. Furutachi, S. Fujinami and M. Suzuki

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Tris[μ-bis(diphenylphosphino)methane-κ²P:P′]di-μ₃-sulfanido-trisilver(I) hexafluoroantimonate dichloromethane disolvate

Y.-H. Qin, M.-M. Wu and Z.-N. Chen

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[Benzyldimethyl(dimethylamino)silyl-κ²C,N](N,N,N,N-tetramethylenediamine-κ²N,N)lithium(I)

H.-P. Shi, D.-S. Liu and S.-P. Huang

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Tris(nitrato-κ²O,O′)tris(triphenylphosphine oxide-κO)terbium(III) acetone sesquisolvate

M. L. Matthews and M. Webster

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An aquazinc(II) complex of 1,10-phenanthroline with fumarate counter-ions

J. Yang, J.-F. Ma and J.-F. Liu

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Quinolinium dichromate, [C₉H₇NH⁺]₂·Cr₂O₇²⁻

T. V. Sundar, V. Parthasarathi, S. Thamotharan and K. G. Sekar

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catena-Poly[[diaquabis(1H-benzimidazole-κN³)nickel(II)]-μ-succinato-κ²O:O′]

Y. Liu, J.-M. Gu and D.-J. Xu

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Diaqua(4,4′-bipyridine)bis(4-cyanobenzoato)cobalt(II)

H.-Y. He, A.-Q. Ma and L.-G. Zhu

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Tetrasodium tetrahydroxytetrathiacalix[4]arenetetrasulfonate tetradecahydrate

H. Akashi and T. Yamauchi

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[(1-tert-Butyl-2-phenylvinylamino)(dimethylamino)dimethylsilyl-κ²N,N′] (N,N,N′,N′-tetramethylenediamine-κ²N,N′)lithium(I)

H.-P. Shi, D.-S. Liu and S.-P. Huang

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A one-dimensional double-wavelike chain coordination polymer: catena-poly[[diaquamanganese(II)]-μ-(2,2′-bipyridyl-3,3′-dicarboxylato-κ⁴N,N′:O,O′)]

H.-T. Zhang, T. Shao, H.-Q. Wang and X.-Z. You

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Triguanidinium hexahydrogenhexamolybdocobaltate(III) tetrahydrate

U. Lee, S.-J. Jang, H.-C. Joo and K.-M. Park

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Bis(N-cyclohexyl-N-methyldithiocarbamato)dimethyltin(IV)

N. Awang, I. Baba, M. S. M. Yusof and B. M. Yamin

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cis-Dichlorobis(diethyl 2-pyridylmethylphosphonate-κN)platinum(II) hemihydrate, cis-[PtCl₂(2-pmpe)₂]·0.5H₂O

L. Chęcińska, M. Małecka, J. Ochocki and K. Aranowska

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Diaquatris(4-pyridylcarboxylato)neodymium(III)

T. Shao and H.-T. Zhang

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Tetraaqua-trans-bis(nicotinato-κN)cadmium(II)

Y. Zhou, W. Bi, X. Li, J. Chen, R. Cao and M. Hong

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Dichlorobis(triphenylphosphine oxide)magnesium

B. E. Kucera, M. M. Olmstead, R. S. Tanke and S. M. Kauzlarich

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[N,N,N′,N′-Tetrakis(2-benzimidazolylmethyl)-1,2-ethanediamine]zinc(II) dinitrate ethanol solvate

Y.-C. Liu, J.-F. Ma, N.-H. Hu and H.-Q. Jia

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Tetrakis[(9-oxo-10-thiaxanthen-2-yloxyethyl)ammonium] decaiodotriplumbate(II)

K. R. Maxcy, R. D. Willett, D. B. Mitzi and A. Afzali

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2-Aminoethylammonium tris(1,2-ethylenediamine)nickel(II) tetraselenoantimonate(V)

M.-L. Fu, W.-T. Chen, L.-Z. Cai, G.-W. Zhou, G.-C. Guo, J.-G. Mao and J.-S. Huang

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cis-Dichlorotetrakis(2-mercapto-1-tert-butylimidazole)lead(II)

R. N. Evans, D. J. Mihalcik, D. S. Jones and D. Rabinovich

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catena-Poly[tetramethylammonium [[(nitrato-κ²O,O′)dioxouranium]-μ₃-sulfato]]

M. B. Doran, A. J. Norquist and D. O'Hare

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Bis(μ-di-tert-butylphosphido)bis[(triethylphosphine)palladium(I)](Pd—Pd)

U. Englert, E. Matern, J. Olkowska-Oetzel and J. Pikies

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Bis[tris(1,3-diaminopropane)manganese(II)] octasulfidotetraantimonate(III) dihydrate

L. Engelke and W. Bensch

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Bis[(S)-β-phenethylammonium] tribromoplumbate(II)

D. G. Billing and A. Lemmerer

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Tris(triphenylphosphine)copper(I) hexafluorophosphate

P. C. Healy and J. V. Hanna

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Bis{2-[(2-aminoethylimino)(phenyl)methyl]pyridine-κ³N}nickel(II) diperchlorate

A. Usman, H.-K. Fun, T. K. Karmakar, B. K. Ghosh and S. K. Chandra

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Diaquaiminodiacetatonickel(II)

Y.-R. Wu, L.-S. Long, R.-B. Huang, L.-S. Zheng and S. W. Ng

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Polymeric aqua(μ₄-maleato-κ⁴O)pyridylnickel(II)

Y. Chen, P. Liu, J. Wang and W.-D. Cheng

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organic compounds

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Pyridinium oxalate(1–) oxalic acid dihydrate

K. Rajagopal, V. Tamilselvi, R. V. Krishnakumar and S. Natarajan

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4,5,9,10-Tetrahydro-4,9-methanodithieno[3,2-b:3′,2′-f][1,5]diazocine

T. Kobayashi, T. Moriwaki and M. Shiro

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2-Methoxymethyl-1,3-dithiolane 1,1,3,3-tetraoxide

Ö. Özcan, Z. Gültekin, W. Frey and T. Hökelek

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1-Acetyl-3-(p-chlorobenzyl)-4-(p-chlorobenzylidenamino)-4,5-dihydro-1H-1,2,4-triazol-5-one

N. Ocak, U. Çoruh, B. Kahveci, S. Şaşmaz, E. Ag~ar, E. M. Vázquez-López and A. Erdönmez

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Disordered 2,2′,3,3′,4,6,6′-hepta-O-pivaloyl-α,α′-trehalose

T. C. Baddeley, S. M. Clow, P. J. Cox, I. G. Davidson, A. M. Murdoch and J. L. Wardell

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(5aR,8aR,9R)-9-(3,4,5-Trimethoxyphenyl)-5a,6,8a,9-tetrahydrofuro[3′,4′:6,7]naphtho[2,3-d][1,3]dioxole-5,8-dione

J.-F. Shi and Y.-G. Wang

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2-Acetylphenylboronic acid monohydrate

A. Ganguly, C. Y. Meyers and P. D. Robinson

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2-Bromo-N-(p-toluenesulfonyl)pyrrole

L. W. Knight, C. W. Padgett, J. W. Huffman and W. T. Pennington

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Dicyclohexylammonium benzenethiolate

K. Baranowska, J. Chojnacki, B. Becker and W. Wojnowski

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Flavone

M. P. Waller, D. E. Hibbs, J. Overgaard, J. R. Hanrahan and T. W. Hambley

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Guanidinium dihydrogen phosphite

W. T. A. Harrison

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Trilobolide-6-O-isobutyrate, a eudesmanolide from Wedelia trilobata

X.-S. Huang, R.-W. Jiang and V.E.-C. Ooi

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2-(2-Hydroxyphenyl)-1,3-dithiane

A. Usman, H.-K. Fun, N. C. Ganguly, M. Datta and K. Ghosh

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Redetermination of 8-tosyloxyquinoline at 100 K: supramolecular aggregation through weak C–H⋯O and C–H⋯N interactions

N. Vembu, M. Nallu, J. Garrison and W. J. Youngs

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(3E)-3-[(4-Butylphenyl)imino]-1,3-dihydro-2H-indol-2-one

M. Akkurt, S. Öztürk, A. Erçağ, M. Ü. Özgür and F. W. Heinemann

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trans-2,3-Bis(methylsulfonyl)indane

M. Parvez, P. D. Clark and A. Primak

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3,3′-Bis(3-cyanopropyl)-1,1′-propylenedi(benzimidazolium) dichloride dihydrate

M. Akkurt, S. Öztürk, H. Küçükbay, N. Okuyucu and H.-K. Fun

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Spiro[1,3-dioxolane-2,4′-[8]phenylsulfonylbicyclo[4.2.0]octan-1-ol]

W. A. Loughlin, M. A. McCleary and P. C. Healy

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4,4′-Trimethylenedipyridinium dinitrate

T. W. Lee, J. P. K. Lau and L. Szeto

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4-(4-Chlorophenyl)-1,3-diphenyl-7-oxa-1,2-diazaspiro[4.4]non-2-en-6-one

X.-F. Li, Y.-Q. Feng, X.-F. Hu and M. Xu

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13-Benzyl-3,10-bis(2,6-dichlorophenyl)-4,11-diphenyl-1,8-dioxa-2,9,13-triazadispiro[4.1.4.3]tetradeca-2,9-dien-6-one chloroform solvate

X.-F. Li, Y.-Q. Feng, X.-F. Hu and M. Xu

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1,3-Diphenoxy-2,2-bis(phenoxymethyl)propane

D. Laliberté, T. Maris and J. D. Wuest

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6-Phenyl-4,5-dihydropyridazin-3(2H)-one

S. Abourichaa, N. Benchat, A. Anaflous, A. Melhaoui, T. Ben-Hadda, B. Oussaid, B. El Bali and M. Bolte

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4-(p-Fluorobenzylamino)-3-phenyl-4,5-dihydro-1H-1,2,4-triazol-5-one

Ş. Işık, B. Kahveci, E. Ag~ar and S. Şaşmaz

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3,4:9,10-Dibenzo-1,12-diformyl-5,8-dioxododecane

P. G. Aravindan, M. Yogavel, M. Thirumavalavan, P. Akilan, D. Velmurugan, M. Kandaswamy, S. Shanmuga Sundara Raj and H.-K. Fun

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1,2,3,4,4a,12a-Hexahydro-2,5,5-trimethyl-1H-[2]benzopyrano[3,2-c]coumarin

R. Krishna, S. Selvanayagam, M. Yogavel, D. Velmurugan, M. Shanmugasundaram, R. Raghunathan, S. Shanmuga Sundara Raj and H.-K. Fun

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N-(N-Benzoylhydrazinocarbothioyl)benzamide

M. S. M. Yusof, B. M. Yamin and M. Shamsuddin

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2,2′-Diamino-4,4′-bi-1,3-thiazolium fumarate

J.-G. Liu, D.-J. Xu and W.-L. Sun

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1-[(5-Chloro-2-hydroxyphenyl)(phenyl)methyl]-2-(2-pyridyl)-1H-benzimidazole

P.-M. Jian, Y.-Z. Li, X.-L. Wu, Y.-X. Ma, D.-H. Pan and B.-H. Chen

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N-Benzoyl-N′-(2-hydroxyethyl)thiourea

Y.-M. Zhang, L. Xian, T.-B. Wei and L.-X. Cai

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3-(Benzoxazol-2-yl)-7-hydroxychromen-2-one methanol solvate

E. F. Franca, A. E. H. Machado, A. M. F. Oliveira-Campos, S. Santos Jr, J. Ellena and S. Guilardi

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1,4-Bis(2-phenylethoxy)benzene

C. M. L. Vande Velde, J. K. Baeke, H. J. Geise and F. Blockhuys

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Diethyl N,N′-m-phenylenedioxamate

I. I. Padilla-Martínez, M. Chaparro-Huerta, F. J. Martínez-Martínez, H. Höpfl and E. V. García-Báez

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3-(3-Benzoylthioureido)propionic acid

M. S. M. Yusof and B. M. Yamin

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4-Methoxyphenyl 4-toluenesulfonate: supramolecular aggregation through C—H⋯O and C—H⋯π interactions

N. Vembu, M. Nallu, J. Garrison, K. Hindi and W. J. Youngs

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2-Trichloroacetyl-1-(1-pyrrolidinyl)cyclopentene

F. B. Kaynak, S. Özbey, H. Şenöz and N. Tunog~lu

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Triethyl benzene-1,3,5-tricarboxylate

S. H. Dale and M. R. J. Elsegood

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Isobutyraldehyde 2,4-dinitrophenylhydrazone

S. Shan, D.-J. Xu and W.-X. Hu

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2,2-Dimethyl-5-(N-methyl-N-methoxyaminomethylene)-1,3-dioxane-4,6-dione

A. J. Blake, H. McNab and K. Withell

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Bis(pentachlorophenyl) disulfide

S.-L. Deng, L.-S. Long, S.-Y. Xie, R.-B. Huang, L.-S. Zheng and S. W. Ng

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Butanedithiol diacetate

H. Fleischer and D. Schollmeyer

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Disordered 4,4′-di-O-isobutyroyl-2,2′,3,3′,6,6′-hex-O-acetyl-α,α′-trehalose

T. C. Baddeley, S. M. Clow, P. J. Cox, I. G. Davidson, C. Ryder and J. L. Wardell

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N-[3,5-Bis(trifluoromethyl)phenyl]-3-methoxysalicylaldimine

N. Karadayı, S. Gözüyeşil, B. Güzel, Canan Kazak and O. Büyükgüngör

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4-(E)-But-1-enyl-2,6-dimethoxyphenyl nicotinate

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DL-Valine-fumaric acid (2/1)

M. Alagar, R. V. Krishnakumar, M. Subha Nandhini and S. Natarajan

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(E)-Azulene-1-carboxaldehyde oxime

K. Mariusz, K. Hafner and H. J. Lindner

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2-Amino-6-bromopyridinium bromide

B. T. Holmes, C. W. Padgett and W. T. Pennington

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(S)-2,2′-Bis(4-nitro-2-pyridyloxy)-1,1′-binaphthalene

R. Wang, L. Xu, G. Chen, Z. Zhou, M. Hong, R. Cao and A. S. C. Chan

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An unexpected product: di-μ-iodo-bis{[2-(N-diphenylphosphinomethyl-N-cyclohexylamino)pyridine]iodomercury(II)}

D.-J. Cui, X.-S. Zeng, X.-B. Leng, F.-B. Xu and Z.-Z. Zhang

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Diethyl [(6-chlorobenzothiazol-2-yl)amino]thiophosphate

B. Shi, R. Chen and Y. Huang

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A new polymorph of 3-phenylpyrazole

A. Haghiri, H.-W. Lerner and M. Bolte

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3-(1-Phenylsulfonyl-2-methylindol-3-ylcarbonyl)propanoic acid

R. Krishna, P. G. Aravindan, M. Yogavel, D. Velmurugan, S. Shanmuga Sundara Raj, H.-K. Fun and P. C. Srinivasan

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L-Leucinium oxalate

K. Rajagopal, R. V. Krishnakumar, M. Subha Nandhini, R. Malathi, S. S. Rajan and S. Natarajan

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2(R)-Hydroxy-4-(4-methoxybenzoyl)-2-methoxycarbonylmethyl-5-(4-methoxyphenyl)-1-(2-methylphenyl)-2,3-dihydro-1H-3-pyrrolone

S. Öztürk, M. Saçmacı, Ş. H. Üngören, M. Akkurt, H.-K. Fun and Y. Akçamur

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N-Hydroxy-2-oxo-2,N′-diphenylacetamidine

O. Büyükgüngör, T. Hökelek, M. Taş and H. Batı

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L-Argininium bis(dihydrogen phosphate)

R. Ittyachan, P. Sagayaraj and B. Kothandapani

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1(5),6(7)-Diepoxy-4-guaiol hemihydrate

X.-Q. Ma, C.-Z. Liao, J.-Y. Su and L.-M. Zeng

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9-(para-tert-Butylphenyl)-9-fluorenol

A. W. McLean, C. Y. Meyers and P. D. Robinson

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3-(4-Methoxyphenyl)-4-(5-phenyl-2,4-pentadienoyl)sydnone

S. Thamotharan, V. Parthasarathi, R. Sanyal, B. Badami and A. Linden

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(9-Anthrylmethyl)trimethylammonium chloride monohydrate

C. M. Beaudry, J. Pehl and K. M. Wovkulich

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1,6,7-Tris(bromomethyl)naphthalene

P. Kuś and P. G. Jones

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N,N′-Bis(4-biphenylyl)urea

S. George and A. Nangia

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Research communications are designed to help authors bring out the science behind their structure determinations. Authors are encouraged to report more than one structure in the same communication and also to include the results of investigations with other techniques. The Research communications format makes Acta E the natural home for structure determinations with interesting science to report.

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