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Acta Cryst. (2003). E59, m367-m369 [ doi:10.1107/S1600536803009243 ]
Abstract: The new molecular metal chalcogenide, (enH)[Ni(en)3][SbSe4] or (C2H9N2)[Ni(C2H8N2)3][SbSe4], has been synthesized by a solvothermal reaction in an ethylenediamine/methanol solution at 443 K. The structure contains tetrahedral SbSe43- anions and octahedral [Ni(en)3]2+ cations, as well as the monoprotonated ethylenediamine cation [enH]+.
Online 23 May 2003
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