(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2003). E59, m367-m369 [ doi:10.1107/S1600536803009243 ]

2-Aminoethylammonium tris(1,2-ethylenediamine)nickel(II) tetraselenoantimonate(V)

M.-L. Fu, W.-T. Chen, L.-Z. Cai, G.-W. Zhou, G.-C. Guo, J.-G. Mao and J.-S. Huang

Online 23 May 2003

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.007 Å
R factor = 0.054
wR factor = 0.088
Data-to-parameter ratio = 24.7

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



PLAT_213  Alert C Atom C11     has ADP max/min Ratio ...........       3.20 prolate

PLAT_360  Alert C Short  C(sp3)-C(sp3) Bond  C(11)  -   C(12)  =       1.42 Ang.

PLAT_420  Alert C D-H Without Acceptor       N(11)  -   H(11A)            ?

PLAT_420  Alert C D-H Without Acceptor       N(15)  -   H(15A)            ?

PLAT_420  Alert C D-H Without Acceptor       N(15)  -   H(15B)            ?

PLAT_420  Alert C D-H Without Acceptor       N(22)  -   H(22C)            ?

General Notes



ABSTM_02  When printed, the submitted absorption T values will be replaced      
          by the scaled T values. Since the ratio of scaled T's is              
          identical to the ratio of reported T values, the scaling does         
          not imply a change to the absorption corrections used in the          
          study.                                                                
          Ratio of Tmax expected/reported      0.769                            
          Tmax scaled      0.769 Tmin scaled      0.587                         


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 6 Alert Level C = Please check