# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 021125J in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 647.24 _exptl_crystal_F_000 1344.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 13.9217 _cell_length_b 14.8411 _cell_length_c 15.0237 _cell_angle_alpha 65.547 _cell_angle_beta 70.265 _cell_angle_gamma 67.182 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 109493.88 0.00 8.87 o 2 0 0 19947.16 25056.18 775.94 o 3 0 0 73.55 112.25 29.66 o 4 0 0 220.22 237.55 39.10 o 5 0 0 13.61 0.00 34.49 o 6 0 0 6734.68 6944.55 195.48 o 7 0 0 4545.23 4513.82 159.62 o 8 0 0 3674.58 3923.25 147.26 o 9 0 0 36.86 168.85 50.04 o 10 0 0 244.66 263.02 77.59 o 11 0 0 2406.36 2778.55 192.88 o 12 0 0 466.79 437.40 83.96 o 13 0 0 1033.14 1063.11 114.41 o 14 0 0 503.93 421.22 100.33 o -14 1 0 810.29 682.83 150.75 o -13 1 0 293.37 298.26 290.42 o -12 1 0 1370.14 1439.92 109.60 o -11 1 0 19.92 215.84 78.19 o -10 1 0 846.64 1007.24 217.26 o -9 1 0 1381.39 1283.84 164.06 o -8 1 0 1166.80 1327.15 90.76 o -7 1 0 1344.35 1427.90 85.84 o -6 1 0 1914.54 1743.31 85.84 o -5 1 0 1446.90 1368.45 84.24 o -4 1 0 6759.74 6941.10 181.12 o -3 1 0 1107.90 1049.90 51.09 o -2 1 0 2601.95 2930.83 124.15 o -1 1 0 3482.92 4442.81 159.62 o 0 1 0 22534.88 0.00 8.87 o 2 1 0 20698.47 18369.80 571.98 o 3 1 0 761.73 1008.63 42.24 o 4 1 0 13923.19 16486.84 296.32 o 5 1 0 50.52 120.28 32.53 o 6 1 0 5610.63 5716.14 131.40 o 7 1 0 14846.73 14360.34 280.34 o 8 1 0 12985.49 13600.35 292.28 o 9 1 0 19257.25 21382.33 408.61 o 10 1 0 4711.94 5347.00 192.80 o 11 1 0 4.90 31.04 68.02 o 12 1 0 611.77 677.85 168.49 o 13 1 0 238.03 458.78 89.47 o 14 1 0 58.22 79.81 124.15 o 15 1 0 693.57 629.62 150.75 o -14 2 0 707.59 842.45 168.49 o -13 2 0 1352.96 1254.80 168.49 o -12 2 0 1306.92 1254.56 108.13 o -11 2 0 393.06 299.29 81.52 o -10 2 0 4.73 54.15 261.60 o -9 2 0 1350.78 1347.65 100.18 o -8 2 0 539.92 640.77 75.25 o -7 2 0 6.99 28.82 53.30 o -6 2 0 156.56 8.10 86.46 o -5 2 0 9024.66 10362.99 532.07 o -4 2 0 5861.55 5627.73 120.95 o -3 2 0 43.75 121.93 28.69 o -2 2 0 8575.37 9541.73 305.94 o -1 2 0 5116.83 5340.50 288.21 o 0 2 0 1531.75 1272.54 62.08 o 1 2 0 39129.04 34212.86 1853.39 o 2 2 0 7573.31 7098.73 221.70 o 3 2 0 5179.68 5385.72 166.27 o 4 2 0 3.94 73.81 26.51 o 5 2 0 43.38 7.95 25.91 o 6 2 0 1162.14 1345.92 54.98 o 7 2 0 4553.74 4261.83 152.39 o 8 2 0 3271.50 3139.65 97.49 o 9 2 0 23612.96 24322.85 460.25 o 10 2 0 7421.12 8073.87 193.23 o 11 2 0 2684.27 2953.15 152.97 o 12 2 0 120.74 42.73 68.12 o 13 2 0 0.11 66.51 119.72 o 14 2 0 91.39 0.00 119.72 o 15 2 0 350.63 336.98 146.32 o -13 3 0 1144.18 1396.69 177.36 o -12 3 0 354.46 354.71 119.72 o -11 3 0 2472.75 2873.19 226.13 o -10 3 0 1238.50 1101.97 119.72 o -9 3 0 593.56 696.47 87.62 o -8 3 0 781.68 1012.91 95.33 o -7 3 0 6517.30 6044.25 192.50 o -6 3 0 3277.94 3160.23 122.39 o -5 3 0 26928.20 29266.65 515.45 o -4 3 0 20715.40 23289.88 412.59 o -3 3 0 7849.01 8001.45 198.03 o -2 3 0 363.91 421.32 40.40 o -1 3 0 1661.62 1695.41 68.73 o 0 3 0 1.40 48.21 70.94 o 1 3 0 92.99 44.00 20.20 o 2 3 0 18758.12 19939.42 580.85 o 3 3 0 2122.23 2518.48 110.85 o 4 3 0 1166.26 943.62 57.64 o 5 3 0 613.99 816.75 44.74 o 6 3 0 8263.28 8226.48 203.72 o 7 3 0 6284.10 6180.48 142.78 o 8 3 0 2619.43 2306.69 95.35 o 9 3 0 5454.68 5581.77 200.79 o 10 3 0 3705.37 3667.15 118.33 o 11 3 0 285.73 245.64 76.70 o 12 3 0 290.89 274.90 115.28 o 13 3 0 229.65 323.68 124.15 o 14 3 0 516.66 700.56 164.06 o 15 3 0 105.40 168.49 150.75 o -13 4 0 222.89 101.98 141.89 o -12 4 0 126.70 124.15 124.15 o -11 4 0 698.64 616.32 133.02 o -10 4 0 130.19 177.36 110.85 o -9 4 0 879.92 867.15 110.85 o -8 4 0 67.31 107.86 106.41 o -7 4 0 225.42 188.66 62.47 o -6 4 0 4547.41 4839.36 124.59 o -5 4 0 3125.20 3026.65 90.06 o -4 4 0 37913.16 40171.39 858.55 o -3 4 0 26188.20 27525.02 598.45 o -2 4 0 7419.72 6367.28 167.92 o -1 4 0 4947.14 5002.52 136.99 o 0 4 0 5640.25 6328.97 334.76 o 1 4 0 3099.61 3693.05 101.86 o 2 4 0 19854.58 23293.93 494.90 o 3 4 0 3196.45 3001.78 133.02 o 4 4 0 4130.10 5023.65 190.66 o 5 4 0 16291.54 18960.81 598.58 o 6 4 0 1616.97 1662.14 135.24 o 7 4 0 86.18 154.01 39.10 o 8 4 0 4339.32 3827.51 108.42 o 9 4 0 1320.43 1516.65 72.17 o 10 4 0 4602.55 4659.99 134.59 o 11 4 0 5.45 54.86 66.05 o 12 4 0 74.24 106.41 110.85 o 13 4 0 379.81 345.85 124.15 o 14 4 0 985.11 1161.69 181.79 o 15 4 0 1239.10 1441.03 186.23 o -12 5 0 188.82 106.41 124.15 o -11 5 0 432.60 447.83 128.58 o -10 5 0 103.55 31.04 106.41 o -9 5 0 7.45 101.98 97.55 o -8 5 0 247.11 181.79 115.28 o -7 5 0 1749.40 1398.11 141.89 o -6 5 0 105.23 166.52 55.40 o -5 5 0 1325.96 1208.57 74.49 o -4 5 0 869.15 530.08 66.51 o -3 5 0 307.98 262.46 46.73 o -2 5 0 16646.67 16957.11 917.82 o -1 5 0 2981.34 2978.98 101.57 o 0 5 0 621.45 624.74 47.03 o 1 5 0 85.87 37.69 28.22 o 2 5 0 11591.54 11825.31 269.63 o 3 5 0 16836.83 18081.46 395.01 o 4 5 0 39282.47 42982.59 1232.63 o 5 5 0 37857.77 42202.22 1219.33 o 6 5 0 19505.95 21327.24 660.66 o 7 5 0 2142.85 2266.20 128.58 o 8 5 0 47.68 36.10 44.34 o 9 5 0 618.39 598.94 75.62 o 10 5 0 1727.19 1627.55 105.36 o 11 5 0 1052.44 1053.03 99.76 o 12 5 0 1527.23 1569.61 168.49 o 13 5 0 0.93 119.72 128.58 o 14 5 0 10.00 31.04 124.15 o 15 5 0 1574.42 1879.99 217.26 o -12 6 0 74.76 62.08 146.32 o -11 6 0 19.80 0.00 124.15 o -10 6 0 76.31 13.30 106.41 o -9 6 0 285.62 203.96 115.28 o -8 6 0 142.75 146.32 106.41 o -7 6 0 0.44 0.00 79.81 o -6 6 0 1217.05 1324.22 85.13 o -5 6 0 286.02 194.16 58.59 o -4 6 0 862.22 991.33 121.93 o -3 6 0 498.78 349.13 49.00 o -2 6 0 513.35 679.81 155.19 o -1 6 0 1.55 0.00 39.10 o 0 6 0 243.63 214.31 37.62 o 1 6 0 189.98 184.29 50.99 o 2 6 0 69.27 111.62 31.04 o 3 6 0 10170.16 9990.85 233.18 o 4 6 0 6589.51 6974.58 261.60 o 5 6 0 7203.03 6841.57 261.60 o 6 6 0 15532.12 15744.91 514.34 o 7 6 0 2405.63 2389.89 141.89 o 8 6 0 6142.20 6358.27 270.47 o 9 6 0 393.26 235.66 63.85 o 10 6 0 2.22 0.00 119.72 o 11 6 0 1325.14 1230.02 102.19 o 12 6 0 1488.30 1768.34 117.17 o 13 6 0 2822.62 2682.53 226.13 o 14 6 0 1066.60 1143.96 181.79 o 15 6 0 11.09 0.00 133.02 o -11 7 0 1116.27 1210.46 181.79 o -10 7 0 798.90 895.66 155.19 o -9 7 0 1121.41 997.64 155.19 o -8 7 0 440.68 656.22 133.02 o -7 7 0 112.37 141.89 101.98 o -6 7 0 765.57 757.29 79.55 o -5 7 0 146.42 185.88 59.64 o -4 7 0 206.18 215.31 55.40 o -3 7 0 2901.27 3046.70 122.39 o -2 7 0 140.82 177.85 66.51 o -1 7 0 579.35 676.64 57.94 o 0 7 0 1078.32 899.88 61.08 o 1 7 0 16.24 38.66 39.10 o 2 7 0 2039.57 2394.24 104.20 o 3 7 0 1697.83 1731.86 68.02 o 4 7 0 1554.93 1888.86 124.15 o 5 7 0 4710.13 4770.92 212.83 o 6 7 0 115.11 133.02 62.08 o 7 7 0 37.37 39.91 66.51 o 8 7 0 27.13 0.00 75.38 o 9 7 0 0.64 35.47 79.81 o 10 7 0 68.09 71.44 69.25 o 11 7 0 702.34 917.41 93.75 o 12 7 0 1027.09 898.96 146.32 o 13 7 0 1747.61 1857.82 195.09 o 14 7 0 622.71 638.49 150.75 o 15 7 0 828.37 917.83 172.92 o -10 8 0 218.24 261.60 133.02 o -9 8 0 985.73 922.26 155.19 o -8 8 0 517.10 789.24 141.89 o -7 8 0 870.48 860.18 141.89 o -6 8 0 69.46 212.83 101.98 o -5 8 0 300.43 389.40 68.02 o -4 8 0 31.65 14.10 59.64 o -3 8 0 22.61 17.74 54.80 o -2 8 0 2652.23 2319.66 110.48 o -1 8 0 7403.05 7011.53 441.18 o 0 8 0 763.46 863.97 115.28 o 1 8 0 3724.53 3691.99 130.09 o 2 8 0 259.67 291.45 46.72 o 3 8 0 742.64 773.11 51.65 o 4 8 0 1238.43 1169.31 73.16 o 5 8 0 3473.23 3578.19 190.66 o 6 8 0 252.76 261.60 84.24 o 7 8 0 164.02 137.45 75.38 o 8 8 0 255.91 150.75 88.68 o 9 8 0 5.19 66.51 79.81 o 10 8 0 1060.45 1183.86 128.58 o 11 8 0 45.27 111.21 75.62 o 12 8 0 3001.62 3070.54 303.72 o 13 8 0 1455.83 1339.05 177.36 o 14 8 0 611.97 629.62 168.49 o 15 8 0 434.60 571.98 164.06 o -9 9 0 130.08 203.96 128.58 o -8 9 0 0.79 0.00 110.85 o -7 9 0 1.04 0.00 119.72 o -6 9 0 3.70 0.00 110.85 o -5 9 0 245.12 282.72 64.77 o -4 9 0 106.00 0.00 62.85 o -3 9 0 3151.81 3350.92 142.59 o -2 9 0 389.04 362.09 62.47 o -1 9 0 2037.36 1903.06 100.18 o 0 9 0 4325.06 3902.85 145.56 o 1 9 0 4588.99 4304.94 215.05 o 2 9 0 7105.40 6830.36 254.95 o 3 9 0 9350.02 10051.17 258.30 o 4 9 0 77.65 195.09 75.38 o 5 9 0 3.13 0.00 70.94 o 6 9 0 1932.37 1866.69 146.32 o 7 9 0 1322.97 1520.84 137.45 o 8 9 0 2435.04 2168.20 164.06 o 9 9 0 8.04 0.00 88.68 o 10 9 0 674.19 532.07 106.41 o 11 9 0 982.77 1086.13 102.89 o 12 9 0 883.29 904.51 104.16 o 13 9 0 1153.19 1245.48 116.79 o 14 9 0 1979.11 2283.48 226.13 o -8 10 0 39.93 88.68 124.15 o -7 10 0 623.58 744.90 150.75 o -6 10 0 174.10 84.24 119.72 o -5 10 0 184.68 153.47 67.07 o -4 10 0 24.95 74.84 63.76 o -3 10 0 668.62 608.73 75.62 o -2 10 0 678.37 758.71 85.84 o -1 10 0 1.30 31.53 56.17 o 0 10 0 1463.81 1216.43 87.62 o 1 10 0 567.95 633.77 82.03 o 2 10 0 2113.26 2168.36 106.05 o 3 10 0 1117.65 1270.85 76.70 o 4 10 0 3089.12 2678.10 172.92 o 5 10 0 364.89 257.17 84.24 o 6 10 0 356.04 394.62 93.11 o 7 10 0 31.39 0.00 84.24 o 8 10 0 2846.76 3276.68 212.83 o 9 10 0 1811.62 1742.54 164.06 o 10 10 0 3069.10 2948.57 203.96 o 11 10 0 1321.86 1326.76 141.89 o 12 10 0 453.55 443.56 91.50 o 13 10 0 76.83 0.00 87.79 o 14 10 0 612.61 811.41 181.79 o -7 11 0 3.40 39.91 128.58 o -6 11 0 131.15 0.00 128.58 o -5 11 0 179.75 177.36 115.28 o -4 11 0 12.37 0.00 68.76 o -3 11 0 347.00 321.58 71.26 o -2 11 0 238.38 141.89 65.84 o -1 11 0 53.60 24.83 106.41 o 0 11 0 399.92 339.02 67.35 o 1 11 0 1712.31 1784.78 126.37 o 2 11 0 1219.02 1192.73 128.58 o 3 11 0 1109.86 1064.15 124.15 o 4 11 0 16.70 0.00 79.81 o 5 11 0 174.59 195.09 84.24 o 6 11 0 915.77 957.73 124.15 o 7 11 0 111.98 226.13 93.11 o 8 11 0 54.95 0.00 88.68 o 9 11 0 585.37 585.28 115.28 o 10 11 0 374.12 270.47 106.41 o 11 11 0 746.18 753.81 100.99 o 12 11 0 1177.99 1173.44 120.43 o 13 11 0 391.86 548.18 109.60 o -6 12 0 593.92 549.81 164.06 o -5 12 0 1557.86 1538.58 195.09 o -4 12 0 356.76 332.87 84.14 o -3 12 0 69.17 51.19 68.12 o -2 12 0 19.32 64.34 70.49 o -1 12 0 30.80 55.71 71.91 o 0 12 0 8.54 0.00 64.77 o 1 12 0 1536.27 1321.31 141.89 o 2 12 0 382.92 478.87 106.41 o 3 12 0 2.37 0.00 84.24 o 4 12 0 1219.10 1055.28 128.58 o 5 12 0 1083.03 1228.20 137.45 o 6 12 0 241.90 181.79 101.98 o 7 12 0 222.16 208.40 106.41 o 8 12 0 3.89 0.00 97.55 o 9 12 0 401.61 456.70 119.72 o 10 12 0 2.56 70.94 115.28 o 11 12 0 0.18 0.00 119.72 o 12 12 0 12.99 117.36 104.20 o 13 12 0 10.53 60.92 99.00 o -5 13 0 187.69 155.19 150.75 o -4 13 0 411.30 319.24 133.02 o -3 13 0 395.06 487.93 135.24 o -2 13 0 169.00 90.65 83.96 o -1 13 0 612.21 546.87 108.63 o 0 13 0 5.10 0.00 88.68 o 1 13 0 29.23 97.55 97.55 o 2 13 0 191.77 57.64 101.98 o 3 13 0 51.88 88.68 88.68 o 4 13 0 28.81 0.00 88.68 o 5 13 0 85.92 115.28 97.55 o 6 13 0 251.57 124.15 106.41 o 7 13 0 144.63 115.28 106.41 o 8 13 0 468.39 412.36 119.72 o 9 13 0 290.20 274.90 110.85 o 10 13 0 174.47 230.56 110.85 o 11 13 0 24.39 79.81 124.15 o 12 13 0 23.26 103.05 96.59 o -3 14 0 60.82 0.00 86.06 o -2 14 0 142.99 88.68 97.55 o -1 14 0 1.01 0.00 97.55 o 0 14 0 316.28 274.90 106.41 o 1 14 0 441.14 235.00 106.41 o 2 14 0 21.84 0.00 93.11 o 3 14 0 1.11 0.00 106.41 o 4 14 0 500.69 558.68 124.15 o 5 14 0 605.74 806.98 133.02 o 6 14 0 754.35 886.79 141.89 o 7 14 0 915.76 1228.20 164.06 o 8 14 0 694.50 1068.58 164.06 o 9 14 0 196.71 150.75 128.58 o 10 14 0 6.05 26.60 119.72 o 11 14 0 41.96 61.57 93.75 o -1 15 0 676.85 598.58 141.89 o 0 15 0 257.10 554.24 133.02 o 1 15 0 180.00 168.49 124.15 o 2 15 0 7.57 0.00 97.55 o 3 15 0 41.72 35.47 106.41 o 4 15 0 3.53 0.00 101.98 o 5 15 0 3.57 0.00 101.98 o 6 15 0 75.36 35.47 115.28 o 7 15 0 3.75 57.64 115.28 o 8 15 0 180.34 336.98 124.15 o 9 15 0 374.37 514.34 137.45 o 4 16 0 11.42 0.00 110.85 o 5 16 0 10.79 0.00 115.28 o -8 -15 1 633.60 638.49 159.62 o -7 -15 1 617.96 571.98 141.89 o -6 -15 1 137.38 199.53 128.58 o -5 -15 1 258.30 159.62 115.28 o -4 -15 1 0.22 0.00 106.41 o -3 -15 1 9.36 0.00 110.85 o -2 -15 1 51.00 0.00 106.41 o -1 -15 1 67.69 88.68 115.28 o 0 -15 1 7.96 0.00 119.72 o -10 -14 1 839.98 983.13 127.52 o -9 -14 1 298.55 461.39 128.58 o -8 -14 1 300.47 470.00 128.58 o -7 -14 1 2.21 39.91 110.85 o -6 -14 1 8.01 0.00 101.98 o -5 -14 1 16.01 57.64 106.41 o -4 -14 1 175.58 62.08 97.55 o -3 -14 1 81.13 17.74 110.85 o -2 -14 1 360.00 372.45 119.72 o -1 -14 1 352.32 314.81 110.85 o 1 -14 1 0.85 0.00 115.28 o 2 -14 1 19.09 0.00 110.85 o -11 -13 1 700.21 642.16 119.22 o -10 -13 1 1359.44 1454.19 266.04 o -9 -13 1 1476.47 1343.48 164.06 o -8 -13 1 1518.42 1445.46 168.49 o -7 -13 1 282.77 181.79 106.41 o -6 -13 1 2.70 0.00 93.11 o -5 -13 1 595.95 496.60 119.72 o -4 -13 1 1182.91 1378.95 150.75 o -3 -13 1 3417.92 3223.47 221.70 o -2 -13 1 892.31 953.30 133.02 o -1 -13 1 622.69 922.26 133.02 o 0 -13 1 258.70 97.55 97.55 o 1 -13 1 2.52 110.85 97.55 o 2 -13 1 72.37 124.58 77.71 o 3 -13 1 246.60 248.30 83.10 o 4 -13 1 3.25 0.00 88.36 o -12 -12 1 1292.65 1174.14 129.86 o -11 -12 1 247.32 422.53 95.84 o -10 -12 1 0.67 0.00 80.93 o -9 -12 1 345.76 235.00 110.85 o -8 -12 1 22.01 0.00 101.98 o -7 -12 1 289.87 532.07 124.15 o -6 -12 1 300.64 164.06 97.55 o -5 -12 1 360.06 341.41 101.98 o -4 -12 1 89.51 110.85 101.98 o -3 -12 1 1978.83 1596.22 155.19 o -2 -12 1 3458.35 3219.04 208.40 o -1 -12 1 5765.11 5901.57 292.64 o 0 -12 1 2098.57 2274.61 181.79 o 1 -12 1 1142.55 1454.33 155.19 o 2 -12 1 1.62 0.00 69.25 o 3 -12 1 284.55 135.89 77.71 o 4 -12 1 579.21 355.90 87.35 o 5 -12 1 831.06 994.53 108.64 o 6 -12 1 761.87 758.20 168.49 o -13 -11 1 555.34 468.90 113.07 o -12 -11 1 457.33 464.97 110.79 o -11 -11 1 730.48 715.36 98.00 o -10 -11 1 425.35 523.78 95.33 o -9 -11 1 31.82 0.00 88.68 o -8 -11 1 8.86 0.00 88.68 o -7 -11 1 8.72 44.34 97.55 o -6 -11 1 233.82 181.79 88.68 o -5 -11 1 808.31 682.83 115.28 o -4 -11 1 260.54 26.60 88.68 o -3 -11 1 85.96 212.83 88.68 o -2 -11 1 69.25 53.21 93.11 o -1 -11 1 509.37 440.57 68.98 o 0 -11 1 2325.41 2369.09 170.71 o 1 -11 1 1189.06 1354.80 105.00 o 2 -11 1 5.77 26.91 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