# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' osada10 in P1- 2003/05/26 18:50:10 037 KENX' _shelx_refln_list_code 4 _shelx_F_calc_maximum 311.42 _exptl_crystal_F_000 896.00 _reflns_d_resolution_high 0.7497 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 10.2302 _cell_length_b 13.4229 _cell_length_c 13.6086 _cell_angle_alpha 62.287 _cell_angle_beta 83.403 _cell_angle_gamma 68.990 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 15083.64 16929.67 728.24 o 2 0 0 27898.23 32721.54 1373.57 o 3 0 0 8572.89 9466.65 369.57 o 4 0 0 670.21 726.93 18.42 o 5 0 0 401.97 394.79 16.35 o 6 0 0 2796.92 2702.40 72.40 o 7 0 0 1381.81 1407.66 41.12 o 8 0 0 3289.38 3567.78 244.18 o 9 0 0 2464.52 2489.91 79.78 o 10 0 0 1497.68 1688.83 108.67 o 11 0 0 1154.19 1091.10 81.99 o 12 0 0 352.53 483.43 62.22 o -12 1 0 453.81 541.57 68.11 o -11 1 0 438.95 428.15 57.47 o -10 1 0 489.59 509.92 56.16 o -9 1 0 43.61 64.73 28.14 o -8 1 0 178.75 162.25 16.32 o -7 1 0 1699.82 1733.91 83.93 o -6 1 0 2431.53 2548.71 54.76 o -5 1 0 3184.07 3232.56 68.23 o -4 1 0 14524.00 14970.14 327.53 o -3 1 0 6334.69 6898.49 122.95 o -2 1 0 21832.23 24782.39 430.06 o -1 1 0 6433.94 6942.25 107.51 o 0 1 0 7678.80 6913.33 947.35 o 1 1 0 1064.93 1188.42 64.07 o 2 1 0 697.16 720.51 21.30 o 3 1 0 22.27 58.37 6.75 o 4 1 0 1353.63 1691.13 51.76 o 5 1 0 5600.80 6431.64 263.97 o 6 1 0 3280.62 3701.43 142.16 o 7 1 0 5438.57 5400.83 141.89 o 8 1 0 3832.04 3624.57 113.51 o 9 1 0 755.58 710.31 38.07 o 10 1 0 773.03 683.67 41.48 o 11 1 0 45.65 64.66 21.36 o 12 1 0 0.17 -14.01 23.62 o -11 2 0 0.56 3.27 26.99 o -10 2 0 3.27 18.12 27.02 o -9 2 0 172.21 188.42 38.81 o -8 2 0 1091.15 1086.83 46.17 o -7 2 0 4547.75 4696.02 90.19 o -6 2 0 7436.16 7600.73 301.75 o -5 2 0 6932.29 6830.10 128.86 o -4 2 0 7539.70 7371.78 196.13 o -3 2 0 3797.08 3509.71 92.09 o -2 2 0 1057.44 983.13 38.22 o -1 2 0 1671.71 1506.77 80.32 o 0 2 0 29.86 31.26 4.01 o 1 2 0 5886.73 6898.40 256.54 o 2 2 0 305.60 304.14 16.70 o 3 2 0 15722.66 17067.51 231.28 o 4 2 0 10125.19 9825.30 258.28 o 5 2 0 11412.00 10682.86 356.48 o 6 2 0 8036.77 7587.78 247.30 o 7 2 0 2903.67 2804.50 58.86 o 8 2 0 1792.40 1833.20 67.08 o 9 2 0 56.42 88.04 17.90 o 10 2 0 113.84 108.80 21.26 o 11 2 0 677.14 707.32 44.42 o 12 2 0 824.10 835.53 50.88 o 13 2 0 214.75 224.48 50.21 o -11 3 0 252.58 267.60 52.90 o -10 3 0 725.02 707.75 70.54 o -9 3 0 1727.64 1640.36 95.33 o -8 3 0 1643.01 1628.72 57.58 o -7 3 0 5922.61 5848.63 100.24 o -6 3 0 588.97 573.02 31.54 o -5 3 0 1537.37 1571.88 33.44 o -4 3 0 652.37 760.21 21.36 o -3 3 0 4480.30 4275.55 44.97 o -2 3 0 4426.05 4657.88 184.69 o -1 3 0 26060.29 26009.15 237.78 o 0 3 0 5086.26 5208.73 220.82 o 1 3 0 86006.69 87371.10 3682.02 o 2 3 0 18122.76 16595.44 748.48 o 3 3 0 826.73 710.76 37.77 o 4 3 0 12055.04 12163.53 288.36 o 5 3 0 80.38 100.99 8.28 o 6 3 0 19.02 58.64 7.43 o 7 3 0 452.56 383.05 24.51 o 8 3 0 1266.32 1225.27 87.10 o 9 3 0 2340.64 2316.92 63.15 o 10 3 0 2148.25 2026.31 63.83 o 11 3 0 2035.02 2063.10 70.04 o 12 3 0 469.55 483.82 40.30 o 13 3 0 200.12 240.05 34.28 o -10 4 0 321.46 281.28 52.21 o -9 4 0 497.01 526.69 39.98 o -8 4 0 212.45 200.94 26.34 o -7 4 0 29.09 47.41 16.94 o -6 4 0 28.14 28.36 13.94 o -5 4 0 1367.85 1305.75 46.91 o -4 4 0 341.59 340.08 12.78 o -3 4 0 3617.70 3808.84 119.36 o -2 4 0 4830.38 5388.72 460.47 o -1 4 0 6961.15 7428.36 79.46 o 0 4 0 3498.29 3799.86 176.99 o 1 4 0 12355.40 14277.60 745.06 o 2 4 0 5496.00 6643.61 268.53 o 3 4 0 3322.01 3755.97 201.02 o 4 4 0 1389.53 1120.42 66.06 o 5 4 0 2263.79 2548.38 49.44 o 6 4 0 3190.25 3516.90 57.88 o 7 4 0 3588.88 3654.02 222.34 o 8 4 0 2864.24 2784.91 63.98 o 9 4 0 3917.15 3870.40 81.55 o 10 4 0 1005.99 1002.84 46.52 o 11 4 0 385.59 404.25 35.49 o 12 4 0 129.00 129.03 26.11 o 13 4 0 5.30 14.65 21.13 o -10 5 0 13.12 24.58 29.28 o -9 5 0 22.58 26.18 18.72 o -8 5 0 123.80 126.40 24.32 o -7 5 0 833.71 823.75 45.32 o -6 5 0 3195.89 3075.96 77.66 o -5 5 0 3569.75 3550.32 79.19 o -4 5 0 5768.19 5678.43 93.71 o -3 5 0 5620.98 5989.52 90.49 o -2 5 0 3437.66 3635.65 65.95 o -1 5 0 995.46 973.32 32.79 o 0 5 0 25.23 18.56 4.37 o 1 5 0 3257.23 3936.01 176.57 o 2 5 0 970.48 979.65 40.18 o 3 5 0 12827.56 13233.53 577.75 o 4 5 0 9490.81 10622.12 601.80 o 5 5 0 13069.87 11792.90 532.78 o 6 5 0 4613.59 4291.48 174.68 o 7 5 0 7074.94 6489.44 784.40 o 8 5 0 1683.76 1615.44 50.59 o 9 5 0 337.79 345.72 31.30 o 10 5 0 52.56 60.08 18.70 o 11 5 0 110.27 109.60 22.94 o 12 5 0 167.46 171.39 36.63 o 13 5 0 333.55 368.29 40.03 o -9 6 0 245.27 294.54 35.58 o -8 6 0 1331.20 1372.56 62.90 o -7 6 0 399.43 433.45 36.14 o -6 6 0 2099.73 2118.64 69.19 o -5 6 0 1159.55 1082.86 48.06 o -4 6 0 17.26 20.78 12.81 o -3 6 0 476.20 415.16 28.45 o -2 6 0 707.15 739.25 33.63 o -1 6 0 3117.51 3260.78 64.17 o 0 6 0 4990.08 5483.32 261.15 o 1 6 0 12273.85 13198.60 653.42 o 2 6 0 13053.00 14214.17 598.16 o 3 6 0 10313.46 10184.79 397.80 o 4 6 0 2334.00 2187.30 86.39 o 5 6 0 2880.34 2741.89 185.10 o 6 6 0 260.15 216.55 20.21 o 7 6 0 3.55 -1.29 10.07 o 8 6 0 238.69 232.41 24.45 o 9 6 0 290.85 285.27 27.81 o 10 6 0 1440.92 1244.93 66.17 o 11 6 0 437.84 422.87 45.79 o 12 6 0 762.50 740.18 48.30 o 13 6 0 421.27 403.79 41.43 o -9 7 0 340.40 349.28 41.21 o -8 7 0 233.05 232.79 32.65 o -7 7 0 221.79 242.62 31.46 o -6 7 0 17.15 27.48 18.31 o -5 7 0 46.90 40.69 17.18 o -4 7 0 244.79 227.08 26.79 o -3 7 0 394.17 311.26 27.97 o -2 7 0 1739.18 1552.67 78.43 o -1 7 0 6236.36 5936.51 92.64 o 0 7 0 8347.13 8396.36 208.14 o 1 7 0 5273.69 5616.12 222.89 o 2 7 0 8746.47 9288.12 383.28 o 3 7 0 1740.66 1770.04 123.94 o 4 7 0 59.10 47.82 8.17 o 5 7 0 94.06 82.39 9.64 o 6 7 0 2159.10 1864.29 50.82 o 7 7 0 392.36 428.98 30.57 o 8 7 0 4060.85 4222.97 118.94 o 9 7 0 1256.57 1231.52 49.95 o 10 7 0 2199.21 2212.16 70.07 o 11 7 0 987.66 938.12 50.55 o 12 7 0 243.76 266.37 33.30 o 13 7 0 192.84 194.00 46.38 o -8 8 0 16.76 16.23 20.66 o -7 8 0 178.86 178.45 30.74 o -6 8 0 590.79 599.04 44.79 o -5 8 0 1681.65 1637.90 65.24 o -4 8 0 1888.14 1923.99 67.25 o -3 8 0 1814.40 1874.35 63.58 o -2 8 0 3462.74 3636.53 82.55 o -1 8 0 1020.88 907.96 40.93 o 0 8 0 914.32 827.76 37.00 o 1 8 0 4.66 4.07 8.29 o 2 8 0 596.76 625.38 22.20 o 3 8 0 130.53 127.89 12.52 o 4 8 0 3059.50 2945.06 126.22 o 5 8 0 2012.25 1889.36 110.79 o 6 8 0 5487.39 5595.67 328.43 o 7 8 0 2310.99 2228.27 69.29 o 8 8 0 2233.96 2198.19 132.50 o 9 8 0 1320.05 1187.82 51.26 o 10 8 0 56.84 49.46 19.80 o 11 8 0 23.11 35.35 19.81 o 12 8 0 50.81 35.16 21.16 o 13 8 0 138.06 126.28 39.93 o -7 9 0 493.97 524.55 45.94 o -6 9 0 502.77 537.98 44.34 o -5 9 0 630.07 604.21 44.92 o -4 9 0 1541.84 1498.87 63.82 o -3 9 0 125.84 127.58 23.44 o -2 9 0 211.49 204.20 25.91 o -1 9 0 110.07 98.04 19.94 o 0 9 0 494.22 452.98 31.77 o 1 9 0 875.93 781.69 48.57 o 2 9 0 3605.55 3652.10 83.92 o 3 9 0 3069.40 3131.10 185.44 o 4 9 0 1709.85 1599.07 74.60 o 5 9 0 1152.30 1131.34 66.60 o 6 9 0 1013.48 949.17 58.07 o 7 9 0 203.75 188.07 27.16 o 8 9 0 219.14 200.13 25.23 o 9 9 0 49.29 48.40 18.69 o 10 9 0 64.86 52.52 20.06 o 11 9 0 710.28 645.35 44.93 o 12 9 0 346.31 333.79 36.84 o -6 10 0 138.04 151.88 31.22 o -5 10 0 53.36 71.00 23.66 o -4 10 0 18.08 11.66 18.39 o -3 10 0 60.35 57.97 21.86 o -2 10 0 561.08 541.66 39.84 o -1 10 0 1819.64 1695.87 61.73 o 0 10 0 2060.49 1976.09 63.61 o 1 10 0 3610.87 3603.60 81.37 o 2 10 0 2171.06 2162.81 61.55 o 3 10 0 2603.20 2712.77 88.06 o 4 10 0 555.68 533.97 30.14 o 5 10 0 189.53 144.02 20.45 o 6 10 0 85.35 94.15 19.05 o 7 10 0 1050.29 1106.45 48.60 o 8 10 0 411.14 434.62 35.30 o 9 10 0 1691.73 1636.34 62.72 o 10 10 0 1358.64 1416.64 79.03 o 11 10 0 699.06 653.54 51.16 o 12 10 0 552.10 520.29 45.42 o -5 11 0 244.42 266.79 36.24 o -4 11 0 411.99 439.84 42.43 o -3 11 0 943.27 1032.34 57.49 o -2 11 0 434.20 458.55 38.76 o -1 11 0 847.14 880.09 65.13 o 0 11 0 168.77 161.89 25.12 o 1 11 0 586.38 567.69 37.39 o 2 11 0 211.32 210.08 25.99 o 3 11 0 353.48 425.44 32.52 o 4 11 0 89.31 96.72 17.90 o 5 11 0 1278.32 1336.51 80.59 o 6 11 0 1041.81 1136.65 104.21 o 7 11 0 1521.08 1535.69 83.55 o 8 11 0 1367.19 1384.91 93.44 o 9 11 0 615.62 639.26 44.16 o 10 11 0 401.42 444.67 40.23 o 11 11 0 53.83 80.92 25.28 o 12 11 0 9.41 16.70 27.87 o -3 12 0 356.85 407.72 41.71 o -2 12 0 65.60 92.82 25.27 o -1 12 0 14.16 15.28 18.02 o 0 12 0 6.68 11.67 16.52 o 1 12 0 11.00 17.63 16.77 o 2 12 0 389.69 368.20 33.44 o 3 12 0 1043.92 958.25 47.24 o 4 12 0 1375.59 1327.91 86.93 o 5 12 0 987.85 917.04 72.67 o 6 12 0 1108.68 966.49 75.20 o 7 12 0 903.20 893.32 73.30 o 8 12 0 138.45 122.81 25.77 o 9 12 0 109.09 138.60 27.14 o 10 12 0 2.31 14.43 22.69 o 11 12 0 84.85 87.99 27.59 o -2 13 0 56.83 52.61 24.93 o -1 13 0 52.24 68.76 23.97 o 0 13 0 762.20 755.09 50.01 o 1 13 0 741.63 716.02 48.00 o 2 13 0 1148.63 1151.80 56.33 o 3 13 0 1151.12 1178.38 54.57 o 4 13 0 567.64 624.28 65.67 o 5 13 0 568.66 618.52 68.02 o 6 13 0 3.54 -1.21 25.32 o 7 13 0 1.91 5.34 25.35 o 8 13 0 75.29 52.36 31.03 o 9 13 0 378.26 416.91 56.62 o 10 13 0 248.07 253.07 36.40 o 0 14 0 283.74 303.74 37.74 o 1 14 0 431.17 453.12 42.38 o 2 14 0 82.99 106.25 25.59 o 3 14 0 151.77 195.29 45.72 o 4 14 0 1.63 -3.58 21.72 o 5 14 0 12.80 10.28 29.06 o 6 14 0 87.11 106.76 38.96 o 7 14 0 262.80 285.18 52.85 o 8 14 0 237.71 250.80 51.31 o 9 14 0 208.46 200.27 46.76 o 1 15 0 4.58 -5.98 24.76 o 2 15 0 1.30 -8.33 21.95 o 4 15 0 185.95 209.63 50.56 o 5 15 0 177.55 149.98 44.84 o -2 -15 1 164.55 172.71 41.77 o -8 -14 1 6.04 -16.58 26.59 o -7 -14 1 25.15 21.45 30.09 o -6 -14 1 43.83 53.60 36.18 o -5 -14 1 394.41 512.27 67.94 o -4 -14 1 224.71 205.96 50.15 o -3 -14 1 292.97 340.82 57.81 o -2 -14 1 499.96 537.83 44.16 o -1 -14 1 108.17 135.96 28.78 o 0 -14 1 221.08 232.43 46.68 o -9 -13 1 155.23 166.88 44.24 o -8 -13 1 167.93 161.73 44.42 o -7 -13 1 783.71 733.89 71.75 o -6 -13 1 543.99 585.36 67.69 o -5 -13 1 772.04 819.38 77.76 o -4 -13 1 1082.75 1005.72 83.15 o -3 -13 1 173.44 174.06 26.90 o -2 -13 1 227.79 217.00 29.71 o -1 -13 1 1.46 -9.05 16.00 o 0 -13 1 56.12 30.28 20.92 o 1 -13 1 183.84 209.82 33.46 o -11 -12 1 315.54 327.87 56.91 o -10 -12 1 281.54 376.22 40.18 o -9 -12 1 592.82 670.33 48.45 o -8 -12 1 490.13 451.15 58.94 o -7 -12 1 437.95 428.29 56.76 o -6 -12 1 547.43 497.14 59.91 o -5 -12 1 28.71 38.38 28.92 o -4 -12 1 16.54 26.20 28.95 o -3 -12 1 10.44 11.22 15.16 o -2 -12 1 390.06 387.42 34.77 o -1 -12 1 684.08 689.85 44.24 o 0 -12 1 451.29 501.48 40.53 o 1 -12 1 640.02 664.44 46.97 o 2 -12 1 250.51 247.27 33.66 o 3 -12 1 452.52 496.19 55.04 o -11 -11 1 430.62 466.43 43.36 o -10 -11 1 583.69 544.87 52.28 o -9 -11 1 467.12 471.51 75.94 o -8 -11 1 172.37 189.35 40.65 o -7 -11 1 128.40 115.21 23.01 o -6 -11 1 115.67 100.85 33.56 o -5 -11 1 429.17 337.72 49.06 o -4 -11 1 1020.96 941.21 44.79 o -3 -11 1 3033.83 2964.63 76.57 o -2 -11 1 564.82 500.42 69.05 o -1 -11 1 2006.92 1953.55 66.14 o 0 -11 1 164.02 144.13 24.46 o 1 -11 1 655.87 661.52 44.30 o 2 -11 1 155.38 175.70 28.88 o 3 -11 1 50.18 58.19 22.45 o 4 -11 1 0.64 18.33 19.03 o -12 -10 1 221.95 231.14 49.32 o -11 -10 1 155.84 176.27 30.00 o -10 -10 1 1.12 1.16 17.52 o -9 -10 1 0.66 -0.27 15.61 o -8 -10 1 767.50 809.32 45.74 o -7 -10 1 1349.04 1433.55 110.44 o -6 -10 1 1402.36 1480.82 100.81 o -5 -10 1 3060.64 3329.91 255.86 o -4 -10 1 2486.88 2415.18 100.60 o -3 -10 1 3794.96 3761.98 131.91 o -2 -10 1 353.01 350.98 28.97 o -1 -10 1 128.85 112.91 25.01 o 0 -10 1 109.12 123.10 21.94 o 1 -10 1 97.68 117.84 22.44 o 2 -10 1 241.21 243.61 29.59 o 3 -10 1 761.94 804.25 49.86 o 4 -10 1 643.67 627.74 45.90 o 5 -10 1 461.50 494.97 47.88 o -12 -9 1 21.99 21.05 21.13 o -11 -9 1 48.76 70.95 23.71 o -10 -9 1 524.39 528.41 41.00 o -9 -9 1 981.69 969.22 49.66 o -8 -9 1 903.06 892.38 45.70 o -7 -9 1 1011.10 997.78 47.10 o -6 -9 1 1150.66 1228.73 47.79 o -5 -9 1 1128.47 1126.92 57.67 o -4 -9 1 914.46 902.77 34.07 o -3 -9 1 241.35 194.16 20.92 o -2 -9 1 2.81 6.12 10.82 o -1 -9 1 190.08 174.38 21.60 o 0 -9 1 1211.77 1182.70 48.77 o 1 -9 1 844.38 779.48 41.32 o 2 -9 1 2150.99 2200.75 70.42 o 3 -9 1 1183.40 1049.68 51.81 o 4 -9 1 789.93 812.68 49.11 o 5 -9 1 546.73 556.27 44.06 o 6 -9 1 10.88 3.06 17.25 o -13 -8 1 203.58 215.84 47.96 o -12 -8 1 409.30 419.06 40.83 o -11 -8 1 957.36 996.90 54.12 o -10 -8 1 1961.16 1920.56 85.59 o -9 -8 1 859.86 890.68 46.22 o -8 -8 1 1535.35 1773.09 62.67 o -7 -8 1 87.76 91.05 18.01 o -6 -8 1 180.81 191.86 22.40 o -5 -8 1 32.61 26.83 7.74 o -4 -8 1 2004.28 1747.78 82.71 o -3 -8 1 1865.97 1865.45 74.81 o -2 -8 1 6662.35 6719.06 171.50 o -1 -8 1 3296.23 2887.24 332.14 o 0 -8 1 6062.78 6151.27 98.95 o 1 -8 1 2984.99 3046.86 73.78 o 2 -8 1 1342.94 1341.53 52.32 o 3 -8 1 700.70 669.29 41.15 o 4 -8 1 2.12 0.65 14.77 o 5 -8 1 47.05 67.45 21.75 o 6 -8 1 467.47 489.15 40.65 o 7 -8 1 421.31 484.15 43.79 o 8 -8 1 580.05 688.20 70.23 o -13 -7 1 333.11 375.34 57.42 o -12 -7 1 615.50 655.86 46.77 o -11 -7 1 342.29 344.73 34.62 o -10 -7 1 364.08 350.35 32.62 o -9 -7 1 3.00 3.46 14.16 o -8 -7 1 191.18 194.38 23.27 o -7 -7 1 405.17 440.77 41.31 o -6 -7 1 5572.70 5664.07 129.38 o -5 -7 1 2122.56 2208.09 118.83 o -4 -7 1 9611.85 9698.47 517.37 o -3 -7 1 7637.03 8091.09 347.03 o -2 -7 1 6876.69 7351.82 287.81 o -1 -7 1 2529.62 2453.77 103.99 o 0 -7 1 444.87 392.45 25.87 o 1 -7 1 27.99 38.45 13.00 o 2 -7 1 393.67 408.16 29.73 o 3 -7 1 955.14 945.99 44.25 o 4 -7 1 903.56 804.38 43.94 o 5 -7 1 1368.67 1325.64 56.92 o 6 -7 1 1268.28 1265.95 62.62 o 7 -7 1 1008.27 1064.34 58.68 o 8 -7 1 524.77 591.88 46.93 o 9 -7 1 130.37 149.50 42.60 o -13 -6 1 57.20 78.59 37.22 o -12 -6 1 106.48 113.33 25.92 o -11 -6 1 4.53 -1.48 16.52 o -10 -6 1 285.00 275.91 30.31 o -9 -6 1 533.51 517.91 35.06 o -8 -6 1 1836.36 1655.15 63.69 o -7 -6 1 3479.47 3403.81 98.45 o -6 -6 1 3888.97 3349.15 66.43 o -5 -6 1 7272.70 6827.04 346.50 o -4 -6 1 1159.75 923.02 49.34 o -3 -6 1 3532.61 3161.11 133.81 o -2 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