Acta Cryst. (2003). E59, i112-i115  [ doi:10.1107/S1600536803014855 ]

Li_0.7NbS₂: structural effects of increased alkali metal content

P. A. Salyer, M. G. Barker, D. H. Gregory, M. O. Jones and C. Wilson

Online 17 July 2003

Key indicators

• Single-crystal X-ray study
• T = 150 K
• Mean (Nb-S) = 0.001 Å
• Disorder in solvent or counterion
• R factor = 0.016
• wR factor = 0.047
• Data-to-parameter ratio = 9.4

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level C:



CRYSC_01  Alert C There is an ordering error in _exptl_crystal_colour.          
          It should be (QUALIFIER) (INTENSITY) (BASE_COLOUR).                   

PLAT_302  Alert C Anion/Solvent Disorder .........................       3.00 Perc.


 0 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 2 Alert Level C = Please check

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