(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]

Acta Cryst. (2003). E59, m633-m635 [ doi:10.1107/S1600536803015691 ]

(Acetylacetonato)carbonyl[diallyl(tert-butyl)phosphine]rhodium(I)

E. Ocando-Mavarez, J. Ascanio, T. González, R. Atencio, M. Rosales and N. Silva

Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.006 Å
R factor = 0.022
wR factor = 0.049
Data-to-parameter ratio = 14.7

checkCIF results

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Problems with publication fields




 Alert Level A:


PUBL_003  Alert A The contact author's name is missing,                         
           _publ_contact_author_name.                                            

ADDSYM reports no extra symmetry

General Notes



REFLT_03                                                                        
         From the CIF: _diffrn_reflns_theta_max           24.98                 
         From the CIF: _reflns_number_total               2795                  
         Count of symmetry unique reflns         1889                           
         Completeness (_total/calc)            147.96%                          
         TEST3: Check Friedels for noncentro structure                          
         Estimate of Friedel pairs measured       906                           
         Fraction of Friedel pairs measured     0.480                           
         Are heavy atom types Z>Si present          yes                         
          WARNING: Large fraction of Friedel related reflns may                 
                   be needed to determine absolute structure                    


 1 Alert Level A = Potentially serious problem

 0 Alert Level B = Potential problem

 0 Alert Level C = Please check