# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' bott36m in C2/m' _shelx_refln_list_code 4 _shelx_F_calc_maximum 181.79 _exptl_crystal_F_000 360.00 _reflns_d_resolution_high 0.7511 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' _cell_length_a 11.7540 _cell_length_b 9.6390 _cell_length_c 5.1732 _cell_angle_alpha 90.000 _cell_angle_beta 112.946 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 242.65 247.22 2.44 o 4 0 0 4632.58 4648.35 123.07 o 6 0 0 624.08 602.04 10.81 o 8 0 0 1631.86 1656.80 24.71 o 10 0 0 84.58 93.96 2.47 o 12 0 0 360.91 374.38 6.45 o 14 0 0 117.14 123.47 6.25 o 1 1 0 6.14 6.44 0.33 o 3 1 0 2098.49 2124.29 69.68 o 5 1 0 1366.04 1383.94 17.21 o 7 1 0 1.79 5.91 1.26 o 9 1 0 2277.50 2330.63 32.92 o 11 1 0 20.58 19.80 1.77 o 13 1 0 3.05 10.81 3.60 o 0 2 0 220.38 186.70 1.96 o 2 2 0 10.55 8.69 0.53 o 4 2 0 52.14 62.32 2.35 o 6 2 0 1819.94 1874.82 32.45 o 8 2 0 37.81 44.48 2.21 o 10 2 0 578.49 561.13 9.43 o 12 2 0 792.11 781.23 6.86 o 14 2 0 28.45 31.34 1.45 o 1 3 0 188.01 252.67 6.80 o 3 3 0 4038.49 4080.66 87.47 o 5 3 0 711.27 680.30 14.43 o 7 3 0 228.24 200.70 2.51 o 9 3 0 258.99 259.37 3.32 o 11 3 0 893.17 899.66 9.59 o 13 3 0 98.07 99.53 2.35 o 0 4 0 7057.61 6583.12 142.91 o 2 4 0 7775.85 8257.96 87.81 o 4 4 0 2657.97 2782.09 42.60 o 6 4 0 4336.44 4401.54 121.21 o 8 4 0 3.75 9.92 2.47 o 10 4 0 163.49 169.76 2.79 o 12 4 0 0.92 1.99 1.74 o 1 5 0 1217.56 1398.40 27.51 o 3 5 0 365.03 292.89 7.04 o 5 5 0 531.53 562.17 6.55 o 7 5 0 4.44 8.52 1.49 o 9 5 0 903.34 896.11 17.29 o 11 5 0 684.45 662.54 10.06 o 13 5 0 360.96 379.34 9.16 o 0 6 0 90.83 90.84 6.74 o 2 6 0 0.38 1.46 2.29 o 4 6 0 97.33 90.44 3.11 o 6 6 0 351.21 332.40 3.06 o 8 6 0 320.70 314.89 4.16 o 10 6 0 1681.72 1696.17 41.63 o 12 6 0 59.74 65.77 2.08 o 1 7 0 1701.88 1828.69 90.14 o 3 7 0 205.54 214.95 4.55 o 5 7 0 479.19 477.50 7.35 o 7 7 0 2.32 10.59 2.04 o 9 7 0 672.63 654.21 12.17 o 11 7 0 231.32 223.77 4.90 o 0 8 0 6565.52 6304.66 34.51 o 2 8 0 620.00 629.84 14.35 o 4 8 0 1657.25 1708.99 29.89 o 6 8 0 199.14 212.22 4.85 o 8 8 0 510.72 493.28 6.45 o 10 8 0 13.19 13.67 1.84 o 1 9 0 225.28 232.55 5.08 o 3 9 0 432.66 484.73 18.48 o 5 9 0 1183.79 1159.21 15.49 o 7 9 0 485.59 476.19 20.95 o 9 9 0 238.46 242.14 13.04 o 0 10 0 1.85 11.90 6.25 o 2 10 0 153.78 141.99 6.94 o 4 10 0 167.91 150.90 7.04 o 6 10 0 344.22 343.18 10.01 o 8 10 0 0.83 -1.14 3.07 o 1 11 0 10.52 29.51 7.98 o 3 11 0 629.25 700.59 9.83 o 5 11 0 158.81 159.87 4.44 o 7 11 0 51.83 53.56 2.43 o 0 12 0 2285.58 2364.69 27.27 o 2 12 0 116.56 123.04 4.47 o 4 12 0 190.80 191.43 8.73 o -12 0 1 189.99 196.93 11.80 o -10 0 1 10.54 7.49 1.02 o -8 0 1 3796.86 4099.27 68.78 o -6 0 1 4713.18 4834.27 30.32 o -4 0 1 2860.20 2746.86 78.72 o -2 0 1 847.48 818.12 31.34 o 0 0 1 246.02 264.14 2.35 o 2 0 1 33048.86 32585.08 318.76 o 4 0 1 3859.17 4168.65 95.65 o 6 0 1 1281.21 1405.38 40.16 o 8 0 1 114.20 119.78 3.43 o 10 0 1 246.99 248.72 4.63 o 12 0 1 0.72 -0.30 5.36 o -13 1 1 10.80 11.13 1.38 o -11 1 1 958.45 925.15 16.10 o -9 1 1 72.60 66.91 1.61 o -7 1 1 191.65 216.96 1.88 o -5 1 1 5603.16 5702.80 98.26 o -3 1 1 2183.24 2158.13 18.20 o -1 1 1 100.18 102.00 2.18 o 1 1 1 9896.05 10330.55 142.56 o 3 1 1 621.23 573.93 11.86 o 5 1 1 606.59 613.81 4.91 o 7 1 1 395.04 377.05 4.38 o 9 1 1 140.70 144.97 2.05 o 11 1 1 103.49 103.46 3.21 o 13 1 1 504.40 512.35 8.87 o -14 2 1 157.06 166.56 6.60 o -12 2 1 101.56 107.43 2.76 o -10 2 1 92.07 99.10 2.40 o -8 2 1 319.63 323.64 2.62 o -6 2 1 139.94 177.82 3.53 o -4 2 1 484.43 503.23 13.23 o -2 2 1 11165.44 10887.34 494.47 o 0 2 1 391.29 361.17 8.20 o 2 2 1 4914.67 4926.82 101.95 o 4 2 1 3699.84 3852.12 25.93 o 6 2 1 814.63 800.58 10.30 o 8 2 1 11.78 12.09 0.71 o 10 2 1 1000.97 958.14 15.55 o 12 2 1 695.55 708.29 8.42 o -13 3 1 5.01 13.65 2.35 o -11 3 1 507.14 511.50 15.85 o -9 3 1 1132.87 1157.50 26.42 o -7 3 1 619.67 623.16 11.90 o -5 3 1 1096.50 1173.48 20.15 o -3 3 1 3510.70 3467.78 58.33 o -1 3 1 324.03 337.85 8.76 o 1 3 1 6380.60 6421.33 101.34 o 3 3 1 17.45 14.93 0.41 o 5 3 1 61.41 65.23 1.23 o 7 3 1 1306.63 1368.48 17.14 o 9 3 1 191.45 177.00 4.29 o 11 3 1 79.91 84.97 2.64 o -14 4 1 661.37 698.05 8.75 o -12 4 1 2076.10 2106.77 38.16 o -10 4 1 995.87 968.82 18.04 o -8 4 1 3574.23 3494.93 26.84 o -6 4 1 18.91 33.30 0.94 o -4 4 1 1383.42 1549.59 48.63 o -2 4 1 16.44 11.33 0.63 o 0 4 1 5121.51 5410.82 80.97 o 2 4 1 228.73 210.79 2.78 o 4 4 1 312.05 360.97 6.14 o 6 4 1 1694.71 1798.11 25.58 o 8 4 1 93.12 95.20 2.28 o 10 4 1 977.08 980.72 6.91 o 12 4 1 2.37 8.34 2.00 o -13 5 1 137.63 135.89 2.84 o -11 5 1 9.99 10.96 1.04 o -9 5 1 912.78 863.08 9.60 o -7 5 1 0.10 5.97 1.77 o -5 5 1 3018.53 3075.71 80.44 o -3 5 1 1231.86 1307.32 20.74 o -1 5 1 1161.15 1319.71 37.42 o 1 5 1 968.88 946.02 11.81 o 3 5 1 1562.32 1629.31 18.82 o 5 5 1 447.19 474.39 5.48 o 7 5 1 604.71 580.43 10.40 o 9 5 1 63.43 67.37 1.90 o 11 5 1 0.24 1.62 1.74 o -12 6 1 10.58 11.83 1.43 o -10 6 1 521.37 495.85 5.44 o -8 6 1 55.49 47.21 1.36 o -6 6 1 543.14 555.39 9.34 o -4 6 1 1626.89 1687.65 46.25 o -2 6 1 1744.69 1727.39 20.26 o 0 6 1 498.64 558.51 5.16 o 2 6 1 1208.99 1194.38 43.12 o 4 6 1 2582.03 2456.17 71.60 o 6 6 1 251.40 242.79 2.93 o 8 6 1 0.02 1.55 2.32 o 10 6 1 206.34 211.57 5.12 o -11 7 1 196.39 197.76 4.30 o -9 7 1 444.45 451.82 6.57 o -7 7 1 8.02 12.30 1.16 o -5 7 1 1879.42 1877.61 27.94 o -3 7 1 502.82 495.55 12.21 o -1 7 1 318.32 311.81 7.29 o 1 7 1 212.18 202.10 3.46 o 3 7 1 2031.41 2014.01 29.83 o 5 7 1 604.18 597.24 5.30 o 7 7 1 182.66 191.27 6.70 o 9 7 1 153.98 161.73 3.05 o 11 7 1 0.69 1.79 3.27 o -10 8 1 130.67 134.10 4.71 o -8 8 1 1221.75 1095.98 8.11 o -6 8 1 881.19 866.28 17.21 o -4 8 1 378.81 352.58 8.33 o -2 8 1 44.35 56.28 11.21 o 0 8 1 448.72 462.01 16.41 o 2 8 1 1366.72 1384.43 33.12 o 4 8 1 124.49 134.80 9.54 o 6 8 1 1368.41 1363.03 31.59 o 8 8 1 180.40 185.06 5.29 o 10 8 1 110.57 122.68 6.05 o -9 9 1 191.55 191.36 7.69 o -7 9 1 166.17 185.32 6.04 o -5 9 1 29.85 35.09 1.49 o -3 9 1 2072.04 1940.95 28.56 o -1 9 1 204.51 187.16 4.63 o 1 9 1 2720.75 2813.35 17.47 o 3 9 1 16.37 20.11 1.71 o 5 9 1 76.15 71.83 2.38 o 7 9 1 24.82 30.15 3.37 o 9 9 1 426.33 423.15 8.09 o -8 10 1 255.94 247.73 8.70 o -6 10 1 0.69 3.10 2.22 o -4 10 1 101.90 104.31 3.71 o -2 10 1 1059.26 1095.10 50.53 o 0 10 1 196.38 187.41 4.94 o 2 10 1 618.15 614.30 9.12 o 4 10 1 356.82 358.83 6.40 o 6 10 1 632.17 619.28 23.45 o -7 11 1 88.56 99.17 4.66 o -5 11 1 361.64 363.70 7.09 o -3 11 1 337.76 349.01 7.29 o -1 11 1 5.78 12.63 5.50 o 1 11 1 791.31 780.10 10.52 o 3 11 1 82.72 88.24 3.61 o 5 11 1 0.11 9.82 6.15 o -4 12 1 0.05 8.65 4.84 o -2 12 1 55.83 55.55 3.15 o 0 12 1 156.26 159.91 5.15 o 2 12 1 405.55 444.14 8.40 o -14 0 2 44.73 42.64 2.78 o -12 0 2 1065.87 1009.76 27.02 o -10 0 2 675.60 628.02 6.57 o -8 0 2 1.95 4.89 2.20 o -6 0 2 957.01 1059.68 16.89 o -4 0 2 64.23 41.23 1.47 o -2 0 2 7451.69 7031.97 24.45 o 0 0 2 7488.62 7609.19 395.70 o 2 0 2 6002.45 6075.30 42.74 o 4 0 2 3095.04 3245.89 25.79 o 6 0 2 67.36 68.82 2.31 o 8 0 2 327.37 314.69 6.50 o 10 0 2 438.40 433.79 28.31 o 12 0 2 50.30 50.68 4.26 o -15 1 2 91.97 97.20 7.04 o -13 1 2 498.42 509.63 12.59 o -11 1 2 265.21 273.17 6.14 o -9 1 2 11.20 14.14 0.88 o -7 1 2 2020.91 2150.24 16.63 o -5 1 2 123.69 113.94 1.61 o -3 1 2 410.91 445.75 13.70 o -1 1 2 2295.36 2252.50 60.72 o 1 1 2 533.18 522.30 6.81 o 3 1 2 1020.23 1152.17 51.12 o 5 1 2 974.57 976.21 20.24 o 7 1 2 1286.10 1241.22 23.58 o 9 1 2 10.55 13.37 0.85 o 11 1 2 279.46 276.32 5.01 o -14 2 2 456.21 450.34 25.09 o -12 2 2 126.17 120.53 3.39 o -10 2 2 3291.45 3345.86 30.42 o -8 2 2 1595.63 1545.28 21.66 o -6 2 2 224.21 220.93 6.12 o -4 2 2 6401.39 6657.08 129.36 o -2 2 2 2971.83 2910.36 65.24 o 0 2 2 3000.46 3051.90 29.68 o 2 2 2 1963.07 2017.83 20.10 o 4 2 2 3264.05 3340.78 38.05 o 6 2 2 193.33 198.55 2.62 o 8 2 2 184.61 184.58 2.95 o 10 2 2 82.05 88.66 2.37 o -15 3 2 0.82 3.70 3.57 o -13 3 2 1145.72 1149.48 11.45 o -11 3 2 29.03 28.10 1.18 o -9 3 2 0.10 5.47 2.09 o -7 3 2 679.88 642.86 6.83 o -5 3 2 1532.17 1521.19 6.69 o -3 3 2 255.77 221.42 4.92 o -1 3 2 62.50 56.72 1.37 o 1 3 2 2546.91 2510.64 22.15 o 3 3 2 145.08 155.63 8.57 o 5 3 2 1299.65 1282.61 23.68 o 7 3 2 163.78 168.77 3.76 o 9 3 2 213.35 205.70 14.03 o 11 3 2 368.40 371.45 5.75 o -14 4 2 31.72 38.40 2.45 o -12 4 2 10.42 10.21 1.19 o -10 4 2 700.01 682.10 17.65 o -8 4 2 2350.44 2201.04 62.43 o -6 4 2 578.67 569.13 28.37 o -4 4 2 4936.50 4990.25 110.13 o -2 4 2 149.14 171.40 2.23 o 0 4 2 1307.90 1337.56 36.07 o 2 4 2 620.25 580.24 28.77 o 4 4 2 202.24 213.82 4.44 o 6 4 2 905.38 908.75 14.05 o 8 4 2 71.58 72.20 2.62 o 10 4 2 146.61 149.46 3.79 o -13 5 2 591.77 619.79 16.17 o -11 5 2 693.51 675.77 12.20 o -9 5 2 825.07 812.76 20.03 o -7 5 2 260.69 290.04 6.95 o -5 5 2 204.28 154.61 6.51 o -3 5 2 259.72 303.96 3.08 o -1 5 2 593.16 538.38 11.86 o 1 5 2 2222.63 2271.81 42.34 o 3 5 2 7.79 9.62 0.93 o 5 5 2 151.39 148.94 2.38 o 7 5 2 907.35 920.05 8.18 o 9 5 2 25.68 26.16 1.52 o -12 6 2 17.29 19.24 2.78 o -10 6 2 2036.10 1980.61 62.95 o -8 6 2 1493.10 1374.59 28.91 o -6 6 2 714.14 656.44 5.10 o -4 6 2 713.88 695.14 28.33 o -2 6 2 4332.44 4474.33 50.06 o 0 6 2 17.20 18.45 1.26 o 2 6 2 204.24 186.77 7.66 o 4 6 2 2064.52 1966.61 35.34 o 6 6 2 239.19 233.19 7.33 o 8 6 2 363.82 352.36 6.01 o 10 6 2 42.69 47.65 2.35 o -13 7 2 75.18 77.55 4.76 o -11 7 2 657.20 696.16 7.84 o -9 7 2 232.21 213.71 3.64 o -7 7 2 165.21 151.16 4.17 o -5 7 2 395.53 403.19 5.14 o -3 7 2 121.09 128.13 2.82 o -1 7 2 915.31 902.45 20.16 o 1 7 2 617.38 608.87 14.20 o 3 7 2 27.40 27.89 1.36 o 5 7 2 7.98 8.54 1.52 o 7 7 2 1206.17 1165.94 13.38 o 9 7 2 19.81 22.72 2.63 o -12 8 2 63.37 81.65 3.82 o -10 8 2 11.45 16.02 1.28 o -8 8 2 327.52 325.19 8.25 o -6 8 2 63.66 46.62 2.76 o -4 8 2 149.89 166.98 5.95 o -2 8 2 1248.79 1172.23 17.65 o 0 8 2 1197.46 1149.57 34.07 o 2 8 2 881.02 882.71 14.34 o 4 8 2 75.77 76.77 2.86 o 6 8 2 108.79 110.67 4.03 o 8 8 2 0.37 8.15 3.80 o -11 9 2 26.30 23.16 2.38 o -9 9 2 0.15 2.26 2.44 o -7 9 2 553.96 505.22 6.77 o -5 9 2 604.06 650.87 22.26 o -3 9 2 477.31 449.96 7.26 o -1 9 2 47.94 36.37 2.31 o 1 9 2 824.44 808.71 21.77 o 3 9 2 479.96 467.02 11.11 o 5 9 2 878.58 887.30 12.74 o 7 9 2 462.62 463.24 12.20 o -8 10 2 495.67 476.15 15.02 o -6 10 2 34.00 33.01 2.30 o -4 10 2 1005.82 1023.20 18.84 o -2 10 2 535.50 525.38 8.31 o 0 10 2 338.51 354.19 6.86 o 2 10 2 547.66 546.84 16.02 o 4 10 2 851.72 859.61 30.94 o 6 10 2 0.13 1.69 7.54 o -7 11 2 280.09 316.54 15.42 o -5 11 2 336.59 337.98 11.65 o -3 11 2 10.59 13.49 10.66 o -1 11 2 186.58 179.48 14.63 o 1 11 2 213.96 220.70 5.80 o 3 11 2 48.17 55.85 3.07 o -4 12 2 466.98 519.97 13.69 o -2 12 2 156.86 146.34 4.98 o 0 12 2 243.70 264.40 9.82 o -14 0 3 307.03 293.74 5.59 o -12 0 3 1182.64 1160.24 26.83 o -10 0 3 131.51 100.67 2.00 o -8 0 3 12.46 13.45 7.49 o -6 0 3 5716.63 6120.27 311.80 o -4 0 3 55.71 44.32 1.82 o -2 0 3 10.30 9.77 1.16 o 0 0 3 1.22 18.33 5.65 o 2 0 3 7285.13 6959.10 30.25 o 4 0 3 1378.78 1381.19 13.79 o 6 0 3 2852.87 2812.46 20.63 o 8 0 3 341.07 326.78 7.34 o 10 0 3 44.31 48.20 3.17 o -15 1 3 211.50 217.16 4.34 o -13 1 3 578.23 576.66 6.06 o -11 1 3 85.48 81.56 1.55 o -9 1 3 821.43 788.71 8.70 o -7 1 3 1465.25 1501.15 22.19 o -5 1 3 169.77 193.80 1.91 o -3 1 3 2051.37 2140.55 28.19 o -1 1 3 886.55 847.33 11.82 o 1 1 3 229.00 226.80 3.05 o 3 1 3 1364.71 1325.75 19.79 o 5 1 3 7.21 16.67 3.75 o 7 1 3 160.91 155.70 3.56 o 9 1 3 1.88 10.76 8.18 o -14 2 3 26.83 25.92 1.57 o -12 2 3 107.92 118.10 2.02 o -10 2 3 964.36 907.86 43.74 o -8 2 3 1540.54 1587.91 25.07 o -6 2 3 24.53 24.51 0.90 o -4 2 3 1657.71 1592.35 17.94 o -2 2 3 734.82 799.96 13.40 o 0 2 3 277.79 282.27 6.04 o 2 2 3 60.15 67.44 1.85 o 4 2 3 158.52 155.69 3.42 o 6 2 3 14.92 15.82 1.41 o 8 2 3 164.55 155.23 4.26 o 10 2 3 22.01 20.33 2.68 o -15 3 3 83.89 87.86 3.57 o -13 3 3 382.67 372.82 3.59 o -11 3 3 263.05 262.07 4.67 o -9 3 3 1433.84 1402.01 19.54 o -7 3 3 575.56 547.90 5.18 o -5 3 3 205.53 202.92 3.15 o -3 3 3 1262.30 1265.02 21.58 o -1 3 3 1921.32 1860.62 17.26 o 1 3 3 149.55 151.02 2.74 o 3 3 3 35.37 32.74 1.76 o 5 3 3 560.80 563.31 31.19 o 7 3 3 109.16 109.69 5.40 o 9 3 3 210.49 223.64 7.34 o -14 4 3 10.98 13.05 1.75 o -12 4 3 1336.13 1296.15 10.56 o -10 4 3 454.95 436.24 15.82 o -8 4 3 3344.16 3297.43 100.75 o -6 4 3 23.31 27.43 1.41 o -4 4 3 374.73 351.87 7.30 o -2 4 3 1437.53 1475.23 29.61 o 0 4 3 2457.61 2400.34 39.82 o 2 4 3 2861.32 2817.24 82.41 o 4 4 3 239.54 246.78 6.34 o 6 4 3 360.34 350.97 6.73 o 8 4 3 1268.03 1252.58 65.36 o -13 5 3 215.06 205.56 7.34 o -11 5 3 84.32 85.24 2.91 o -9 5 3 71.92 70.63 3.22 o -7 5 3 3229.58 3079.59 110.44 o -5 5 3 3.99 3.24 2.72 o -3 5 3 1448.64 1460.86 8.64 o -1 5 3 386.03 353.09 5.02 o 1 5 3 0.91 0.82 1.83 o 3 5 3 31.68 29.02 1.49 o 5 5 3 628.90 638.48 6.29 o 7 5 3 0.41 -2.88 2.88 o -12 6 3 86.92 82.01 3.00 o -10 6 3 516.10 492.86 8.88 o -8 6 3 943.13 935.26 45.27 o -6 6 3 33.18 39.48 2.01 o -4 6 3 1284.30 1276.68 20.37 o -2 6 3 27.11 25.44 2.35 o 0 6 3 61.45 64.53 2.15 o 2 6 3 502.37 484.08 8.87 o 4 6 3 82.69 75.52 3.36 o 6 6 3 25.99 26.41 5.48 o 8 6 3 116.43 124.23 6.10 o -11 7 3 14.45 20.57 2.83 o -9 7 3 59.66 52.48 5.85 o -7 7 3 1719.53 1649.19 33.91 o -5 7 3 93.73 95.92 2.65 o -3 7 3 353.76 340.74 11.90 o -1 7 3 468.24 468.73 22.10 o 1 7 3 121.62 123.44 3.00 o 3 7 3 365.12 358.14 4.98 o 5 7 3 421.44 407.26 10.04 o 7 7 3 11.87 17.95 11.90 o -10 8 3 98.57 84.19 4.96 o -8 8 3 232.47 209.46 8.72 o -6 8 3 576.90 521.81 8.92 o -4 8 3 359.13 382.55 22.12 o -2 8 3 2.64 3.59 4.17 o 0 8 3 13.22 15.06 1.35 o 2 8 3 2462.26 2416.32 55.08 o 4 8 3 364.77 370.04 5.40 o 6 8 3 755.15 770.48 15.37 o -9 9 3 664.77 702.99 9.24 o -7 9 3 268.46 282.39 20.78 o -5 9 3 146.45 122.78 4.06 o -3 9 3 226.48 199.32 5.90 o -1 9 3 1623.67 1559.33 14.09 o 1 9 3 291.20 267.83 5.92 o 3 9 3 49.04 58.67 3.22 o 5 9 3 8.98 16.60 11.85 o -8 10 3 226.28 239.31 7.54 o -6 10 3 7.85 13.99 9.87 o -4 10 3 649.48 638.94 21.22 o -2 10 3 71.27 73.12 3.40 o 0 10 3 103.91 109.90 11.65 o 2 10 3 3.76 26.67 5.87 o -5 11 3 29.86 32.19 2.55 o -3 11 3 205.69 205.43 5.86 o -1 11 3 469.45 490.85 8.89 o 1 11 3 4.39 16.96 9.32 o -14 0 4 16.52 20.63 2.58 o -12 0 4 2601.11 2585.25 28.28 o -10 0 4 911.64 850.86 16.84 o -8 0 4 1929.54 1694.18 17.45 o -6 0 4 1156.77 1256.00 14.38 o -4 0 4 3784.27 3908.34 17.90 o -2 0 4 1398.08 1448.80 10.80 o 0 0 4 650.41 679.54 10.71 o 2 0 4 4.35 23.21 6.45 o 4 0 4 380.52 365.75 8.43 o 6 0 4 16.36 15.07 2.28 o 8 0 4 834.10 750.84 12.60 o -15 1 4 113.66 113.91 3.75 o -13 1 4 47.14 50.05 1.73 o -11 1 4 260.02 266.98 3.70 o -9 1 4 278.48 285.45 6.41 o -7 1 4 388.19 384.59 10.66 o -5 1 4 141.13 147.21 2.54 o -3 1 4 901.14 862.09 17.71 o -1 1 4 437.54 446.73 9.08 o 1 1 4 115.41 112.60 4.41 o 3 1 4 390.75 384.21 5.99 o 5 1 4 719.95 658.64 15.07 o 7 1 4 471.53 443.58 7.14 o -14 2 4 156.90 161.57 5.97 o -12 2 4 219.92 230.59 4.93 o -10 2 4 1.07 -4.00 4.76 o -8 2 4 351.90 347.79 8.90 o -6 2 4 8.65 8.44 0.73 o -4 2 4 32.37 33.27 1.11 o -2 2 4 282.00 285.90 11.91 o 0 2 4 712.59 696.98 16.22 o 2 2 4 126.25 122.47 3.47 o 4 2 4 1085.21 1102.88 24.15 o 6 2 4 252.60 269.09 5.28 o -13 3 4 1.55 1.87 3.91 o -11 3 4 135.30 146.93 3.95 o -9 3 4 368.40 347.01 8.33 o -7 3 4 483.88 485.66 4.47 o -5 3 4 487.49 479.13 5.42 o -3 3 4 274.39 262.75 3.08 o -1 3 4 853.83 846.14 24.85 o 1 3 4 79.01 85.44 4.56 o 3 3 4 1101.85 1076.51 40.46 o 5 3 4 12.80 12.40 1.45 o 7 3 4 3.56 7.80 1.33 o -14 4 4 418.05 435.28 5.91 o -12 4 4 362.41 336.31 8.13 o -10 4 4 1498.41 1529.98 46.17 o -8 4 4 162.87 176.27 5.64 o -6 4 4 7412.61 7293.32 27.65 o -4 4 4 0.87 8.01 2.57 o -2 4 4 295.78 304.54 4.42 o 0 4 4 21.27 19.15 1.39 o 2 4 4 512.49 497.30 5.71 o 4 4 4 102.91 97.20 2.72 o 6 4 4 59.89 63.07 2.31 o -13 5 4 53.73 50.36 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