# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' mvc1 in P-1 2003/06/23 14:19:36 055 KENX' _shelx_refln_list_code 4 _shelx_F_calc_maximum 435.99 _exptl_crystal_F_000 1504.00 _reflns_d_resolution_high 0.8997 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 9.7641 _cell_length_b 10.4448 _cell_length_c 27.2451 _cell_angle_alpha 80.396 _cell_angle_beta 83.548 _cell_angle_gamma 63.566 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 57558.38 58464.69 1667.55 o 2 0 0 4201.91 4189.13 667.50 o 3 0 0 16215.24 16134.44 1392.15 o 4 0 0 21599.29 21379.34 1796.42 o 5 0 0 22351.84 20454.08 1862.27 o 6 0 0 32640.36 31450.42 2446.64 o 7 0 0 15599.93 18297.32 2405.47 o 8 0 0 3773.63 2626.27 2561.30 o 9 0 0 58.55 -1904.92 2206.72 o -9 1 0 452.04 895.91 2439.09 o -8 1 0 3097.06 1844.99 2134.01 o -7 1 0 8252.76 5734.89 2174.41 o -6 1 0 28314.51 26425.15 2404.63 o -5 1 0 14248.04 12463.16 1709.39 o -4 1 0 12854.88 12414.80 1427.51 o -3 1 0 3018.59 3412.61 810.95 o -2 1 0 88914.42 92571.52 1940.45 o -1 1 0 47259.33 36769.84 8345.66 o 0 1 0 46403.48 50720.56 1055.67 o 1 1 0 29615.10 28030.45 1787.89 o 2 1 0 2501.74 2430.49 638.14 o 3 1 0 3153.96 2622.34 839.41 o 4 1 0 24139.94 24774.91 1630.13 o 5 1 0 24623.51 24956.06 1872.28 o 6 1 0 8827.13 9776.25 2557.17 o 7 1 0 250.85 793.02 1617.64 o 8 1 0 1484.49 610.43 1789.42 o 9 1 0 10.67 288.39 1977.81 o 10 1 0 144.46 809.02 2409.64 o -8 2 0 1454.02 414.75 2268.50 o -7 2 0 7370.07 7043.41 2069.69 o -6 2 0 11392.30 10360.29 2197.47 o -5 2 0 8492.48 7902.36 2708.07 o -4 2 0 2423.61 3588.67 1246.36 o -3 2 0 91.72 323.01 1046.49 o -2 2 0 224.93 169.95 624.28 o -1 2 0 7714.34 7295.47 578.29 o 0 2 0 6719.73 6790.71 466.54 o 1 2 0 5399.61 5104.25 358.54 o 2 2 0 840.89 938.12 576.20 o 3 2 0 4536.45 4348.48 1035.69 o 4 2 0 865.32 1427.75 897.12 o 5 2 0 324.73 278.34 1978.34 o 6 2 0 132.71 630.23 1185.15 o 7 2 0 533.47 -111.29 1364.45 o 8 2 0 125.86 -281.55 1600.21 o 9 2 0 305.91 -518.69 1873.95 o 10 2 0 11.38 977.01 2272.66 o -8 3 0 147.70 386.20 2684.09 o -7 3 0 2182.01 2861.14 2693.60 o -6 3 0 618.88 127.65 1738.24 o -5 3 0 100.02 -1350.44 1397.87 o -4 3 0 2428.41 1685.78 1266.31 o -3 3 0 18.87 551.47 1034.47 o -2 3 0 72.83 402.51 675.35 o -1 3 0 2096.57 1900.75 578.80 o 0 3 0 11689.10 11970.68 664.57 o 1 3 0 36410.13 38020.95 1098.98 o 2 3 0 3241.95 4247.22 789.03 o 3 3 0 221.82 772.97 887.28 o 4 3 0 615.66 -597.77 1016.58 o 5 3 0 2584.29 3356.75 1009.57 o 6 3 0 16633.90 17239.39 1680.81 o 7 3 0 12481.64 14760.80 1880.82 o 8 3 0 3382.42 4296.52 1703.30 o 9 3 0 596.41 941.94 1864.40 o 10 3 0 548.06 57.21 2164.34 o -7 4 0 4.50 479.60 3584.58 o -6 4 0 546.34 -1850.03 1850.03 o -5 4 0 621.95 3643.46 1728.07 o -4 4 0 1839.04 2869.91 2451.74 o -3 4 0 370.50 506.34 1170.04 o -2 4 0 603.65 1050.35 781.21 o -1 4 0 4382.29 3881.34 732.55 o 0 4 0 26151.27 23475.77 1896.31 o 1 4 0 14367.72 15198.11 2124.75 o 2 4 0 6650.93 7107.29 586.49 o 3 4 0 382.17 229.95 939.98 o 4 4 0 1814.45 2954.75 1118.22 o 5 4 0 20917.76 21013.54 979.20 o 6 4 0 28246.81 28446.64 1440.96 o 7 4 0 18457.69 16892.82 1804.81 o 8 4 0 11145.37 10016.15 1822.56 o 9 4 0 661.98 343.15 1746.35 o 10 4 0 36.34 -1208.53 2113.77 o -6 5 0 5869.52 4895.20 4026.97 o -5 5 0 2630.12 2954.63 1857.65 o -4 5 0 4683.09 5413.69 2441.40 o -3 5 0 3548.51 4217.77 1378.14 o -2 5 0 3325.97 4567.43 981.61 o -1 5 0 24275.39 25279.43 1225.09 o 0 5 0 36505.98 37616.09 2629.03 o 1 5 0 53947.73 50815.71 2725.40 o 2 5 0 30078.50 31627.97 1164.70 o 3 5 0 2923.89 4519.77 1535.69 o 4 5 0 40.40 -404.13 1033.42 o 5 5 0 19155.86 19040.13 4988.23 o 6 5 0 33152.46 32409.66 2600.99 o 7 5 0 13397.55 12400.09 1263.27 o 8 5 0 16338.82 15475.73 1902.15 o 9 5 0 2514.36 2499.45 1779.57 o 10 5 0 186.56 264.61 3427.47 o -5 6 0 9266.56 4469.35 3969.08 o -4 6 0 4581.51 4014.56 3299.30 o -3 6 0 941.01 1336.99 1537.15 o -2 6 0 436.95 646.38 1092.19 o -1 6 0 14638.84 14830.44 1223.42 o 0 6 0 13206.74 13035.99 1113.44 o 1 6 0 19124.20 18603.15 1336.05 o 2 6 0 14589.19 14921.02 1227.99 o 3 6 0 223.58 195.13 696.08 o 4 6 0 98.66 913.98 1256.85 o 5 6 0 8154.03 7939.11 1595.84 o 6 6 0 13235.42 12037.96 1943.71 o 7 6 0 4597.90 4556.18 1841.81 o 8 6 0 3069.32 1112.17 2848.64 o 9 6 0 1049.71 3601.12 3113.25 o 10 6 0 38.19 -2534.43 3588.71 o -4 7 0 5031.85 9401.77 4051.77 o -3 7 0 829.20 -727.67 3018.16 o -2 7 0 18.36 690.46 2844.51 o -1 7 0 4870.25 4605.02 1432.17 o 0 7 0 8140.72 7793.94 1423.36 o 1 7 0 7540.06 6760.42 1195.43 o 2 7 0 4383.82 4173.34 1123.79 o 3 7 0 1635.19 1354.84 1017.45 o 4 7 0 2315.30 384.12 1419.75 o 5 7 0 491.37 109.10 1477.21 o 6 7 0 8.21 1669.68 1511.13 o 7 7 0 144.05 56.72 1705.86 o 8 7 0 47.17 1475.77 1989.65 o 9 7 0 417.84 -554.02 3129.79 o 10 7 0 54.79 -173.65 3406.80 o -3 8 0 6.36 1951.47 3613.52 o -2 8 0 194.94 1649.65 3295.17 o -1 8 0 1195.85 3592.85 3138.06 o 0 8 0 53.05 31.35 1015.57 o 1 8 0 4.74 -304.88 1173.45 o 2 8 0 697.30 916.19 1209.18 o 3 8 0 589.58 298.73 1141.56 o 4 8 0 486.97 1241.25 1100.19 o 5 8 0 552.64 758.78 1600.28 o 6 8 0 2507.90 2417.53 1774.07 o 7 8 0 3039.64 3256.10 1941.64 o 8 8 0 1987.18 3767.24 2590.24 o 9 8 0 129.81 2577.45 2477.66 o 10 8 0 39.92 -4031.10 4031.10 o -2 9 0 5.46 -33.08 3869.86 o -1 9 0 280.58 2708.07 3452.28 o 0 9 0 2305.61 4015.01 2185.94 o 1 9 0 2177.01 4615.54 2080.15 o 2 9 0 2142.14 2690.56 1425.24 o 3 9 0 1433.82 502.91 1362.46 o 4 9 0 148.04 -698.31 1278.67 o 5 9 0 4930.86 5491.28 1939.07 o 6 9 0 10587.58 11301.80 2373.11 o 7 9 0 3772.94 5474.66 2098.98 o 8 9 0 5306.89 6747.90 2490.89 o 9 9 0 2078.34 1810.15 2566.34 o 0 10 0 5389.95 5303.20 2734.32 o 1 10 0 5492.47 6134.67 2477.61 o 2 10 0 9373.08 11193.06 2524.44 o 3 10 0 1703.29 3638.46 1704.82 o 4 10 0 53.35 2660.91 2024.32 o 5 10 0 943.49 1665.56 1994.66 o 6 10 0 5713.39 4961.23 2360.24 o 7 10 0 8722.89 8245.11 2468.68 o 8 10 0 6375.27 3036.77 2437.99 o 2 11 0 3720.77 1674.46 3762.36 o 3 11 0 1956.37 868.24 3522.56 o 4 11 0 43.18 3038.83 3609.39 o 5 11 0 1930.12 1555.21 2391.58 o 6 11 0 2872.17 2976.63 2520.73 o 7 11 0 3806.56 4197.74 2651.92 o -6 -11 1 1020.22 1631.24 2513.60 o -5 -11 1 94.49 3738.07 2600.71 o -4 -11 1 47.77 1323.03 3890.53 o -3 -11 1 113.72 -376.24 3799.57 o -8 -10 1 81.50 -46.28 2373.62 o -7 -10 1 50.39 585.54 2231.67 o -6 -10 1 274.33 2344.83 2227.60 o -5 -10 1 115.18 -213.97 2048.40 o -4 -10 1 405.63 1131.95 2009.61 o -3 -10 1 78.18 1342.63 2146.38 o -2 -10 1 2074.59 2427.07 2352.64 o -1 -10 1 1974.39 4201.01 2418.66 o 0 -10 1 2360.28 1126.53 2492.66 o -9 -9 1 167.55 2084.55 2743.84 o -8 -9 1 2414.13 1442.07 2213.39 o -7 -9 1 5212.63 7560.76 2250.14 o -6 -9 1 2523.28 3713.96 2096.17 o -5 -9 1 2517.45 2116.07 1862.98 o -4 -9 1 267.08 1023.64 1338.09 o -3 -9 1 56.54 -52.07 1370.24 o -2 -9 1 2759.48 4948.14 1634.43 o -1 -9 1 7725.35 9765.39 2285.05 o 0 -9 1 8686.96 12158.27 2505.43 o 1 -9 1 3333.79 4233.69 3522.56 o 2 -9 1 825.92 3080.17 3811.97 o -10 -8 1 194.06 -529.21 3960.81 o -9 -8 1 13.88 1309.01 2407.11 o -8 -8 1 1437.16 487.68 1959.47 o -7 -8 1 5696.41 7838.22 2147.73 o -6 -8 1 13537.86 12818.14 2242.23 o -5 -8 1 4077.23 3268.18 1733.33 o -4 -8 1 2761.94 2293.69 1152.76 o -3 -8 1 566.92 1871.20 1189.15 o -2 -8 1 5890.18 7306.19 1671.41 o -1 -8 1 6641.47 5945.60 2183.92 o 0 -8 1 8385.49 9968.17 2194.16 o 1 -8 1 6691.97 7913.36 3229.02 o 2 -8 1 982.28 1120.44 3253.82 o 3 -8 1 0.55 988.14 3679.67 o -10 -7 1 1171.15 6007.37 3754.09 o -9 -7 1 7.05 -248.07 3257.96 o -8 -7 1 7151.48 9164.88 2381.09 o -7 -7 1 14388.18 14126.55 2846.58 o -6 -7 1 20673.75 18852.34 3714.81 o -5 -7 1 14265.11 11097.86 2429.00 o -4 -7 1 11756.80 11419.71 1447.23 o -3 -7 1 906.02 913.60 1016.26 o -2 -7 1 6027.20 5259.16 1123.31 o -1 -7 1 7014.02 7093.60 1195.88 o 0 -7 1 6713.01 7666.10 1779.89 o 1 -7 1 5785.38 5135.00 2976.81 o 2 -7 1 3301.10 2493.08 2939.60 o 3 -7 1 2.49 -2889.99 2889.99 o 4 -7 1 94.98 1798.49 3778.90 o -10 -6 1 1175.39 2294.63 3439.87 o -9 -6 1 437.41 -1624.84 2980.95 o -8 -6 1 3817.69 4490.03 2865.18 o -7 -6 1 10337.33 11854.92 2175.95 o -6 -6 1 11171.96 8624.67 1765.40 o -5 -6 1 8107.38 7598.30 1606.05 o -4 -6 1 2160.17 2203.89 1283.56 o -3 -6 1 2063.15 2828.22 762.77 o -2 -6 1 4764.17 4107.86 940.76 o -1 -6 1 939.74 674.76 760.96 o 0 -6 1 2126.54 1941.03 877.01 o 1 -6 1 865.39 2050.69 2199.53 o 2 -6 1 438.47 3468.81 2517.89 o 3 -6 1 1.67 -249.92 1465.38 o 4 -6 1 19.49 -3005.75 3005.75 o 5 -6 1 809.12 -570.56 3762.36 o -10 -5 1 1555.09 2025.89 3501.89 o -9 -5 1 38.13 -164.71 1749.79 o -8 -5 1 378.97 393.46 1435.78 o -7 -5 1 287.57 -598.69 1177.81 o -6 -5 1 71.23 1676.11 780.13 o -5 -5 1 2.93 676.89 1195.67 o -4 -5 1 26.26 246.22 1062.33 o -3 -5 1 4.62 659.02 598.46 o -2 -5 1 23.13 -1.20 650.00 o -1 -5 1 812.28 547.68 645.22 o 0 -5 1 5466.27 5976.29 781.45 o 1 -5 1 7292.78 6764.13 854.35 o 2 -5 1 3245.74 2979.53 882.08 o 3 -5 1 839.56 439.95 1268.90 o 4 -5 1 1373.62 1551.31 1501.92 o 5 -5 1 2463.58 1021.21 3092.58 o 6 -5 1 3223.23 2273.95 3811.97 o -10 -4 1 136.57 1740.40 2207.11 o -9 -4 1 29.58 554.44 1787.60 o -8 -4 1 1753.78 1791.34 1568.64 o -7 -4 1 9171.53 9850.45 1587.41 o -6 -4 1 8133.86 9190.92 1337.06 o -5 -4 1 5721.98 4136.16 974.98 o -4 -4 1 8646.10 8423.79 1353.55 o -3 -4 1 952.11 890.40 609.22 o -2 -4 1 19906.13 20211.76 806.70 o -1 -4 1 23304.75 23888.64 867.94 o 0 -4 1 25992.11 25889.38 996.10 o 1 -4 1 24150.46 24374.95 1011.56 o 2 -4 1 8963.41 9427.25 890.98 o 3 -4 1 4247.88 3387.78 952.89 o 4 -4 1 553.37 1226.38 1312.19 o 5 -4 1 7145.69 6539.35 1759.51 o 6 -4 1 10374.16 11987.34 2609.17 o 7 -4 1 5069.04 7222.91 4022.83 o -10 -3 1 1136.98 2165.76 2532.36 o -9 -3 1 11.63 375.95 1830.87 o -8 -3 1 4263.77 3152.25 2364.91 o -7 -3 1 7972.63 7960.69 1618.08 o -6 -3 1 32109.88 31356.96 2106.33 o -5 -3 1 27275.07 27159.29 3005.75 o -4 -3 1 16135.53 15986.75 1099.14 o -3 -3 1 50.82 533.74 611.67 o -2 -3 1 64338.50 63951.55 1739.81 o -1 -3 1 59886.04 58029.36 8188.48 o 0 -3 1 22099.97 21960.54 740.86 o 1 -3 1 12720.40 13427.65 706.94 o 2 -3 1 45439.51 37909.65 3242.96 o 3 -3 1 223.02 776.37 747.56 o 4 -3 1 6584.49 7379.52 1377.44 o 5 -3 1 3256.86 3843.59 1561.71 o 6 -3 1 8989.18 8793.90 1968.76 o 7 -3 1 7561.21 6266.69 2861.05 o 8 -3 1 2745.36 206.72 3907.07 o -10 -2 1 4093.99 3714.23 2385.60 o -9 -2 1 148.98 498.01 1951.99 o -8 -2 1 4660.18 6448.99 1886.87 o -7 -2 1 16300.48 17934.08 2111.36 o -6 -2 1 33896.82 38833.22 4502.43 o -5 -2 1 27878.48 26825.47 1820.39 o -4 -2 1 11095.53 12841.64 2001.08 o -3 -2 1 1468.65 1826.79 891.23 o -2 -2 1 5493.94 6217.00 445.49 o -1 -2 1 40908.07 40386.71 719.56 o 0 -2 1 93140.13 95718.13 1190.88 o 1 -2 1 2124.75 2421.61 438.57 o 2 -2 1 7998.26 7863.06 781.79 o 3 -2 1 4837.55 5277.83 863.04 o 4 -2 1 28.59 137.84 1083.98 o 5 -2 1 4223.93 4422.35 1457.77 o 6 -2 1 5423.86 4682.45 1682.58 o 7 -2 1 2913.31 4843.16 3150.46 o 8 -2 1 1521.57 1803.84 2306.88 o -10 -1 1 2248.49 870.72 2467.54 o -9 -1 1 22.98 664.63 2058.50 o -8 -1 1 883.05 -227.95 1811.31 o -7 -1 1 7003.42 4897.59 1862.39 o -6 -1 1 18589.11 16848.08 1840.06 o -5 -1 1 22824.13 23897.26 2255.35 o -4 -1 1 4663.38 5800.65 1591.77 o -3 -1 1 6937.76 5990.84 1459.47 o -2 -1 1 4262.02 5036.06 737.81 o -1 -1 1 3339.70 2978.70 241.97 o 0 -1 1 9783.18 10016.15 587.43 o 1 -1 1 10176.59 10453.73 496.14 o 2 -1 1 44985.44 36552.75 14297.90 o 3 -1 1 718.13 1520.09 747.60 o 4 -1 1 2025.06 459.53 1020.65 o 5 -1 1 266.38 914.72 1290.16 o 6 -1 1 69.21 86.56 1451.43 o 7 -1 1 466.31 -1016.44 1725.39 o 8 -1 1 54.54 -23.96 1978.28 o 9 -1 1 347.31 1243.14 2442.72 o -9 0 1 18.85 1189.43 2251.19 o -8 0 1 174.06 551.36 2016.17 o -7 0 1 2377.52 1949.63 1707.96 o -6 0 1 874.41 -85.20 1350.05 o -5 0 1 2144.96 1788.77 1167.81 o -4 0 1 424.73 -57.17 920.78 o -3 0 1 2006.64 1439.50 882.54 o -2 0 1 32631.74 34652.71 1455.83 o -1 0 1 1932.73 1847.17 451.33 o 1 0 1 6417.98 7617.95 404.60 o 2 0 1 35088.00 34609.60 979.59 o 3 0 1 12382.34 13647.96 1009.40 o 4 0 1 1032.47 271.76 1165.92 o 5 0 1 3963.38 4429.15 1279.74 o 6 0 1 7282.79 5773.59 1694.00 o 7 0 1 4506.05 5811.79 1799.06 o 8 0 1 7983.15 6078.13 2088.39 o 9 0 1 2430.75 1592.12 2297.42 o -9 1 1 101.77 -250.16 2494.75 o -8 1 1 13.73 790.41 2215.59 o -7 1 1 29.49 11.86 2027.95 o -6 1 1 2628.71 5113.78 1659.13 o -5 1 1 905.74 1534.00 1243.14 o -4 1 1 2271.01 2657.41 1133.73 o -3 1 1 3837.06 2526.65 1548.36 o -2 1 1 4537.85 4280.82 730.86 o -1 1 1 38801.80 43812.63 1905.99 o 0 1 1 36045.88 35080.61 959.20 o 1 1 1 26653.03 26860.11 1491.30 o 2 1 1 57245.71 59485.92 1953.19 o 3 1 1 8105.97 8605.90 874.04 o 4 1 1 7.65 -659.48 1314.76 o 5 1 1 5419.05 5751.21 1358.07 o 6 1 1 44956.11 45735.71 2679.21 o 7 1 1 17510.18 17037.40 2130.86 o 8 1 1 12676.65 10661.25 2865.18 o 9 1 1 3701.99 2601.38 2089.74 o 10 1 1 0.66 -1342.67 2357.10 o -8 2 1 289.09 2234.40 2447.35 o -7 2 1 1438.08 1383.55 2451.74 o -6 2 1 10004.50 8645.18 1887.94 o -5 2 1 18864.51 19842.67 2675.00 o -4 2 1 18533.17 20267.27 1831.57 o -3 2 1 2378.49 3781.37 1492.54 o -2 2 1 255.88 515.20 511.64 o -1 2 1 20649.82 20304.10 1315.64 o 0 2 1 51915.01 52131.67 1248.28 o 1 2 1 51879.79 52934.16 2143.66 o 2 2 1 57886.49 57761.84 3416.44 o 3 2 1 5424.79 4831.86 713.02 o 4 2 1 7842.71 6338.75 1227.94 o 5 2 1 4898.33 5463.67 1133.85 o 6 2 1 27771.47 29647.42 3311.70 o 7 2 1 22348.65 22115.97 2294.63 o 8 2 1 14854.79 15438.46 2211.98 o 9 2 1 1105.83 319.26 1903.73 o 10 2 1 4.39 1340.86 2272.18 o -8 3 1 246.73 5360.49 4314.31 o -7 3 1 4909.56 5959.95 2248.19 o -6 3 1 8797.52 8538.42 2013.42 o -5 3 1 17105.09 16238.73 2075.89 o -4 3 1 34159.66 35189.36 2330.48 o -3 3 1 934.51 1337.50 1089.75 o -2 3 1 323.13 311.32 706.49 o -1 3 1 10030.53 10813.29 691.55 o 0 3 1 24296.63 24995.26 988.15 o 1 3 1 21494.41 22322.69 1245.43 o 2 3 1 37486.37 37916.65 2734.94 o 3 3 1 5095.91 6118.70 1111.12 o 4 3 1 96.87 334.98 627.29 o 5 3 1 6670.65 7403.34 1513.21 o 6 3 1 9207.07 9335.88 1447.38 o 7 3 1 7277.75 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