data_I _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_limit_l_max 30 loop_ _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_wavelength_id all _diffrn_orient_matrix_type 'X=UH' _diffrn_orient_matrix_UB_11 -0.02993 _diffrn_orient_matrix_UB_12 0.07641 _diffrn_orient_matrix_UB_13 -0.07515 _diffrn_orient_matrix_UB_21 -0.10450 _diffrn_orient_matrix_UB_22 0.03821 _diffrn_orient_matrix_UB_23 -0.00192 _diffrn_orient_matrix_UB_31 0.01154 _diffrn_orient_matrix_UB_32 0.03301 _diffrn_orient_matrix_UB_33 0.02897 _cell_formula_units_Z 3 _exptl_crystal_density_diffrn 1.461 _exptl_crystal_density_method 'not measured' _exptl_special_details ; ? ; _chemical_formula_weight 602.139 _diffrn_radiation_type ' MoK\a' loop_ _symmetry_equiv_pos_as_xyz '+X,+Y,+Z' '-X,-Y,-Z' '-X+ 1/3,-Y+ 2/3,-Z+ 2/3' '+X+ 1/3,+Y+ 2/3,+Z+ 2/3' '+X+ 2/3,+Y+ 1/3,+Z+ 1/3' '-X+ 2/3,-Y+ 1/3,-Z+ 1/3' '-Y,+X-Y,+Z' '+Y,-X+Y,-Z' '+Y+ 1/3,-X+Y+ 2/3,-Z+ 2/3' '-Y+ 1/3,+X-Y+ 2/3,+Z+ 2/3' '-Y+ 2/3,+X-Y+ 1/3,+Z+ 1/3' '+Y+ 2/3,-X+Y+ 1/3,-Z+ 1/3' '-X+Y,-X,+Z' '+X-Y,+X,-Z' '+X-Y+ 1/3,+X+ 2/3,-Z+ 2/3' '-X+Y+ 1/3,-X+ 2/3,+Z+ 2/3' '-X+Y+ 2/3,-X+ 1/3,+Z+ 1/3' '+X-Y+ 2/3,+X+ 1/3,-Z+ 1/3' _symmetry_space_group_name_H-M 'R -3 ' _symmetry_cell_setting 'Hexagonal' _chemical_formula_moiety 'C12 H36 Al Cl3 O6 S6 ' _chemical_formula_sum 'C12 H36 Al Cl3 O6 S6 ' _chemical_name_systematic ; ? ; _cell_length_a 10.3765(6) _cell_length_b 10.3765(6) _cell_length_c 22.0208(12) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 120.00 _cell_volume 2053.4(2) _diffrn_reflns_number 2680 _diffrn_reflns_theta_max 29.98 _diffrn_reflns_theta_min 3.93 _diffrn_reflns_theta_full 29.98 _cell_measurement_reflns_used 1340 _cell_measurement_theta_min 2.952 _cell_measurement_theta_max 30.034 _diffrn_measurement_method 'CCD' _computing_cell_refinement 'HKL Scalepack (Otwinowski & Minor 1997)' _computing_structure_solution 'SIR97(Cascarano al.,Acta Cryst.,1996,A52,C-79)' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _exptl_absorpt_correction_type none _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Al' 'Al' 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _exptl_absorpt_coefficient_mu 0.849 _reflns_number_total 1340 _reflns_number_gt 1266 _reflns_threshold_expression >2sigma(I) _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0316P)^2^+2.3297P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_extinction_method SHELXL _refine_ls_extinction_coef 0.0018(3) _refine_ls_extinction_expression 'Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^' _refine_ls_number_reflns 1340 _refine_ls_number_parameters 44 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0270 _refine_ls_R_factor_gt 0.0256 _refine_ls_wR_factor_ref 0.0678 _refine_ls_wR_factor_gt 0.0668 _refine_ls_goodness_of_fit_ref 1.109 _refine_ls_restrained_S_all 1.109 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.0000 0.0000 0.0000 0.02766(17) Uani 1 6 d S . . Cl2 Cl 0.0000 0.0000 0.2509 0.03096(14) Uani 1 3 d S . . C1 C 0.24971(17) 0.24361(15) 0.12848(6) 0.0321(3) Uani 1 1 d . . . C2 C 0.30666(14) 0.37757(14) 0.01919(6) 0.0271(3) Uani 1 1 d . . . S S 0.23359(3) 0.38616(3) 0.090813(13) 0.01964(11) Uani 1 1 d . . . Al Al 0.3333 0.6667 0.1667 0.01667(17) Uani 1 6 d S . . O O 0.35982(9) 0.53114(9) 0.11850(4) 0.02161(18) Uani 1 1 d . . . H1A H 0.1855 0.1497 0.1093 0.039 Uiso 1 1 d R . . H1B H 0.2216 0.2394 0.1703 0.039 Uiso 1 1 d R . . H1C H 0.3508 0.2647 0.1262 0.039 Uiso 1 1 d R . . H2A H 0.3154 0.4569 -0.0061 0.032 Uiso 1 1 d R . . H2B H 0.2411 0.2837 0.0003 0.032 Uiso 1 1 d R . . H2C H 0.4030 0.3874 0.0246 0.032 Uiso 1 1 d R . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0216(3) 0.022 0.0398(4) 0.000 0.000 0.011 Cl2 0.0334(3) 0.033 0.0260(3) 0.000 0.000 0.017 C1 0.0406(7) 0.0220(6) 0.0334(7) 0.0055(5) 0.0013(5) 0.0154(5) C2 0.0277(6) 0.0240(6) 0.0246(6) -0.0024(4) 0.0027(4) 0.0094(5) S 0.01714(15) 0.01628(14) 0.02438(16) -0.00070(9) 0.00040(9) 0.00753(10) Al 0.0149(2) 0.0149(2) 0.0201(4) 0.000 0.000 0.00747(11) O 0.0181(4) 0.0184(4) 0.0278(4) -0.0051(3) -0.0010(3) 0.0088(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 S 1.7751(13) . ? C2 S 1.7715(12) . ? S O 1.5427(8) . ? Al O 1.8880(8) 3_565 ? Al O 1.8880(8) 15 ? Al O 1.8880(8) 2_665 ? Al O 1.8880(8) 14_455 ? Al O 1.8880(8) . ? Al O 1.8881(8) 13_565 ? C1 H1A 0.9600 . ? C1 H1B 0.9599 . ? C1 H1C 0.9601 . ? C2 H2A 0.9600 . ? C2 H2B 0.9599 . ? C2 H2C 0.9600 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O S C2 102.99(5) . . ? O S C1 103.89(6) . . ? C2 S C1 98.81(6) . . ? O Al O 180.0 3_565 15 ? O Al O 91.52(4) 3_565 2_665 ? O Al O 88.48(4) 15 2_665 ? O Al O 88.48(4) 3_565 14_455 ? O Al O 91.52(4) 15 14_455 ? O Al O 180.0 2_665 14_455 ? O Al O 91.52(4) 3_565 . ? O Al O 88.48(4) 15 . ? O Al O 91.52(4) 2_665 . ? O Al O 88.48(4) 14_455 . ? O Al O 88.48(4) 3_565 13_565 ? O Al O 91.52(4) 15 13_565 ? O Al O 88.48(4) 2_665 13_565 ? O Al O 91.52(4) 14_455 13_565 ? O Al O 180.0 . 13_565 ? S O Al 125.42(5) . . ? S C1 H1A 109.5 . . ? S C1 H1B 109.5 . . ? H1A C1 H1B 109.5 . . ? S C1 H1C 109.5 . . ? H1A C1 H1C 109.5 . . ? H1B C1 H1C 109.5 . . ? S C2 H2A 109.5 . . ? S C2 H2B 109.5 . . ? H2A C2 H2B 109.5 . . ? S C2 H2C 109.5 . . ? H2A C2 H2C 109.5 . . ? H2B C2 H2C 109.5 . . ? _diffrn_measured_fraction_theta_max 0.998 _diffrn_measured_fraction_theta_full 0.998 _refine_diff_density_max 0.495 _refine_diff_density_min -0.432 _refine_diff_density_rms 0.055 _publ_section_references ; Mackay, S., Gilmore, C. J.,Edwards, C., Stewart, N. & Shankland, K. (1999). maXus Computer Program for the Solution and Refinement of Crystal Structures. Bruker Nonius, The Netherlands, MacScience, Japan & The University of Glasgow. Johnson, C. K. (1976). ORTEP-II. A Fortran Thermal-Ellipsoid Plot Program. Report ORNL-5138. Oak Ridge National Laboratory, Oak Ridge, Tennessee, USA. Otwinowski, Z. and Minor, W, (1997). In Methods in Enzymology, 276, edited by C.W. Carter, Jr. & R.M. Sweet pp. 307-326, New York:Academic Press. LePage, Y. (1987). J. Appl. Cryst. 20, 264-269. Altomare, A., Burla, M.C., Camalli, M., Cascarano, G.L., Giacovazzo, C., Guagliardi, A., Moliterni, A.G.G & Spagna, R. (1999). J. Appl. Cryst. 32, 115-119. Sheldrick, G. M. (1997). SHELXL97. Program for the Refinement of Crystal Structures. University of G\"ottingen, Germany. ; # Intensity data loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma -12 12 -9 216.3 288.7 21.8 -12 12 -3 713.5 723.2 50.4 -12 12 0 1246.1 1293.7 76.9 -12 12 3 113.4 89.1 18.0 -12 12 9 116.0 76.0 17.6 -12 13 -4 938.1 1022.9 71.0 -12 13 -1 443.6 393.5 38.8 -12 13 2 203.5 451.8 24.9 -11 11 -13 4730.3 3689.2 215.2 -11 11 -10 57.7 3.8 9.2 -11 11 -7 5012.0 3646.3 184.9 -11 11 -4 20.6 14.4 5.7 -11 11 -1 2017.4 1318.7 67.7 -11 11 2 2033.2 1356.7 66.8 -11 11 5 1230.9 673.6 41.6 -11 11 8 17.4 167.5 6.9 -11 11 11 566.7 566.7 38.6 -11 11 14 2047.0 1177.3 122.0 -11 12 -11 616.3 417.8 41.3 -11 12 -8 714.6 780.7 37.3 -11 12 -5 815.3 579.4 40.7 -11 12 -2 17.8 28.1 7.6 -11 12 1 611.1 271.2 30.4 -11 12 4 710.9 547.6 36.1 -11 12 7 325.1 138.0 19.1 -11 12 10 46.0 44.7 11.3 -11 13 -6 547.6 438.3 45.8 -11 13 -3 2513.3 1539.1 108.5 -11 13 0 12.8 6.7 8.3 -11 13 3 1179.9 812.9 55.7 -11 13 6 669.8 273.6 38.0 -10 10 -14 3528.2 2723.7 157.6 -10 10 -11 556.8 623.9 27.0 -10 10 -5 4577.9 3709.0 100.2 -10 10 -2 166.2 32.2 5.6 -10 10 1 1103.0 803.4 23.7 -10 10 4 2714.6 2391.6 52.4 -10 10 7 291.3 242.0 9.5 -10 10 10 420.6 332.7 16.6 -10 10 13 1230.4 975.8 55.4 -10 10 16 253.9 185.2 16.9 -10 11 -15 2335.9 2086.4 123.5 -10 11 -12 7103.1 6514.9 308.4 -10 11 -9 1008.7 806.0 41.7 -10 11 -6 3385.4 2989.2 107.3 -10 11 -3 875.9 919.0 27.7 -10 11 0 9575.7 7343.7 218.7 -10 11 6 66.1 104.6 6.2 -10 11 12 6544.9 5285.3 240.7 -10 11 15 100.8 53.0 12.9 -10 12 -13 39.8 15.8 12.4 -10 12 -10 31.1 0.7 10.1 -10 12 -7 69.9 98.1 8.5 -10 12 -4 602.8 586.3 31.2 -10 12 -1 100.8 59.7 10.0 -10 12 2 22.4 30.9 7.9 -10 12 5 58.6 93.5 9.4 -10 12 8 1740.9 1499.9 70.5 -10 12 11 24.7 76.0 8.8 -10 13 -11 51.9 33.2 13.3 -10 13 -8 2176.0 1707.1 125.1 -10 13 -5 193.7 175.0 18.7 -10 13 -2 549.2 676.1 30.8 -10 13 1 24.7 25.1 8.9 -10 13 4 4032.0 3810.9 166.7 -10 13 7 62.9 60.4 10.5 -10 13 10 188.7 187.7 15.2 -10 14 0 3258.2 2532.3 149.9 -9 9 -21 442.7 361.5 35.9 -9 9 -18 29.2 52.0 11.6 -9 9 -15 302.6 223.1 13.6 -9 9 -12 972.6 906.7 27.9 -9 9 -9 2775.3 2317.2 56.7 -9 9 -6 47.3 127.2 3.2 -9 9 -3 1514.0 1060.9 22.8 -9 9 0 272.8 327.9 6.2 -9 9 3 2227.8 1649.3 29.7 -9 9 6 3555.7 2200.8 48.3 -9 9 9 469.5 402.3 10.6 -9 9 12 103.7 182.9 7.1 -9 9 15 342.5 452.4 16.8 -9 9 18 1041.8 672.5 48.2 -9 10 -19 45.0 106.3 17.7 -9 10 -16 734.1 804.1 53.4 -9 10 -13 270.9 423.4 15.2 -9 10 -10 1508.0 1235.1 43.9 -9 10 -4 107.1 162.2 5.6 -9 10 -1 1349.2 1036.0 28.2 -9 10 2 275.5 89.6 9.7 -9 10 5 794.7 367.7 16.1 -9 10 8 2217.2 1931.6 50.0 -9 10 11 165.5 88.4 8.1 -9 10 17 107.0 38.2 11.6 -9 10 20 255.3 266.6 19.0 -9 11 -17 1333.9 1011.7 95.9 -9 11 -11 2286.2 1801.4 96.2 -9 11 -8 246.0 263.5 12.3 -9 11 -5 1509.7 1187.7 40.7 -9 11 -2 886.2 446.4 26.6 -9 11 1 811.0 425.4 23.5 -9 11 4 431.3 515.9 14.2 -9 11 7 1255.0 1099.2 36.6 -9 11 10 1647.2 896.7 56.7 -9 11 13 617.7 739.5 25.7 -9 11 16 410.1 335.7 23.8 -9 12 -15 338.8 315.9 33.9 -9 12 -12 559.1 389.8 42.6 -9 12 -9 853.3 540.8 58.3 -9 12 -6 728.5 238.4 38.8 -9 12 -3 2807.0 1969.4 99.2 -9 12 0 238.4 233.2 14.9 -9 12 3 1651.8 1025.7 61.3 -9 12 6 464.7 287.0 22.0 -9 12 9 1383.8 938.9 57.1 -9 12 12 777.1 791.7 33.9 -9 12 15 3135.8 2471.6 133.7 -9 13 -10 194.1 290.8 23.5 -9 13 -7 2211.3 1558.3 135.3 -9 13 -4 909.6 893.1 53.1 -9 13 -1 2338.6 1875.2 106.7 -9 13 2 674.8 345.7 35.2 -9 13 5 182.8 128.7 15.3 -9 13 8 21.2 7.9 8.7 -9 13 11 100.4 60.8 12.6 -9 14 -5 1691.8 964.0 118.3 -9 14 -2 2994.3 1835.7 150.6 -9 14 1 5282.5 4341.1 236.5 -9 14 4 150.0 218.3 15.7 -9 14 7 3449.9 2498.3 160.0 -8 8 -22 1351.8 1548.3 146.3 -8 8 -19 127.7 198.0 13.3 -8 8 -16 200.6 318.1 9.9 -8 8 -13 20.7 21.6 4.4 -8 8 -10 1409.9 977.7 25.2 -8 8 -7 42.7 87.1 3.4 -8 8 -4 242.5 158.5 5.2 -8 8 -1 2600.8 2187.6 28.5 -8 8 2 2352.1 1145.9 24.4 -8 8 5 6088.7 5162.4 57.8 -8 8 8 2687.7 2760.0 32.6 -8 8 11 2517.5 1945.4 33.6 -8 8 14 15.5 0.1 3.9 -8 8 17 1269.4 823.2 35.8 -8 8 20 1511.8 1369.3 61.4 -8 8 23 1265.9 1196.8 56.6 -8 9 -20 3134.2 2658.6 228.3 -8 9 -17 1838.4 1708.2 70.7 -8 9 -14 2784.1 2406.8 65.6 -8 9 -11 2952.4 2465.8 64.5 -8 9 -8 20701.9 17267.5 277.3 -8 9 -5 398.0 270.8 11.7 -8 9 -2 12865.9 9710.1 172.7 -8 9 1 273.2 210.6 5.8 -8 9 4 22728.6 17658.2 256.9 -8 9 7 903.3 530.7 16.4 -8 9 10 4155.3 4014.3 73.8 -8 9 13 1604.4 1505.1 39.2 -8 9 16 8806.0 7515.4 285.7 -8 9 19 1606.7 1340.6 70.0 -8 9 22 713.5 527.7 35.4 -8 10 -18 805.4 601.8 56.7 -8 10 -15 317.3 256.1 17.4 -8 10 -12 1718.9 1905.9 53.3 -8 10 -9 18.9 13.4 4.6 -8 10 -6 1014.4 463.9 26.7 -8 10 -3 214.2 132.0 7.8 -8 10 3 8.7 1.4 4.2 -8 10 6 308.4 135.2 9.3 -8 10 9 1705.6 1566.5 34.6 -8 10 12 423.5 366.7 14.1 -8 10 15 19.3 24.1 6.9 -8 10 21 61.2 42.8 11.7 -8 11 -19 1289.9 1024.7 93.3 -8 11 -16 4797.8 4564.5 279.6 -8 11 -13 1539.1 905.3 77.3 -8 11 -10 2796.7 2542.8 107.1 -8 11 -7 125.8 100.2 10.0 -8 11 -4 16413.1 11785.4 329.2 -8 11 -1 26.4 52.9 5.4 -8 11 2 3903.6 3686.4 76.8 -8 11 5 390.8 303.6 14.1 -8 11 8 11343.9 9165.6 236.5 -8 11 11 818.1 688.7 31.6 -8 11 14 1812.2 1754.4 69.0 -8 11 17 919.4 817.9 44.5 -8 12 -14 47.5 57.9 15.8 -8 12 -11 996.7 843.6 67.9 -8 12 -8 1483.7 1569.6 86.1 -8 12 -5 822.9 580.5 37.3 -8 12 -2 1053.5 679.6 40.8 -8 12 1 575.4 508.4 24.5 -8 12 4 532.7 493.1 24.8 -8 12 7 17.9 39.7 8.1 -8 12 10 14.8 0.1 7.4 -8 12 13 255.3 163.6 15.8 -8 12 16 202.9 352.6 16.7 -8 13 -12 1228.4 966.9 89.1 -8 13 -9 694.6 680.4 50.8 -8 13 -6 982.2 1037.9 66.1 -8 13 -3 194.1 172.5 22.2 -8 13 0 7258.2 6512.2 287.9 -8 13 3 1054.9 1108.9 53.1 -8 13 6 862.3 1042.5 42.2 -8 13 9 897.1 926.7 41.0 -8 13 12 335.3 272.1 20.2 -8 14 -7 679.6 668.3 54.2 -8 14 -4 2678.3 2080.2 178.5 -8 14 -1 725.4 585.5 45.9 -8 14 2 358.7 287.5 23.8 -8 14 5 1046.3 860.4 55.1 -8 14 8 40.4 87.8 11.7 -7 7 -20 1743.3 1850.4 56.0 -7 7 -14 584.5 454.7 14.2 -7 7 -11 833.4 450.6 14.1 -7 7 -8 1490.7 1672.5 20.0 -7 7 -5 44.8 21.8 3.5 -7 7 -2 2689.2 846.0 29.7 -7 7 1 2635.1 1340.9 25.1 -7 7 4 2318.3 1497.6 23.5 -7 7 7 720.2 433.0 10.1 -7 7 10 587.5 509.6 8.5 -7 7 13 358.7 434.3 9.0 -7 7 16 1787.3 1928.0 43.7 -7 7 19 12.6 5.9 4.7 -7 7 22 103.1 130.7 9.1 -7 7 25 91.4 81.8 11.5 -7 8 -24 826.1 918.5 105.2 -7 8 -21 1676.3 1485.7 81.8 -7 8 -18 46.7 67.5 5.5 -7 8 -15 1978.7 2014.7 42.2 -7 8 -12 802.2 823.3 17.0 -7 8 -9 593.3 460.7 11.9 -7 8 -6 2632.3 2039.2 34.4 -7 8 -3 1701.5 1695.7 25.3 -7 8 0 4112.2 3970.8 42.1 -7 8 3 35.5 66.8 2.3 -7 8 6 3035.7 2555.9 32.3 -7 8 9 575.1 805.1 10.7 -7 8 12 100.8 65.7 3.9 -7 8 18 498.1 585.6 18.7 -7 8 21 363.7 376.3 20.5 -7 8 24 13.1 0.0 8.4 -7 9 -22 44.8 61.1 14.4 -7 9 -19 456.6 558.3 46.6 -7 9 -16 13.3 34.0 5.8 -7 9 -13 48.3 9.7 4.3 -7 9 -10 1266.4 801.8 23.4 -7 9 -7 10.1 20.5 3.7 -7 9 -4 2047.7 1862.4 30.3 -7 9 -1 19.0 9.3 3.3 -7 9 2 1629.2 1244.2 22.5 -7 9 5 34.3 6.2 3.4 -7 9 8 816.5 726.1 15.6 -7 9 11 212.4 283.4 8.1 -7 9 14 709.7 432.0 19.3 -7 9 17 395.0 323.1 18.6 -7 9 20 100.6 183.3 11.2 -7 9 23 368.2 354.1 23.6 -7 10 -20 38.5 29.5 15.4 -7 10 -14 891.2 755.8 31.7 -7 10 -11 113.1 174.4 7.3 -7 10 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