# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 4(C14H12O8).3(CH4O) in P-1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 487.02 _exptl_crystal_F_000 1388.00 _reflns_d_resolution_high 0.8409 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 12.4830 _cell_length_b 12.6558 _cell_length_c 19.0259 _cell_angle_alpha 94.608 _cell_angle_beta 100.871 _cell_angle_gamma 98.399 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 721.98 932.75 166.50 o 2 0 0 20603.77 20743.69 649.56 o 3 0 0 17.73 39.22 9.16 o 4 0 0 777.34 712.07 32.05 o 5 0 0 1098.50 1061.87 45.03 o 6 0 0 88.45 107.14 16.72 o 7 0 0 133.03 163.32 21.76 o 8 0 0 179.39 182.12 24.36 o 9 0 0 23.53 26.52 19.47 o 10 0 0 699.96 630.22 64.12 o 11 0 0 235.29 285.99 43.81 o 12 0 0 46.60 36.45 49.07 o 13 0 0 29.38 91.60 57.49 o 14 0 0 10.05 -9.81 56.55 o -14 1 0 196.67 307.99 81.09 o -13 1 0 87.51 98.85 57.95 o -12 1 0 67.01 41.52 31.33 o -11 1 0 284.61 206.47 39.25 o -10 1 0 16.09 43.82 25.49 o -9 1 0 7.00 14.40 19.12 o -8 1 0 48.93 42.81 17.40 o -7 1 0 532.59 616.54 51.92 o -6 1 0 2198.25 2200.29 83.02 o -5 1 0 4454.62 4492.46 151.81 o -4 1 0 178.27 166.89 15.93 o -3 1 0 6343.58 5835.93 188.79 o -2 1 0 24095.72 24784.79 774.94 o -1 1 0 2452.11 2236.55 119.18 o 0 1 0 1379.27 1145.03 65.90 o 1 1 0 149.16 171.39 10.43 o 2 1 0 447.00 409.42 18.83 o 3 1 0 63.09 62.11 12.02 o 4 1 0 1661.37 1475.99 56.24 o 5 1 0 434.33 453.44 28.46 o 6 1 0 3638.89 3586.84 125.90 o 7 1 0 239.06 317.88 33.73 o 8 1 0 32.01 15.29 16.29 o 9 1 0 180.67 178.33 28.01 o 10 1 0 164.39 137.79 35.57 o 11 1 0 0.04 24.77 46.97 o 12 1 0 7.82 -59.12 45.33 o 13 1 0 23.24 44.17 54.21 o 14 1 0 6.19 28.98 56.78 o -14 2 0 0.34 8.65 56.32 o -13 2 0 104.13 138.96 41.65 o -12 2 0 272.67 343.33 49.82 o -11 2 0 390.37 441.69 52.98 o -10 2 0 185.28 200.14 36.81 o -9 2 0 123.71 114.75 23.90 o -8 2 0 29.77 60.37 18.20 o -7 2 0 0.00 -6.71 11.81 o -6 2 0 3066.49 3085.41 110.42 o -5 2 0 1382.16 1363.98 54.24 o -4 2 0 1855.14 1856.30 67.60 o -3 2 0 1081.92 953.36 37.46 o -2 2 0 944.85 893.10 42.20 o -1 2 0 180.15 150.02 18.69 o 0 2 0 1824.49 1805.64 105.39 o 1 2 0 175.29 145.38 12.15 o 2 2 0 3127.52 2992.39 117.25 o 3 2 0 5632.62 5817.26 189.50 o 4 2 0 138.25 130.57 16.62 o 5 2 0 2205.65 2168.98 81.13 o 6 2 0 1322.98 1386.76 58.36 o 7 2 0 807.53 782.54 44.53 o 8 2 0 43.86 57.69 23.66 o 9 2 0 109.64 91.41 41.95 o 10 2 0 6.05 29.21 43.93 o 11 2 0 2.56 46.03 48.37 o 12 2 0 0.06 62.39 54.45 o 13 2 0 0.23 50.24 59.82 o -14 3 0 32.10 -8.16 37.58 o -13 3 0 167.38 196.40 44.51 o -12 3 0 687.19 720.29 100.37 o -11 3 0 489.63 397.61 59.35 o -10 3 0 566.76 633.85 97.21 o -9 3 0 47.14 62.35 24.37 o -8 3 0 44.42 59.46 18.59 o -7 3 0 576.01 639.53 38.87 o -6 3 0 151.37 139.36 18.05 o -5 3 0 213.71 269.01 21.44 o -4 3 0 1520.51 1212.87 60.89 o -3 3 0 310.01 324.02 26.60 o -2 3 0 1.73 33.18 18.23 o -1 3 0 437.83 498.44 42.53 o 0 3 0 8216.56 7424.71 414.31 o 1 3 0 229.83 188.47 29.56 o 2 3 0 399.81 392.61 24.02 o 3 3 0 45.38 60.98 12.74 o 4 3 0 830.62 772.32 40.79 o 5 3 0 6.64 10.61 14.13 o 6 3 0 1042.46 917.47 80.39 o 7 3 0 278.66 307.75 50.36 o 8 3 0 162.74 186.52 31.30 o 9 3 0 2692.57 2303.15 156.33 o 10 3 0 2824.63 2619.32 176.19 o 11 3 0 16.56 13.09 51.18 o -14 4 0 25.03 60.17 39.09 o -13 4 0 24.80 83.60 36.26 o -12 4 0 29.37 45.94 31.61 o -11 4 0 331.23 246.38 42.54 o -10 4 0 826.87 886.29 72.26 o -9 4 0 50.89 27.63 21.09 o -8 4 0 28.55 59.97 24.19 o -7 4 0 86.72 95.58 17.57 o -6 4 0 182.83 195.64 20.16 o -5 4 0 715.38 835.00 54.16 o -4 4 0 3226.90 3406.95 159.37 o -3 4 0 879.52 793.11 64.26 o -2 4 0 1625.00 1421.01 95.34 o -1 4 0 423.03 421.32 42.06 o 0 4 0 1.23 45.33 17.53 o 1 4 0 0.07 19.80 9.26 o 2 4 0 706.89 677.29 34.88 o 3 4 0 2339.18 2242.19 93.77 o 4 4 0 1997.29 2426.11 102.45 o 5 4 0 168.14 234.83 25.19 o 6 4 0 1427.12 1445.46 71.04 o 7 4 0 336.57 482.92 89.73 o 8 4 0 42.37 -28.51 25.70 o 9 4 0 100.46 103.75 43.46 o 10 4 0 5.06 46.97 44.87 o -14 5 0 11.01 59.95 51.88 o -13 5 0 4.26 41.36 34.42 o -12 5 0 29.89 20.76 30.73 o -11 5 0 1527.06 1321.85 141.84 o -10 5 0 99.60 86.64 29.14 o -9 5 0 1.21 -3.78 22.29 o -8 5 0 268.17 281.35 60.17 o -7 5 0 425.83 456.50 46.21 o -6 5 0 707.37 628.04 45.03 o -5 5 0 1343.63 1359.78 97.44 o -4 5 0 8.38 -13.09 19.63 o -3 5 0 4947.52 4983.69 295.37 o -2 5 0 94.89 135.77 28.51 o -1 5 0 24.06 24.30 18.69 o 0 5 0 1640.31 1778.30 115.20 o 1 5 0 1631.85 1625.68 71.73 o 2 5 0 58.73 47.37 12.74 o 3 5 0 606.72 605.73 43.35 o 4 5 0 285.65 307.21 26.51 o 5 5 0 1.28 -7.02 13.57 o 6 5 0 33.66 52.07 33.07 o 7 5 0 57.73 113.57 34.82 o 8 5 0 828.45 804.09 79.68 o -14 6 0 2.05 49.71 41.47 o -13 6 0 38.94 62.44 38.49 o -12 6 0 234.10 194.28 45.01 o -11 6 0 71.85 77.69 34.17 o -10 6 0 43.14 80.38 32.71 o -9 6 0 20.76 57.77 26.64 o -8 6 0 105.20 127.69 29.66 o -7 6 0 2.14 20.98 20.77 o -6 6 0 98.99 123.15 41.36 o -5 6 0 292.98 327.15 51.88 o -4 6 0 415.23 596.12 67.53 o -3 6 0 1179.89 1125.64 89.50 o -2 6 0 387.81 386.51 49.07 o -1 6 0 3293.09 3529.50 215.69 o 0 6 0 885.03 923.03 71.97 o 1 6 0 618.03 658.33 38.93 o 2 6 0 366.81 392.98 38.67 o 3 6 0 59.53 138.31 44.75 o 4 6 0 905.92 961.67 51.11 o 5 6 0 69.73 77.81 19.66 o 6 6 0 32.48 42.53 30.85 o 7 6 0 51.26 25.24 34.12 o -13 7 0 42.17 26.17 46.97 o -12 7 0 0.08 44.55 36.10 o -11 7 0 39.88 29.28 29.41 o -10 7 0 141.93 171.99 53.75 o -9 7 0 1.82 -16.36 28.74 o -8 7 0 172.48 71.51 40.19 o -7 7 0 156.23 153.29 47.44 o -5 7 0 4.76 23.84 29.91 o -4 7 0 239.35 232.04 45.10 o -3 7 0 717.34 682.58 73.84 o -2 7 0 926.85 866.95 80.15 o -1 7 0 82.46 72.21 28.28 o 0 7 0 408.63 431.14 53.51 o 1 7 0 18.75 28.71 15.03 o 2 7 0 1037.68 1087.01 56.01 o 3 7 0 353.20 371.73 32.07 o 4 7 0 303.80 312.06 31.14 o 5 7 0 711.28 609.20 60.99 o -13 8 0 4.45 2.34 46.74 o -12 8 0 45.37 121.98 57.02 o -11 8 0 52.98 127.12 57.49 o -10 8 0 156.60 196.06 57.72 o -9 8 0 36.86 100.01 47.67 o -8 8 0 31.17 18.93 33.42 o -7 8 0 189.89 155.63 51.88 o -6 8 0 285.91 233.68 54.21 o -5 8 0 14.95 50.01 34.82 o -4 8 0 87.03 121.51 40.43 o -3 8 0 10.55 -13.55 27.81 o -2 8 0 20.37 53.51 28.28 o -1 8 0 498.85 792.41 78.75 o 0 8 0 31.17 15.94 15.36 o 1 8 0 58.62 142.87 24.38 o 2 8 0 1480.22 1399.51 69.76 o 3 8 0 499.69 498.04 57.25 o -12 9 0 61.44 3.27 49.07 o -11 9 0 117.79 82.49 52.34 o -10 9 0 0.68 -36.22 35.52 o -9 9 0 721.08 699.64 107.96 o -8 9 0 17.70 26.41 36.69 o -7 9 0 520.82 579.99 94.64 o -6 9 0 56.80 73.14 44.40 o -5 9 0 206.91 225.50 54.45 o -4 9 0 474.75 487.22 74.31 o -3 9 0 18.47 54.68 34.82 o -2 9 0 327.29 423.66 64.26 o -1 9 0 220.13 347.01 56.08 o 0 9 0 0.84 51.29 20.36 o 1 9 0 76.78 66.95 28.39 o 2 9 0 237.98 290.57 50.36 o -12 10 0 94.29 205.17 68.00 o -11 10 0 8.81 32.01 52.11 o -10 10 0 143.73 222.00 74.78 o -9 10 0 418.81 513.63 98.85 o -8 10 0 107.57 188.58 62.39 o -7 10 0 278.52 447.26 87.86 o -6 10 0 3.71 7.24 37.86 o -5 10 0 0.01 -52.23 34.82 o -4 10 0 340.17 353.79 67.07 o -3 10 0 23.13 -14.72 35.99 o -2 10 0 1.63 42.30 37.62 o -1 10 0 249.29 269.20 53.98 o 0 10 0 59.01 85.41 25.22 o 1 10 0 69.86 19.86 35.29 o -11 11 0 0.08 29.44 57.72 o -10 11 0 24.19 2.34 47.20 o -9 11 0 13.96 68.94 51.88 o -8 11 0 354.86 431.84 93.00 o -7 11 0 3.74 -7.24 40.43 o -6 11 0 68.80 56.78 45.33 o -5 11 0 201.14 150.49 54.45 o -4 11 0 0.12 -12.15 40.66 o -3 11 0 59.91 84.12 47.67 o -2 11 0 51.82 37.62 40.66 o -1 11 0 114.24 89.03 46.27 o 0 11 0 4.03 2.57 36.45 o -10 12 0 23.80 44.87 55.62 o -9 12 0 0.02 57.95 53.98 o -8 12 0 31.70 38.32 58.19 o -7 12 0 278.82 247.93 78.28 o -6 12 0 661.04 609.67 96.28 o -5 12 0 30.88 43.93 49.54 o -4 12 0 19.96 -10.98 41.59 o -3 12 0 8.28 -40.19 39.73 o -2 12 0 6.02 11.45 44.87 o -1 12 0 14.15 75.95 46.03 o -9 13 0 56.25 198.16 82.72 o -8 13 0 5.32 103.99 64.26 o -7 13 0 153.66 282.52 85.76 o -5 13 0 80.01 97.44 57.72 o -4 13 0 96.60 266.16 72.21 o -3 13 0 187.87 229.47 66.37 o -2 13 0 10.90 -26.64 45.10 o -7 14 0 2.61 -64.03 64.73 o -6 14 0 28.83 47.20 73.38 o -5 14 0 0.03 -35.05 49.77 o -4 14 0 198.15 347.95 82.96 o -3 14 0 33.88 24.07 56.32 o 3 -15 1 15.51 -27.34 57.72 o 2 -14 1 377.75 321.78 80.62 o 3 -14 1 1.43 -44.63 46.50 o 4 -14 1 293.62 360.10 82.26 o 5 -14 1 24.63 121.28 67.53 o 6 -14 1 45.75 112.63 62.63 o 7 -14 1 12.12 144.65 79.22 o 1 -13 1 534.82 489.56 85.53 o 2 -13 1 1.17 -32.72 45.57 o 3 -13 1 52.36 57.25 55.38 o 4 -13 1 184.81 87.63 55.62 o 5 -13 1 31.36 111.00 58.65 o 6 -13 1 15.44 -31.78 52.11 o 8 -13 1 0.17 -32.72 50.94 o 9 -13 1 27.21 73.14 64.96 o 0 -12 1 37.94 65.20 49.54 o 1 -12 1 8.20 12.85 43.70 o 2 -12 1 201.90 157.03 55.62 o 3 -12 1 547.18 593.08 93.71 o 4 -12 1 89.13 111.23 51.41 o 5 -12 1 33.41 83.89 48.61 o 6 -12 1 4.53 27.57 45.80 o 8 -12 1 195.95 293.74 89.27 o 9 -12 1 3.70 68.94 61.93 o 10 -12 1 25.61 -3.04 56.78 o -1 -11 1 16.15 58.89 40.43 o 0 -11 1 180.50 254.71 58.65 o 1 -11 1 114.41 109.83 49.54 o 2 -11 1 983.01 1093.15 113.57 o 3 -11 1 58.66 97.91 46.27 o 4 -11 1 177.39 105.39 49.07 o 5 -11 1 10.63 13.55 41.59 o 6 -11 1 686.84 597.52 93.24 o 7 -11 1 485.46 422.26 82.26 o 8 -11 1 1.35 24.77 54.91 o 9 -11 1 5.61 68.00 57.02 o 10 -11 1 0.41 102.35 57.49 o 11 -11 1 8.99 85.99 61.93 o -2 -10 1 104.56 160.77 46.27 o -1 -10 1 492.11 635.61 81.32 o 0 -10 1 16.89 70.80 37.86 o 1 -10 1 19.78 -21.26 31.78 o 2 -10 1 30.28 39.49 37.39 o 3 -10 1 7.83 13.79 35.52 o 4 -10 1 216.22 223.63 55.38 o 5 -10 1 6.44 -39.49 36.22 o 6 -10 1 520.45 512.93 83.89 o 7 -10 1 990.08 814.61 106.56 o 8 -10 1 2265.53 2089.80 201.67 o 9 -10 1 1.52 -12.85 43.70 o 10 -10 1 50.84 -9.11 42.06 o 11 -10 1 0.23 15.42 52.11 o 12 -10 1 0.77 53.98 52.81 o -3 -9 1 1.64 15.89 29.91 o -2 -9 1 12.48 3.97 28.28 o -1 -9 1 21.75 27.33 23.48 o 0 -9 1 180.15 273.11 46.03 o 1 -9 1 535.31 567.84 74.08 o 2 -9 1 1791.06 1599.54 125.02 o 3 -9 1 585.85 596.12 79.22 o 4 -9 1 1224.61 1159.52 113.10 o 5 -9 1 508.23 570.88 82.02 o 6 -9 1 120.57 91.84 47.67 o 8 -9 1 816.69 756.19 111.23 o 9 -9 1 279.34 268.50 71.51 o 10 -9 1 5.01 -28.74 40.89 o 11 -9 1 8.90 6.08 45.33 o 12 -9 1 6.75 37.39 51.64 o -4 -8 1 69.24 59.82 32.01 o -3 -8 1 65.10 89.27 34.58 o -2 -8 1 130.49 105.27 20.87 o -1 -8 1 183.20 253.99 44.87 o 0 -8 1 400.42 501.94 63.09 o 1 -8 1 92.00 124.55 37.62 o 2 -8 1 1667.10 1956.60 140.68 o 3 -8 1 362.84 388.61 60.06 o 4 -8 1 1467.36 1458.86 117.54 o 5 -8 1 0.42 -7.24 28.98 o 6 -8 1 121.52 181.80 52.11 o 8 -8 1 123.56 140.91 50.71 o 9 -8 1 22.66 -23.13 30.14 o 10 -8 1 199.16 110.53 54.21 o 11 -8 1 0.00 18.93 40.89 o 12 -8 1 67.11 132.73 58.65 o 13 -8 1 29.20 69.40 53.05 o -5 -7 1 69.09 96.74 34.58 o -4 -7 1 117.20 124.38 22.73 o -3 -7 1 1456.34 1590.58 74.80 o -2 -7 1 1182.59 1129.65 57.29 o -1 -7 1 0.84 14.43 12.74 o 0 -7 1 218.64 230.88 41.13 o 1 -7 1 129.03 138.34 35.05 o 2 -7 1 99.26 144.41 36.69 o 3 -7 1 239.31 249.34 45.80 o 4 -7 1 646.54 729.78 80.85 o 5 -7 1 192.61 169.89 42.53 o 6 -7 1 306.16 229.94 55.85 o 7 -7 1 491.16 531.15 81.55 o 8 -7 1 17.17 27.89 24.46 o 9 -7 1 27.73 26.96 53.86 o 10 -7 1 1.07 -5.32 35.87 o 11 -7 1 45.94 35.06 29.99 o 12 -7 1 131.41 97.84 38.85 o 13 -7 1 46.49 17.16 54.68 o -6 -6 1 505.17 564.45 42.48 o -5 -6 1 20.17 37.39 23.95 o -4 -6 1 924.57 840.46 97.91 o -3 -6 1 290.02 271.81 29.79 o -2 -6 1 430.18 445.25 31.27 o -1 -6 1 668.96 631.79 37.27 o 0 -6 1 75.53 65.20 25.24 o 1 -6 1 1483.17 1390.86 99.78 o 2 -6 1 921.38 994.77 80.15 o 3 -6 1 5084.31 5287.71 316.40 o 4 -6 1 25.65 21.50 22.20 o 5 -6 1 1042.81 1124.89 77.46 o 6 -6 1 1212.61 1146.86 66.05 o 7 -6 1 477.70 446.42 47.98 o 8 -6 1 30.93 20.01 21.79 o 9 -6 1 0.06 0.26 21.59 o 10 -6 1 3.69 -5.47 23.46 o 11 -6 1 209.06 156.12 41.50 o 12 -6 1 199.23 173.52 43.31 o 13 -6 1 1.44 -15.19 73.38 o 14 -6 1 31.06 39.28 39.76 o -8 -5 1 86.84 66.83 35.52 o -7 -5 1 45.35 78.94 23.04 o -6 -5 1 222.12 253.40 29.47 o -5 -5 1 121.95 171.42 32.36 o -4 -5 1 6.25 1.78 12.35 o -3 -5 1 4497.91 4977.27 197.34 o -2 -5 1 542.20 605.50 34.11 o -1 -5 1 16.15 16.21 13.79 o 0 -5 1 919.76 1043.38 75.95 o 1 -5 1 256.92 264.06 37.62 o 2 -5 1 701.96 740.30 67.30 o 3 -5 1 0.02 47.90 23.13 o 4 -5 1 288.07 322.83 32.49 o 5 -5 1 554.25 519.12 43.22 o 6 -5 1 43.11 92.98 24.50 o 7 -5 1 875.63 822.07 62.68 o 8 -5 1 273.33 359.18 57.02 o 9 -5 1 1052.20 985.82 76.16 o 10 -5 1 124.56 119.04 33.51 o 11 -5 1 116.97 164.57 40.19 o 12 -5 1 57.19 102.66 62.28 o 13 -5 1 55.71 66.37 38.21 o 14 -5 1 126.62 81.44 43.52 o -9 -4 1 20.37 3.51 31.31 o -8 -4 1 72.45 51.69 36.57 o -7 -4 1 1144.63 1168.76 127.12 o -6 -4 1 417.36 472.91 44.05 o -5 -4 1 10748.03 11424.07 438.47 o -4 -4 1 5015.08 4895.25 193.41 o -3 -4 1 2051.48 1971.12 83.35 o -2 -4 1 1193.58 1122.67 50.77 o -1 -4 1 431.58 397.19 24.40 o 0 -4 1 138.85 159.37 26.87 o 1 -4 1 17.24 57.95 19.86 o 2 -4 1 3354.99 3278.76 197.93 o 3 -4 1 4.04 0.50 10.89 o 4 -4 1 590.64 808.07 48.99 o 5 -4 1 15711.40 16765.72 533.46 o 6 -4 1 3378.45 3301.15 118.23 o 7 -4 1 18.52 49.23 20.51 o 8 -4 1 196.08 168.05 33.11 o 9 -4 1 14.05 25.93 22.52 o 10 -4 1 18.08 11.07 22.30 o 11 -4 1 20.33 26.54 26.77 o 12 -4 1 0.17 39.20 30.37 o 13 -4 1 26.39 -2.51 51.18 o 14 -4 1 15.94 53.81 35.62 o -11 -3 1 91.35 114.97 52.58 o -10 -3 1 4.95 -20.33 39.73 o -9 -3 1 294.83 298.37 81.79 o -8 -3 1 0.04 33.81 19.57 o -7 -3 1 18.54 -7.70 14.64 o -6 -3 1 33.92 56.23 16.27 o -5 -3 1 282.18 407.46 55.94 o -4 -3 1 408.47 435.98 26.53 o -3 -3 1 461.70 408.79 27.41 o -2 -3 1 3330.23 3060.75 103.45 o -1 -3 1 87.57 123.39 25.59 o 0 -3 1 47.97 47.90 17.99 o 1 -3 1 250.10 269.20 32.48 o 2 -3 1 6724.23 6163.89 239.11 o 3 -3 1 387.59 380.43 28.53 o 4 -3 1 6.89 32.23 8.50 o 5 -3 1 45.55 48.79 11.25 o 6 -3 1 149.66 167.93 29.28 o 7 -3 1 34.46 43.51 15.17 o 8 -3 1 13.00 4.51 19.42 o 9 -3 1 17.63 16.40 20.70 o 10 -3 1 495.45 473.23 82.14 o 11 -3 1 427.94 399.77 60.52 o 12 -3 1 677.05 732.10 127.36 o 13 -3 1 25.98 18.61 34.56 o 14 -3 1 10.70 57.49 66.13 o -12 -2 1 105.08 38.09 51.41 o -11 -2 1 119.90 231.81 60.99 o -10 -2 1 312.00 358.95 46.67 o -9 -2 1 0.07 -10.23 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