# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_I _shelx_title ' 15 in C2/c Zn(C7H2NO5)3H2O¡¤H2O¡¤0.25MeCN' _shelx_refln_list_code 4 _shelx_F_calc_maximum 463.77 _exptl_crystal_F_000 1332.00 _reflns_d_resolution_high 0.8407 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 14.6504 _cell_length_b 7.0380 _cell_length_c 22.6423 _cell_angle_alpha 90.000 _cell_angle_beta 91.866 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 38755.56 46169.45 2313.03 o 4 0 0 82993.02 80840.78 4050.27 o 6 0 0 3389.78 2749.33 148.64 o 8 0 0 15185.38 15166.94 773.67 o 10 0 0 2862.10 3058.10 172.55 o 12 0 0 4750.89 4608.72 254.14 o 14 0 0 2837.01 2808.18 167.86 o 16 0 0 1098.50 1060.16 88.62 o 1 1 0 1288.21 1720.79 58.37 o 3 1 0 8128.93 8824.44 315.85 o 5 1 0 45.81 65.76 12.19 o 7 1 0 224.27 228.82 18.47 o 9 1 0 584.14 652.16 36.11 o 11 1 0 463.19 569.87 38.05 o 13 1 0 3858.19 4180.20 165.92 o 15 1 0 649.81 696.94 49.38 o 17 1 0 75.71 78.94 29.40 o 0 2 0 3590.41 3928.33 142.90 o 2 2 0 215086.53 146766.31 4241.66 o 4 2 0 13816.45 15339.50 387.58 o 6 2 0 54681.05 52183.73 1853.22 o 8 2 0 23823.36 26133.18 934.75 o 10 2 0 16176.91 16605.66 600.44 o 12 2 0 375.05 327.24 40.68 o 14 2 0 226.08 214.33 29.11 o 16 2 0 1986.62 2117.51 146.76 o 1 3 0 289.15 347.01 13.77 o 3 3 0 4070.94 4368.83 113.97 o 5 3 0 2990.39 3304.90 88.46 o 7 3 0 792.56 839.91 33.55 o 9 3 0 3826.57 3886.35 122.57 o 11 3 0 637.58 597.30 41.77 o 13 3 0 86.14 65.41 42.67 o 15 3 0 41.54 -30.48 30.48 o 0 4 0 38670.70 33331.93 1186.39 o 2 4 0 23235.10 23855.18 602.09 o 4 4 0 61863.34 55624.45 1614.92 o 6 4 0 6518.09 7315.12 221.67 o 8 4 0 6085.52 6002.29 228.28 o 10 4 0 122.93 73.20 25.17 o 12 4 0 1982.05 1980.95 93.99 o 14 4 0 181.17 198.34 59.55 o 1 5 0 313.49 301.00 24.69 o 3 5 0 118.72 119.92 17.73 o 5 5 0 835.57 834.23 37.85 o 7 5 0 3.12 18.78 15.70 o 9 5 0 747.03 756.97 49.83 o 11 5 0 16.01 17.22 66.35 o 13 5 0 182.96 219.21 50.64 o 0 6 0 5064.96 6005.77 323.06 o 2 6 0 6248.39 4926.56 190.57 o 4 6 0 6449.75 7007.01 264.88 o 6 6 0 14981.30 13841.99 414.32 o 8 6 0 39.26 99.46 39.39 o 10 6 0 1917.60 1648.94 86.51 o 12 6 0 384.27 423.03 104.80 o 1 7 0 1106.66 1039.39 58.13 o 3 7 0 370.26 318.42 35.07 o 5 7 0 514.98 527.39 46.06 o 7 7 0 448.46 496.61 45.66 o 9 7 0 46.91 -2.34 39.39 o 0 8 0 2633.75 2327.57 150.98 o 2 8 0 2249.63 2498.22 113.61 o 4 8 0 1905.03 1524.94 140.55 o -17 1 1 1643.42 1809.27 90.66 o -15 1 1 1345.78 1312.74 69.06 o -13 1 1 3318.96 3305.48 162.94 o -11 1 1 27421.48 28224.52 1011.90 o -9 1 1 28054.66 28387.50 1015.51 o -7 1 1 20772.18 21152.36 757.27 o -5 1 1 10688.33 7763.02 281.14 o -3 1 1 31338.32 25640.44 910.41 o -1 1 1 82686.78 57874.56 1671.67 o 1 1 1 32396.11 27294.58 790.09 o 3 1 1 43.08 271.52 20.78 o 5 1 1 1518.14 899.46 38.93 o 7 1 1 1631.46 1821.18 74.26 o 9 1 1 13.61 22.13 12.57 o 11 1 1 4160.40 3943.40 154.35 o 13 1 1 3120.41 3198.39 131.37 o 15 1 1 812.93 750.52 49.73 o 17 1 1 1569.15 1695.79 96.01 o -16 2 1 7.56 -34.70 34.70 o -14 2 1 1055.78 1118.08 59.68 o -12 2 1 612.13 658.28 45.83 o -10 2 1 0.83 -52.87 52.87 o -8 2 1 744.92 948.57 45.10 o -6 2 1 133.79 77.17 21.57 o -4 2 1 3910.72 3188.29 103.02 o -2 2 1 12797.22 13412.49 338.55 o 0 2 1 7768.43 8005.13 202.94 o 2 2 1 66202.42 62597.88 1568.09 o 4 2 1 220.43 309.88 18.29 o 6 2 1 224.01 312.26 16.65 o 8 2 1 370.80 392.52 21.29 o 10 2 1 128.59 132.90 16.67 o 12 2 1 2195.07 2114.95 91.30 o 14 2 1 91.50 113.61 26.62 o 16 2 1 1661.56 1582.97 120.04 o -15 3 1 3844.66 3847.24 229.76 o -13 3 1 7378.94 7798.81 423.41 o -11 3 1 943.05 811.20 50.01 o -9 3 1 17966.21 19385.50 570.09 o -7 3 1 19004.16 18558.34 544.55 o -5 3 1 31745.73 31696.23 798.53 o -3 3 1 31169.77 28779.18 724.56 o -1 3 1 13247.23 12034.10 305.14 o 1 3 1 6722.91 5992.54 153.90 o 3 3 1 10527.10 8720.30 221.97 o 5 3 1 27.33 20.67 7.15 o 7 3 1 45.90 19.35 9.69 o 9 3 1 1178.32 1086.55 42.91 o 11 3 1 154.00 207.06 29.34 o 13 3 1 1006.41 995.69 88.15 o 15 3 1 2838.68 3193.14 200.68 o -14 4 1 68.54 -13.36 35.17 o -12 4 1 336.17 439.54 44.19 o -10 4 1 3141.36 3280.97 136.15 o -8 4 1 214.37 138.12 25.32 o -6 4 1 1393.37 1459.95 53.88 o -4 4 1 94.19 95.41 40.44 o -2 4 1 1984.29 1888.67 53.53 o 0 4 1 4290.12 4180.70 110.45 o 2 4 1 311.94 352.47 15.45 o 4 4 1 10652.86 10246.18 304.64 o 6 4 1 490.47 444.95 25.66 o 8 4 1 863.54 1099.92 243.82 o 10 4 1 1632.36 1696.84 81.39 o 12 4 1 318.55 296.57 50.64 o 14 4 1 29.10 78.77 43.61 o -13 5 1 2755.15 2780.52 179.12 o -11 5 1 5217.27 5807.33 228.93 o -9 5 1 1966.58 1893.30 89.59 o -7 5 1 22096.43 23969.18 705.33 o -5 5 1 18243.55 18010.62 531.85 o -3 5 1 4659.51 4674.83 145.73 o -1 5 1 322.21 173.13 21.90 o 1 5 1 1656.81 1474.40 52.93 o 3 5 1 4220.61 3873.92 122.46 o 5 5 1 4578.89 4221.68 133.90 o 7 5 1 268.18 215.78 22.38 o 9 5 1 3.30 -16.48 21.00 o 11 5 1 376.34 271.94 37.12 o 13 5 1 1080.68 1176.21 105.03 o -12 6 1 87.12 40.96 56.38 o -10 6 1 574.16 711.15 53.54 o -8 6 1 19.06 -18.35 18.35 o -6 6 1 177.36 148.88 56.15 o -4 6 1 490.36 581.60 41.21 o -2 6 1 189.70 151.05 23.84 o 0 6 1 62.76 85.84 24.14 o 2 6 1 274.79 193.28 43.72 o 4 6 1 89.30 120.97 27.02 o 6 6 1 2677.56 2343.45 83.69 o 8 6 1 1653.78 1876.96 73.48 o 10 6 1 9.66 -2.70 30.83 o 12 6 1 369.34 333.38 61.89 o -9 7 1 2595.94 2840.30 188.49 o -7 7 1 1019.41 1238.27 104.56 o -5 7 1 5641.07 5880.94 229.62 o -3 7 1 3520.10 3345.12 139.72 o -1 7 1 2633.44 2443.54 107.41 o 1 7 1 1017.86 926.26 56.19 o 3 7 1 688.22 597.68 69.40 o 5 7 1 5.26 -0.93 23.37 o 7 7 1 25.09 -22.01 37.75 o 9 7 1 427.74 376.75 63.77 o -4 8 1 164.68 147.70 34.11 o -2 8 1 771.99 750.74 53.38 o 0 8 1 264.84 197.13 36.30 o 2 8 1 121.06 147.89 32.63 o 4 8 1 6.56 77.41 30.16 o -16 0 2 3198.05 3404.37 203.97 o -14 0 2 7001.95 6805.23 366.67 o -12 0 2 20123.03 20873.79 1066.25 o -10 0 2 10363.87 10194.60 528.91 o -8 0 2 7384.53 8211.90 425.75 o -6 0 2 15947.76 18327.96 927.46 o -4 0 2 1290.22 1495.76 82.52 o -2 0 2 13712.52 14185.79 713.18 o 2 0 2 19216.14 16216.31 814.93 o 4 0 2 133.25 128.94 16.88 o 6 0 2 25451.01 25219.93 1272.57 o 8 0 2 5638.84 6404.56 336.19 o 10 0 2 6061.62 5566.19 296.81 o 14 0 2 281.14 287.19 45.48 o 16 0 2 1435.47 1745.21 123.32 o -17 1 2 117.77 46.97 30.83 o -15 1 2 1776.56 1633.59 80.80 o -13 1 2 2015.58 1872.41 84.74 o -11 1 2 437.35 436.41 33.58 o -9 1 2 42.16 60.99 16.45 o -7 1 2 1610.21 1774.86 72.19 o -5 1 2 1117.02 1372.31 79.95 o -3 1 2 12860.59 15276.14 544.52 o -1 1 2 5573.56 3705.94 108.98 o 1 1 2 7504.53 6116.74 154.49 o 3 1 2 1208.83 2181.16 56.90 o 5 1 2 17621.59 19959.75 580.63 o 7 1 2 1652.88 1872.11 75.89 o 9 1 2 0.25 -10.28 11.25 o 11 1 2 3586.02 3614.81 143.19 o 13 1 2 19.15 17.97 41.26 o 15 1 2 196.29 268.10 33.44 o 17 1 2 175.75 270.48 39.68 o -16 2 2 3452.07 3690.40 226.94 o -14 2 2 5114.80 5289.40 296.46 o -12 2 2 7186.05 7153.96 269.08 o -10 2 2 15884.88 16874.17 610.35 o -8 2 2 2687.79 2979.30 116.64 o -6 2 2 3167.82 3099.98 118.10 o -4 2 2 201.40 127.72 11.81 o -2 2 2 2764.32 2464.70 74.89 o 0 2 2 90.91 48.18 5.79 o 2 2 2 7898.07 7899.86 232.45 o 4 2 2 17441.81 16367.03 412.84 o 6 2 2 1891.58 2063.37 66.35 o 8 2 2 4911.36 4545.52 139.52 o 10 2 2 5906.00 6634.12 236.74 o 12 2 2 520.73 353.96 30.96 o 14 2 2 3182.07 3608.34 212.88 o 16 2 2 451.33 497.96 66.11 o -15 3 2 20.09 24.62 43.61 o -13 3 2 3161.82 2898.68 177.24 o -11 3 2 60.74 102.95 26.49 o -9 3 2 2951.32 2948.10 117.47 o -7 3 2 8.89 -5.39 9.38 o -5 3 2 279.96 251.05 14.14 o -3 3 2 16322.21 17459.03 441.72 o -1 3 2 9.94 -10.21 15.43 o 1 3 2 4346.12 5058.14 130.50 o 3 3 2 16235.81 15600.51 456.69 o 5 3 2 7.14 -17.26 17.26 o 7 3 2 2341.54 2745.64 75.22 o 9 3 2 337.95 284.60 19.50 o 11 3 2 569.68 536.18 60.96 o 13 3 2 23.08 28.60 34.70 o 15 3 2 711.27 790.31 82.52 o -14 4 2 4045.53 3901.86 232.57 o -12 4 2 2545.68 2545.28 113.53 o -10 4 2 2717.98 2909.93 123.93 o -8 4 2 6320.85 6559.18 248.82 o -6 4 2 4782.96 5473.54 145.11 o -4 4 2 71.69 43.41 23.39 o -2 4 2 924.45 655.86 23.91 o 0 4 2 96.18 174.26 22.88 o 2 4 2 47.17 301.22 23.75 o 4 4 2 4665.34 5242.88 160.33 o 6 4 2 1396.96 1156.81 45.33 o 8 4 2 3182.56 3516.76 113.39 o 10 4 2 459.40 399.93 37.80 o 12 4 2 2622.87 2822.72 176.30 o 14 4 2 2450.04 2735.97 176.30 o -13 5 2 9.66 18.05 38.92 o -11 5 2 1972.28 1926.17 93.64 o -9 5 2 762.47 691.93 47.58 o -7 5 2 3016.87 2860.36 96.73 o -5 5 2 775.06 690.03 34.97 o -3 5 2 2071.62 1971.67 68.48 o -1 5 2 2.60 20.78 16.02 o 1 5 2 12.36 4.23 11.83 o 3 5 2 1418.71 1132.70 44.39 o 5 5 2 4.45 1.61 20.55 o 7 5 2 506.50 425.00 28.98 o 9 5 2 223.78 155.25 62.95 o 11 5 2 14.26 28.63 25.69 o 13 5 2 47.00 14.77 37.51 o -12 6 2 1051.55 1116.94 73.26 o -10 6 2 503.16 496.76 47.86 o -8 6 2 3499.89 3994.34 133.26 o -6 6 2 2579.67 2306.52 101.99 o -4 6 2 1650.37 1684.91 78.97 o -2 6 2 320.39 179.37 37.86 o 0 6 2 134.11 84.23 30.13 o 2 6 2 712.15 808.26 47.10 o 4 6 2 1.86 6.17 18.89 o 6 6 2 4577.39 4720.71 151.17 o 8 6 2 46.01 -32.35 32.35 o 10 6 2 474.48 531.16 56.97 o 12 6 2 703.91 783.05 84.87 o -9 7 2 1203.50 1247.48 107.38 o -7 7 2 465.28 402.48 44.52 o -5 7 2 1450.28 1473.31 78.14 o -3 7 2 698.69 753.14 79.24 o -1 7 2 185.96 122.84 26.17 o 1 7 2 187.25 170.45 28.50 o 3 7 2 1.32 -9.10 77.02 o 5 7 2 40.18 -9.09 20.48 o 7 7 2 24.76 -20.53 28.60 o 9 7 2 387.74 333.61 67.99 o -4 8 2 287.93 278.59 39.54 o -2 8 2 43.25 57.76 28.23 o 0 8 2 0.63 -0.37 26.14 o 2 8 2 82.11 17.23 26.19 o 4 8 2 46.80 30.85 25.93 o -17 1 3 1281.62 1262.07 72.36 o -15 1 3 2052.26 2275.45 102.18 o -13 1 3 5309.33 5647.84 218.04 o -11 1 3 5180.17 5508.12 210.18 o -9 1 3 535.62 428.70 29.67 o -7 1 3 465.03 491.56 28.28 o -5 1 3 6503.45 8020.49 290.35 o -3 1 3 4022.78 5130.66 186.15 o -1 1 3 10440.26 11155.85 324.20 o 1 1 3 22592.63 20314.07 588.65 o 3 1 3 12302.60 12524.99 315.41 o 5 1 3 8009.59 9172.23 269.43 o 7 1 3 26585.17 26777.54 779.34 o 9 1 3 19050.64 19062.43 558.45 o 11 1 3 9060.21 9498.09 624.56 o 13 1 3 4204.84 4350.61 171.47 o 15 1 3 2249.75 2121.30 97.34 o 17 1 3 1420.65 1379.50 74.60 o -16 2 3 35.65 -29.07 29.07 o -14 2 3 600.05 679.98 66.00 o -12 2 3 296.23 243.62 45.48 o -10 2 3 1865.42 2233.29 92.93 o -8 2 3 1376.41 1247.01 55.48 o -6 2 3 41.51 35.42 10.88 o -4 2 3 13722.40 17610.83 629.27 o -2 2 3 434.61 650.55 23.15 o 0 2 3 856.76 1161.36 37.03 o 2 2 3 10.65 26.86 7.87 o 4 2 3 410.51 325.85 12.61 o 6 2 3 2364.22 2416.96 76.52 o 8 2 3 5997.39 5668.45 171.57 o 10 2 3 649.32 668.01 31.45 o 12 2 3 1066.43 935.78 50.39 o 14 2 3 128.34 194.59 47.36 o 16 2 3 490.50 545.32 69.40 o -15 3 3 1738.67 1640.41 122.85 o -13 3 3 160.33 198.34 50.17 o -11 3 3 786.36 915.91 49.99 o -9 3 3 3239.68 4038.97 156.32 o -7 3 3 345.96 405.19 26.68 o -5 3 3 2188.09 2155.68 69.47 o -3 3 3 1877.31 2383.72 65.26 o -1 3 3 7399.07 8313.57 212.61 o 1 3 3 11068.26 12025.78 304.77 o 3 3 3 23577.51 24501.76 713.63 o 5 3 3 22064.90 20213.68 510.37 o 7 3 3 2937.48 3038.17 82.36 o 9 3 3 3967.73 3311.44 132.09 o 11 3 3 6795.19 6715.91 363.86 o 13 3 3 3422.95 2968.07 182.87 o 15 3 3 2197.40 2352.89 158.48 o -14 4 3 65.16 18.52 37.51 o -12 4 3 759.77 907.81 58.07 o -10 4 3 411.33 367.53 36.47 o -8 4 3 2334.23 2801.24 116.97 o -6 4 3 416.00 352.15 29.14 o -4 4 3 1190.99 1442.95 43.67 o -2 4 3 3113.26 2913.91 79.58 o 0 4 3 2898.73 2949.32 79.46 o 2 4 3 1759.76 1804.12 60.88 o 4 4 3 6239.97 6031.78 182.87 o 6 4 3 5714.82 5756.86 176.16 o 8 4 3 950.29 946.92 40.06 o 10 4 3 1705.46 1610.10 77.42 o 12 4 3 137.34 236.55 57.67 o 14 4 3 34.11 17.82 39.86 o -13 5 3 635.64 603.71 53.20 o -11 5 3 49.64 67.82 33.33 o -9 5 3 178.01 205.91 53.92 o -7 5 3 269.76 337.98 27.92 o -5 5 3 1465.59 1583.50 59.37 o -3 5 3 601.81 582.72 29.26 o -1 5 3 904.19 934.61 44.81 o 1 5 3 2662.13 2479.97 81.81 o 3 5 3 4212.43 4064.91 127.91 o 5 5 3 4253.41 4148.53 131.45 o 7 5 3 2144.74 1992.93 71.22 o 9 5 3 3758.62 3611.31 148.68 o 11 5 3 2640.65 2432.09 111.03 o 13 5 3 3727.85 3862.71 234.91 o -12 6 3 705.43 678.83 62.33 o -10 6 3 576.58 706.31 57.64 o -8 6 3 12.70 -4.06 69.86 o -6 6 3 967.62 1155.31 63.45 o -4 6 3 6.17 25.91 29.19 o -2 6 3 186.92 227.44 28.56 o 0 6 3 1991.48 1885.66 84.55 o 2 6 3 935.15 1007.88 53.27 o 4 6 3 601.73 623.03 34.15 o 6 6 3 1862.37 1823.42 68.80 o 8 6 3 3285.49 3216.65 136.60 o 10 6 3 839.72 785.05 57.26 o -9 7 3 119.71 182.40 55.80 o -7 7 3 138.14 113.66 30.30 o -5 7 3 28.84 79.92 68.46 o -3 7 3 192.93 188.70 32.60 o -1 7 3 740.42 670.86 47.89 o 1 7 3 1490.75 1318.12 68.39 o 3 7 3 1246.36 1051.85 59.28 o 5 7 3 557.07 450.88 46.65 o 7 7 3 2273.94 2001.92 142.54 o 9 7 3 354.17 396.45 72.21 o -4 8 3 466.10 438.42 45.32 o -2 8 3 89.05 115.62 35.31 o 0 8 3 450.80 419.27 70.33 o 2 8 3 1574.90 1559.27 80.71 o 4 8 3 731.94 716.31 53.53 o -16 0 4 155.66 108.78 41.73 o -14 0 4 5.85 46.65 35.64 o -12 0 4 696.67 798.28 66.11 o -10 0 4 2540.68 2348.20 137.38 o -8 0 4 1141.92 1642.75 97.53 o -6 0 4 4187.75 6108.69 317.91 o -4 0 4 30480.36 28834.13 1450.28 o -2 0 4 44133.76 42331.35 2122.66 o 0 0 4 8950.66 9861.69 497.02 o 2 0 4 44088.88 41042.84 2058.43 o 4 0 4 14991.31 12382.07 651.87 o 6 0 4 26816.17 24789.53 881.45 o 8 0 4 16011.99 15145.10 542.12 o 10 0 4 20420.18 19418.36 991.23 o 12 0 4 5817.18 6524.60 349.32 o 14 0 4 12468.79 11669.02 610.96 o 16 0 4 1740.39 2115.40 141.14 o -17 1 4 126.94 120.97 35.45 o -15 1 4 251.35 321.33 36.11 o -13 1 4 7.12 -15.83 15.83 o -11 1 4 18.15 -16.57 18.05 o -9 1 4 651.58 880.12 44.90 o -7 1 4 1168.19 1590.74 66.55 o -5 1 4 7027.01 7118.16 258.85 o -3 1 4 4860.78 5383.06 195.60 o -1 1 4 1312.45 1594.70 71.04 o 1 1 4 375.59 363.79 13.70 o 3 1 4 98.92 99.72 9.71 o 5 1 4 2966.07 3004.70 91.58 o 7 1 4 1807.86 1953.58 63.56 o 9 1 4 5413.15 5798.69 175.40 o 11 1 4 42.48 90.18 24.38 o 13 1 4 175.33 222.00 26.97 o 15 1 4 86.60 147.96 45.72 o 17 1 4 2.88 -30.01 30.01 o -16 2 4 1045.60 1027.40 61.72 o -14 2 4 115.80 85.79 25.91 o -12 2 4 48.28 24.58 19.51 o -10 2 4 157.10 157.34 21.62 o -8 2 4 900.87 849.13 42.46 o -6 2 4 11237.55 11504.76 416.06 o -4 2 4 2059.25 1643.50 65.12 o -2 2 4 133.83 256.76 100.25 o 2 2 4 1564.28 1162.65 39.42 o 4 2 4 40099.97 36675.92 920.80 o 6 2 4 37699.07 36142.23 908.43 o 8 2 4 42254.40 39345.50 1143.97 o 10 2 4 13735.38 13748.15 499.09 o 12 2 4 12068.52 11519.21 605.34 o 14 2 4 724.47 870.26 81.12 o 16 2 4 1438.57 1163.08 99.40 o -15 3 4 98.02 123.79 53.45 o -13 3 4 82.82 104.33 39.39 o -11 3 4 1427.15 1522.90 70.90 o -9 3 4 584.08 472.16 31.99 o -7 3 4 288.97 407.91 70.69 o -5 3 4 1995.36 2260.44 89.17 o -3 3 4 1235.67 1151.04 39.95 o -1 3 4 4345.79 4883.69 126.98 o 1 3 4 38.24 95.88 8.73 o 3 3 4 109.88 118.91 11.81 o 5 3 4 866.50 1035.37 31.39 o 7 3 4 2127.46 2405.12 66.58 o 9 3 4 1249.96 971.44 50.90 o 11 3 4 638.11 674.97 67.52 o 13 3 4 16.27 60.72 41.26 o 15 3 4 167.11 324.47 58.61 o -14 4 4 116.55 107.14 49.23 o -12 4 4 164.42 122.36 29.00 o -10 4 4 71.30 71.48 23.73 o -8 4 4 151.95 149.60 28.09 o -6 4 4 1460.37 1488.68 53.64 o -4 4 4 1185.24 1058.91 34.89 o -2 4 4 6507.92 5320.16 139.61 o 0 4 4 16210.05 14690.45 372.89 o 2 4 4 28817.83 24063.94 702.96 o 4 4 4 9321.12 8539.50 255.20 o 6 4 4 9842.24 9480.00 283.47 o 8 4 4 2667.55 3136.23 127.98 o 10 4 4 9495.62 8850.85 331.38 o 12 4 4 2917.46 3001.83 185.68 o 14 4 4 3275.47 3065.83 192.71 o -13 5 4 373.60 278.73 92.14 o -11 5 4 127.47 93.68 30.84 o -9 5 4 9.55 -5.76 70.92 o -7 5 4 100.32 23.95 24.38 o -5 5 4 11.07 13.63 14.10 o -3 5 4 112.03 157.50 17.41 o -1 5 4 80.09 44.51 26.26 o 1 5 4 1540.65 1609.60 57.12 o 3 5 4 3.86 -25.57 25.57 o 5 5 4 3614.74 3780.18 121.03 o 7 5 4 2634.72 2570.26 87.43 o 9 5 4 99.21 167.36 30.50 o 11 5 4 0.21 -16.88 32.82 o 13 5 4 0.36 46.65 42.67 o -10 6 4 1089.18 1200.69 71.56 o -8 6 4 1189.96 1299.06 105.97 o -6 6 4 458.76 618.48 71.04 o -4 6 4 1648.02 1657.79 79.06 o -2 6 4 1405.95 1488.72 103.16 o 0 6 4 2824.65 2414.41 102.61 o 2 6 4 4446.50 4276.68 167.91 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