(IUCr) Crystallography Journals Online checkcif report

[Contents scheme]
Acta Cryst. (2003). E59, m855-m858 [ doi:10.1107/S1600536803019160 ]
1-(4-Fluorobenzyl)pyridinium bis(maleonitriledithiolato)platinate(III)

X. Ren, J. Xie and Q. Meng

Online 11 September 2003
Key indicators

Single-crystal X-ray study
T = 293 K
Mean (C-C) = 0.023 Å
R factor = 0.052
wR factor = 0.135
Data-to-parameter ratio = 13.7
checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low .......       0.99       
PLAT342_ALERT_3_B Low Bond Precision on C-C bonds (x 1000) Ang ...         23       

Alert level C
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT165_ALERT_3_C Nr. of Status R Flagged Non-Hydrogen Atoms .....          6       
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C30     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C35     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C40     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C42     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C54     
PLAT241_ALERT_2_C Check High   U(eq) as Compared to Neighbors ....        C56     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C27     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C43     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C46     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C55     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....        C58     
PLAT242_ALERT_2_C Check Low    U(eq) as Compared to Neighbors ....         C4     
PLAT301_ALERT_3_C Main Residue  Disorder .........................       3.00 Perc. 
PLAT334_ALERT_2_C Small Av Benzene C-C Dist. C55    -   C60      =       1.34 Ang.  
PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond  C25    -   C26      =       1.36 Ang.  
PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond  C26    -   C27      =       1.34 Ang.  
PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond  C27    -   C28      =       1.39 Ang.  
PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond  C28    -   C29      =       1.32 Ang.  
PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond  C33    -   C34      =       1.32 Ang.  
PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond  C34    -   C35      =       1.36 Ang.  
PLAT366_ALERT_2_C Short? C(sp?)-C(sp?) Bond  C35    -   C36      =       1.34 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C1     -   C2       =       1.42 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C3     -   C4       =       1.46 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C5     -   C6       =       1.46 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C7     -   C8       =       1.42 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C9     -   C10      =       1.46 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C11    -   C12      =       1.44 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C13    -   C14      =       1.43 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C15    -   C16      =       1.42 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C17    -   C18      =       1.42 Ang.  
PLAT371_ALERT_2_C Long   C(sp2)-C(sp1) Bond  C21    -   C22      =       1.48 Ang.  
PLAT751_ALERT_4_C Bond    Calc     1.35800, Rep    1.358(6) ......  Senseless su    
              C37  -N14     1.555   1.555                                       
PLAT751_ALERT_4_C Bond    Calc     1.35854, Rep    1.358(6) ......  Senseless su    
              C37  -C38     1.555   1.555                                       
PLAT751_ALERT_4_C Bond    Calc     1.35762, Rep    1.358(6) ......  Senseless su    
              C38  -C39     1.555   1.555                                       
PLAT751_ALERT_4_C Bond    Calc     1.35800, Rep    1.358(6) ......  Senseless su    
              C39  -C40     1.555   1.555                                       
PLAT751_ALERT_4_C Bond    Calc     1.35868, Rep    1.358(6) ......  Senseless su    
              C40  -C41     1.555   1.555                                       
PLAT751_ALERT_4_C Bond    Calc     1.35735, Rep    1.358(6) ......  Senseless su    
              C41  -N14     1.555   1.555                                       

   0 ALERT level A = In general: serious problem
   2 ALERT level B = Potentially serious problem
  39 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
  30 ALERT type 2 Indicator that the structure model may be wrong or deficient
   4 ALERT type 3 Indicator that the structure quality may be low
   7 ALERT type 4 Improvement, methodology, query or suggestion