Acta Cryst. (2003). E59, m953-m954  [ doi:10.1107/S1600536803020385 ]

Bis(1,4,7-trithiacyclononane-³S,S',S'')iron(II) bis(perchlorate)

T. W. Green, J. A. Krause Bauer and W. B. Connick

Online 30 September 2003

Key indicators

• Single-crystal X-ray study
• T = 175 K
• Mean (C-C) = 0.003 Å
• R factor = 0.026
• wR factor = 0.065
• Data-to-parameter ratio = 20.1

checkCIF/PLATON results

No syntax errors found




Alert level B
PLAT029_ALERT_3_B _diffrn_measured_fraction_theta_full Low .......       0.98       

Alert level C
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ ....          ?
PLAT125_ALERT_4_C No _symmetry_space_group_name_Hall Given .......          ?
PLAT142_ALERT_4_C su on b - Axis Small or Missing (x 100000) .....         10 Ang.  
PLAT232_ALERT_2_C Hirshfeld Test Diff (M-X)  Fe2    -   S4       =       6.93 su    
PLAT790_ALERT_4_C Centre of Gravity not Within Unit Cell: Resd.  #          4       
              Cl O4                                                             

   0 ALERT level A = In general: serious problem
   1 ALERT level B = Potentially serious problem
   5 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   1 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   1 ALERT type 3 Indicator that the structure quality may be low
   3 ALERT type 4 Improvement, methodology, query or suggestion

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