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In the title compound, [Co(C11H15N2O2)2]Cl, the CoIII atom is six-coordinated by four N atoms and two O atoms from two Schiff base ligands, and is in a distorted octahedral geometry. The alcohol O atoms and the amine N atoms in the Schiff base and the chloride anions contribute to the formation of intermolec­ular hydrogen bonds.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S160053680301955X/ww6111sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S160053680301955X/ww6111Isup2.hkl
Contains datablock I

CCDC reference: 225662

Key indicators

  • Single-crystal X-ray study
  • T = 298 K
  • Mean [sigma](C-C) = 0.006 Å
  • R factor = 0.041
  • wR factor = 0.113
  • Data-to-parameter ratio = 14.0

checkCIF/PLATON results

No syntax errors found



Alert level C PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 3 N3 -CO1 -N1 -C1 147.00 3.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 8 N3 -CO1 -N1 -C8 -40.00 3.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 11 O1 -CO1 -N2 -C10 89.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 16 O1 -CO1 -N2 -C9 -37.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 23 N1 -CO1 -N3 -C12 153.00 3.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 28 N1 -CO1 -N3 -C19 -32.00 3.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 32 O3 -CO1 -N4 -C21 104.00 4.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 37 O3 -CO1 -N4 -C20 -21.00 5.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 44 N2 -CO1 -O1 -C3 39.00 2.00 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_C Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 50 N4 -CO1 -O3 -C14 25.00 5.00 1.555 1.555 1.555 1.555
0 ALERT level A = In general: serious problem 0 ALERT level B = Potentially serious problem 10 ALERT level C = Check and explain 0 ALERT level G = General alerts; check 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 0 ALERT type 3 Indicator that the structure quality may be low 10 ALERT type 4 Improvement, methodology, query or suggestion

Computing details top

Data collection: SMART (Siemens, 1996); cell refinement: SMART'; data reduction: SAINT (Siemens, 1996); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997a); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997a); molecular graphics: SHELXTL (Sheldrick, 1997b); software used to prepare material for publication: SHELXTL.

Bis(N-(2-(2-hydroxyethylamino)ethyl)salicylideneimine)cobalt(III) chloride top
Crystal data top
C22H30CoN4O4·ClF(000) = 1064
Mr = 508.88Dx = 1.477 Mg m3
Monoclinic, P21/nMo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 2ynCell parameters from 2737 reflections
a = 9.802 (5) Åθ = 2.3–22.8°
b = 24.879 (13) ŵ = 0.90 mm1
c = 10.425 (6) ÅT = 298 K
β = 115.849 (7)°Prism, dark red
V = 2288 (2) Å30.29 × 0.18 × 0.15 mm
Z = 4
Data collection top
Bruker SMART CCD area-detector
diffractometer
4049 independent reflections
Radiation source: fine-focus sealed tube2768 reflections with I > 2σ(I)
Graphite monochromatorRint = 0.047
φ and ω scansθmax = 25.0°, θmin = 1.6°
Absorption correction: multi-scan
(SADABS; Sheldrick, 1996)
h = 811
Tmin = 0.780, Tmax = 0.876k = 2925
12017 measured reflectionsl = 1212
Refinement top
Refinement on F2Primary atom site location: structure-invariant direct methods
Least-squares matrix: fullSecondary atom site location: difference Fourier map
R[F2 > 2σ(F2)] = 0.041Hydrogen site location: inferred from neighbouring sites
wR(F2) = 0.113H-atom parameters constrained
S = 0.97 w = 1/[σ2(Fo2) + (0.0578P)2]
where P = (Fo2 + 2Fc2)/3
4049 reflections(Δ/σ)max < 0.001
289 parametersΔρmax = 0.39 e Å3
0 restraintsΔρmin = 0.27 e Å3
Special details top

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F2 against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F2, conventional R-factors R are based on F, with F set to zero for negative F2. The threshold expression of F2 > σ(F2) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F2 are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Co10.75183 (5)0.135038 (17)0.63432 (5)0.03379 (16)
Cl10.00415 (14)0.01166 (4)0.19345 (13)0.0755 (4)
N10.6133 (3)0.08907 (10)0.4895 (3)0.0364 (7)
N20.9114 (3)0.09174 (10)0.6115 (3)0.0373 (7)
H20.94020.06540.67880.045*
N30.8936 (3)0.17848 (11)0.7821 (3)0.0340 (6)
N40.7550 (3)0.08869 (11)0.7951 (3)0.0402 (7)
H40.81720.06030.80420.048*
O10.5973 (3)0.17670 (9)0.6472 (2)0.0401 (6)
O21.2464 (3)0.05241 (13)0.7442 (3)0.0777 (9)
H2A1.18420.03280.75360.117*
O30.7494 (3)0.17986 (9)0.4868 (2)0.0394 (6)
O40.6915 (4)0.01987 (12)0.8842 (3)0.0823 (10)
H4B0.77710.01280.89350.123*
C10.4718 (4)0.09736 (14)0.4151 (4)0.0402 (9)
H10.41930.07360.34100.048*
C20.3881 (4)0.14035 (14)0.4374 (4)0.0385 (8)
C30.4556 (4)0.17789 (13)0.5503 (4)0.0372 (8)
C40.3618 (4)0.21856 (14)0.5607 (4)0.0464 (9)
H4A0.40270.24390.63320.056*
C50.2115 (5)0.22202 (16)0.4668 (5)0.0584 (11)
H50.15260.24980.47580.070*
C60.1466 (5)0.18460 (18)0.3588 (4)0.0614 (12)
H60.04410.18670.29660.074*
C70.2344 (4)0.14466 (16)0.3445 (4)0.0514 (10)
H70.19080.11980.27120.062*
C80.6864 (4)0.04386 (14)0.4562 (4)0.0499 (10)
H8A0.62530.03120.36000.060*
H8B0.70120.01450.52210.060*
C90.8361 (4)0.06480 (15)0.4706 (4)0.0505 (10)
H9A0.89840.03540.46490.061*
H9B0.82080.09010.39480.061*
C101.0506 (4)0.12009 (14)0.6284 (4)0.0490 (10)
H10A1.09170.13900.71880.059*
H10B1.02360.14680.55350.059*
C111.1733 (4)0.08457 (15)0.6236 (4)0.0498 (10)
H11A1.12870.06150.54040.060*
H11B1.24810.10710.61240.060*
C120.9281 (4)0.22699 (14)0.7692 (4)0.0377 (8)
H120.98320.24620.85250.045*
C130.8891 (4)0.25411 (13)0.6374 (4)0.0381 (8)
C140.8093 (4)0.22831 (13)0.5040 (4)0.0353 (8)
C150.7985 (4)0.25623 (15)0.3831 (4)0.0449 (9)
H150.75150.23970.29440.054*
C160.8553 (4)0.30731 (15)0.3921 (4)0.0498 (10)
H160.84530.32460.30930.060*
C170.9267 (5)0.33356 (15)0.5207 (4)0.0564 (11)
H170.96200.36850.52500.068*
C180.9444 (5)0.30718 (13)0.6410 (4)0.0481 (10)
H180.99420.32440.72850.058*
C190.9539 (4)0.15232 (15)0.9216 (4)0.0474 (10)
H19A0.99130.17900.99690.057*
H19B1.03680.12850.93300.057*
C200.8278 (5)0.12121 (15)0.9284 (4)0.0520 (10)
H20A0.75420.14550.93620.062*
H20B0.86640.09781.01100.062*
C210.6090 (4)0.06649 (16)0.7802 (4)0.0551 (11)
H21A0.55950.04890.68820.066*
H21B0.54480.09610.78060.066*
C220.6199 (5)0.02698 (17)0.8937 (4)0.0585 (11)
H22A0.67630.04300.98690.070*
H22B0.51900.01850.88310.070*
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Co10.0274 (3)0.0366 (3)0.0369 (3)0.0007 (2)0.0136 (2)0.0012 (2)
Cl10.0709 (8)0.0669 (7)0.0880 (8)0.0187 (6)0.0341 (7)0.0259 (6)
N10.0318 (17)0.0376 (16)0.0412 (16)0.0006 (13)0.0172 (14)0.0010 (13)
N20.0338 (17)0.0360 (16)0.0452 (17)0.0038 (13)0.0201 (14)0.0045 (13)
N30.0329 (16)0.0383 (16)0.0329 (15)0.0003 (13)0.0163 (13)0.0001 (12)
N40.0312 (17)0.0394 (17)0.0472 (18)0.0000 (13)0.0146 (14)0.0061 (14)
O10.0317 (14)0.0434 (14)0.0429 (14)0.0051 (11)0.0143 (12)0.0050 (11)
O20.0439 (19)0.100 (2)0.087 (2)0.0177 (17)0.0264 (17)0.0213 (19)
O30.0415 (15)0.0411 (14)0.0340 (13)0.0034 (11)0.0149 (11)0.0008 (10)
O40.082 (2)0.066 (2)0.095 (2)0.0066 (19)0.035 (2)0.0099 (18)
C10.036 (2)0.046 (2)0.037 (2)0.0059 (17)0.0152 (17)0.0003 (16)
C20.035 (2)0.044 (2)0.0370 (19)0.0005 (17)0.0160 (16)0.0062 (16)
C30.036 (2)0.038 (2)0.042 (2)0.0062 (17)0.0213 (18)0.0096 (16)
C40.041 (2)0.047 (2)0.056 (2)0.0060 (18)0.025 (2)0.0069 (18)
C50.047 (3)0.058 (3)0.077 (3)0.021 (2)0.033 (2)0.021 (2)
C60.034 (2)0.086 (3)0.056 (3)0.016 (2)0.013 (2)0.018 (2)
C70.039 (2)0.071 (3)0.040 (2)0.006 (2)0.0137 (19)0.0074 (19)
C80.040 (2)0.044 (2)0.063 (3)0.0042 (18)0.020 (2)0.0161 (19)
C90.042 (2)0.054 (2)0.059 (2)0.0027 (19)0.026 (2)0.0181 (19)
C100.040 (2)0.048 (2)0.066 (3)0.0028 (18)0.030 (2)0.0079 (19)
C110.037 (2)0.053 (2)0.066 (3)0.0048 (19)0.029 (2)0.008 (2)
C120.034 (2)0.044 (2)0.037 (2)0.0008 (17)0.0167 (16)0.0094 (16)
C130.039 (2)0.038 (2)0.042 (2)0.0042 (16)0.0217 (17)0.0028 (16)
C140.0264 (18)0.038 (2)0.042 (2)0.0060 (16)0.0158 (16)0.0024 (16)
C150.035 (2)0.057 (2)0.039 (2)0.0053 (18)0.0132 (17)0.0055 (18)
C160.047 (2)0.052 (3)0.054 (2)0.010 (2)0.025 (2)0.018 (2)
C170.067 (3)0.039 (2)0.070 (3)0.004 (2)0.035 (2)0.004 (2)
C180.057 (3)0.039 (2)0.054 (2)0.0011 (19)0.030 (2)0.0056 (18)
C190.048 (2)0.053 (2)0.034 (2)0.0040 (19)0.0110 (18)0.0002 (17)
C200.058 (3)0.056 (2)0.041 (2)0.004 (2)0.021 (2)0.0046 (18)
C210.039 (2)0.066 (3)0.059 (3)0.002 (2)0.021 (2)0.015 (2)
C220.047 (3)0.073 (3)0.055 (3)0.010 (2)0.021 (2)0.010 (2)
Geometric parameters (Å, º) top
Co1—O11.888 (2)C7—H70.9300
Co1—O31.891 (2)C8—C91.502 (5)
Co1—N31.899 (3)C8—H8A0.9700
Co1—N11.909 (3)C8—H8B0.9700
Co1—N21.997 (3)C9—H9A0.9700
Co1—N42.023 (3)C9—H9B0.9700
N1—C11.277 (4)C10—C111.510 (5)
N1—C81.454 (4)C10—H10A0.9700
N2—C101.477 (4)C10—H10B0.9700
N2—C91.485 (4)C11—H11A0.9700
N2—H20.9100C11—H11B0.9700
N3—C121.276 (4)C12—C131.425 (5)
N3—C191.463 (4)C12—H120.9300
N4—C211.477 (4)C13—C141.418 (5)
N4—C201.494 (4)C13—C181.422 (5)
N4—H40.9100C14—C151.402 (5)
O1—C31.314 (4)C15—C161.375 (5)
O2—C111.396 (4)C15—H150.9300
O2—H2A0.8200C16—C171.376 (5)
O3—C141.319 (4)C16—H160.9300
O4—C221.386 (5)C17—C181.359 (5)
O4—H4B0.8200C17—H170.9300
C1—C21.427 (5)C18—H180.9300
C1—H10.9300C19—C201.486 (5)
C2—C71.395 (5)C19—H19A0.9700
C2—C31.420 (5)C19—H19B0.9700
C3—C41.403 (5)C20—H20A0.9700
C4—C51.371 (5)C20—H20B0.9700
C4—H4A0.9300C21—C221.506 (5)
C5—C61.383 (5)C21—H21A0.9700
C5—H50.9300C21—H21B0.9700
C6—C71.364 (5)C22—H22A0.9700
C6—H60.9300C22—H22B0.9700
O1—Co1—O390.46 (10)N2—C9—C8107.3 (3)
O1—Co1—N387.48 (11)N2—C9—H9A110.2
O3—Co1—N393.97 (11)C8—C9—H9A110.2
O1—Co1—N193.97 (11)N2—C9—H9B110.2
O3—Co1—N187.57 (11)C8—C9—H9B110.2
N3—Co1—N1177.88 (11)H9A—C9—H9B108.5
O1—Co1—N2177.45 (10)N2—C10—C11115.1 (3)
O3—Co1—N287.37 (11)N2—C10—H10A108.5
N3—Co1—N293.98 (12)C11—C10—H10A108.5
N1—Co1—N284.62 (12)N2—C10—H10B108.5
O1—Co1—N488.68 (11)C11—C10—H10B108.5
O3—Co1—N4178.61 (10)H10A—C10—H10B107.5
N3—Co1—N484.90 (12)O2—C11—C10114.2 (3)
N1—Co1—N493.58 (12)O2—C11—H11A108.7
N2—Co1—N493.52 (11)C10—C11—H11A108.7
C1—N1—C8119.9 (3)O2—C11—H11B108.7
C1—N1—Co1126.4 (2)C10—C11—H11B108.7
C8—N1—Co1113.4 (2)H11A—C11—H11B107.6
C10—N2—C9111.6 (3)N3—C12—C13125.3 (3)
C10—N2—Co1117.3 (2)N3—C12—H12117.4
C9—N2—Co1106.5 (2)C13—C12—H12117.4
C10—N2—H2107.0C14—C13—C18119.2 (3)
C9—N2—H2107.0C14—C13—C12122.2 (3)
Co1—N2—H2107.0C18—C13—C12118.4 (3)
C12—N3—C19121.0 (3)O3—C14—C15118.4 (3)
C12—N3—Co1125.9 (2)O3—C14—C13124.7 (3)
C19—N3—Co1112.9 (2)C15—C14—C13116.8 (3)
C21—N4—C20110.4 (3)C16—C15—C14121.8 (4)
C21—N4—Co1117.5 (2)C16—C15—H15119.1
C20—N4—Co1106.9 (2)C14—C15—H15119.1
C21—N4—H4107.2C15—C16—C17121.6 (4)
C20—N4—H4107.2C15—C16—H16119.2
Co1—N4—H4107.2C17—C16—H16119.2
C3—O1—Co1124.7 (2)C18—C17—C16118.4 (4)
C11—O2—H2A109.5C18—C17—H17120.8
C14—O3—Co1125.6 (2)C16—C17—H17120.8
C22—O4—H4B109.5C17—C18—C13122.0 (4)
N1—C1—C2124.9 (3)C17—C18—H18119.0
N1—C1—H1117.6C13—C18—H18119.0
C2—C1—H1117.6N3—C19—C20107.2 (3)
C7—C2—C3119.8 (3)N3—C19—H19A110.3
C7—C2—C1117.9 (3)C20—C19—H19A110.3
C3—C2—C1122.3 (3)N3—C19—H19B110.3
O1—C3—C4117.8 (3)C20—C19—H19B110.3
O1—C3—C2125.2 (3)H19A—C19—H19B108.5
C4—C3—C2117.0 (3)C19—C20—N4107.9 (3)
C5—C4—C3121.8 (4)C19—C20—H20A110.1
C5—C4—H4A119.1N4—C20—H20A110.1
C3—C4—H4A119.1C19—C20—H20B110.1
C4—C5—C6120.6 (4)N4—C20—H20B110.1
C4—C5—H5119.7H20A—C20—H20B108.4
C6—C5—H5119.7N4—C21—C22115.3 (3)
C7—C6—C5119.4 (4)N4—C21—H21A108.4
C7—C6—H6120.3C22—C21—H21A108.4
C5—C6—H6120.3N4—C21—H21B108.4
C6—C7—C2121.4 (4)C22—C21—H21B108.4
C6—C7—H7119.3H21A—C21—H21B107.5
C2—C7—H7119.3O4—C22—C21110.9 (3)
N1—C8—C9105.6 (3)O4—C22—H22A109.5
N1—C8—H8A110.6C21—C22—H22A109.5
C9—C8—H8A110.6O4—C22—H22B109.5
N1—C8—H8B110.6C21—C22—H22B109.5
C9—C8—H8B110.6H22A—C22—H22B108.0
H8A—C8—H8B108.7
O1—Co1—N1—C113.9 (3)C8—N1—C1—C2179.8 (3)
O3—Co1—N1—C176.4 (3)Co1—N1—C1—C26.8 (5)
N3—Co1—N1—C1147 (3)N1—C1—C2—C7178.5 (3)
N2—Co1—N1—C1164.0 (3)N1—C1—C2—C32.1 (5)
N4—Co1—N1—C1102.8 (3)Co1—O1—C3—C4167.2 (2)
O1—Co1—N1—C8172.7 (2)Co1—O1—C3—C214.5 (5)
O3—Co1—N1—C897.0 (2)C7—C2—C3—O1177.4 (3)
N3—Co1—N1—C840 (3)C1—C2—C3—O12.1 (5)
N2—Co1—N1—C89.4 (2)C7—C2—C3—C40.9 (5)
N4—Co1—N1—C883.8 (2)C1—C2—C3—C4179.6 (3)
O1—Co1—N2—C1089 (2)O1—C3—C4—C5178.1 (3)
O3—Co1—N2—C1057.2 (3)C2—C3—C4—C50.3 (5)
N3—Co1—N2—C1036.6 (3)C3—C4—C5—C60.8 (6)
N1—Co1—N2—C10145.1 (3)C4—C5—C6—C71.3 (6)
N4—Co1—N2—C10121.7 (3)C5—C6—C7—C20.7 (6)
O1—Co1—N2—C937 (2)C3—C2—C7—C60.5 (5)
O3—Co1—N2—C968.6 (2)C1—C2—C7—C6179.9 (3)
N3—Co1—N2—C9162.4 (2)C1—N1—C8—C9138.6 (3)
N1—Co1—N2—C919.2 (2)Co1—N1—C8—C935.3 (3)
N4—Co1—N2—C9112.5 (2)C10—N2—C9—C8172.4 (3)
O1—Co1—N3—C1273.6 (3)Co1—N2—C9—C843.2 (3)
O3—Co1—N3—C1216.7 (3)N1—C8—C9—N250.8 (4)
N1—Co1—N3—C12153 (3)C9—N2—C10—C1162.1 (4)
N2—Co1—N3—C12104.3 (3)Co1—N2—C10—C11174.6 (3)
N4—Co1—N3—C12162.5 (3)N2—C10—C11—O272.0 (4)
O1—Co1—N3—C19101.2 (2)C19—N3—C12—C13172.9 (3)
O3—Co1—N3—C19168.5 (2)Co1—N3—C12—C1312.7 (5)
N1—Co1—N3—C1932 (3)N3—C12—C13—C141.9 (5)
N2—Co1—N3—C1980.9 (2)N3—C12—C13—C18176.0 (3)
N4—Co1—N3—C1912.3 (2)Co1—O3—C14—C15179.6 (2)
O1—Co1—N4—C2151.9 (3)Co1—O3—C14—C131.6 (5)
O3—Co1—N4—C21104 (4)C18—C13—C14—O3178.1 (3)
N3—Co1—N4—C21139.5 (3)C12—C13—C14—O37.8 (5)
N1—Co1—N4—C2142.0 (3)C18—C13—C14—C153.9 (5)
N2—Co1—N4—C21126.8 (3)C12—C13—C14—C15170.2 (3)
O1—Co1—N4—C2072.7 (2)O3—C14—C15—C16178.6 (3)
O3—Co1—N4—C2021 (5)C13—C14—C15—C163.3 (5)
N3—Co1—N4—C2014.9 (2)C14—C15—C16—C170.4 (6)
N1—Co1—N4—C20166.6 (2)C15—C16—C17—C181.9 (6)
N2—Co1—N4—C20108.6 (2)C16—C17—C18—C131.2 (6)
O3—Co1—O1—C370.3 (3)C14—C13—C18—C171.7 (6)
N3—Co1—O1—C3164.2 (3)C12—C13—C18—C17172.6 (4)
N1—Co1—O1—C317.3 (3)C12—N3—C19—C20138.1 (3)
N2—Co1—O1—C339 (2)Co1—N3—C19—C2037.0 (3)
N4—Co1—O1—C3110.8 (3)N3—C19—C20—N448.9 (4)
O1—Co1—O3—C1476.3 (3)C21—N4—C20—C19167.3 (3)
N3—Co1—O3—C1411.2 (3)Co1—N4—C20—C1938.5 (3)
N1—Co1—O3—C14170.3 (3)C20—N4—C21—C2264.3 (4)
N2—Co1—O3—C14105.0 (3)Co1—N4—C21—C22172.9 (3)
N4—Co1—O3—C1425 (5)N4—C21—C22—O467.1 (5)
Hydrogen-bond geometry (Å, º) top
D—H···AD—HH···AD···AD—H···A
N2—H2···Cl1i0.912.263.157 (3)168
N4—H4···Cl1i0.912.553.458 (3)172
O2—H2A···Cl1i0.822.343.154 (3)170
O4—H4B···Cl1i0.822.753.500 (4)154
Symmetry code: (i) x+1, y, z+1.
 

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