Acta Cryst. (2004). E60, o126-o128  [ doi:10.1107/S1600536803025170 ]

2'-(p-Chlorobenzoyl)-2,2',3,3',4',5',6',6a'-octahydro-1H-indan-2-spiro-3'-(1H-pyrrolizine)-1'-spiro-3''-indoline-1,2'',3-trione

P. R. Seshadri, S. Selvanayagam, D. Velmurugan, K. Ravikumar, A. R. Sureshbabu and R. Raghunathan

Online 24 December 2003

Key indicators

• Single-crystal X-ray study
• T = 293 K
• R factor = 0.051
• wR factor = 0.144
• Data-to-parameter ratio = 16.1

checkCIF/PLATON results

No syntax errors found



Alert level A
PLAT029_ALERT_3_A _diffrn_measured_fraction_theta_full Low .......       0.91       

Alert level C
REFLT03_ALERT_3_C  Reflection count < 95% complete
           From the CIF: _diffrn_reflns_theta_max           28.15
           From the CIF: _diffrn_reflns_theta_full           0.00
           From the CIF: _reflns_number_total               5223
           TEST2: Reflns within _diffrn_reflns_theta_max
           Count of symmetry unique reflns         5731
           Completeness (_total/calc)             91.14%
PLAT066_ALERT_1_C Predicted and Reported Transmissions Identical .          ?
PLAT152_ALERT_1_C Supplied and Calc Volume s.u. Inconsistent .....          ?
PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of .      35.00 A   3  

   1 ALERT level A = In general: serious problem
   0 ALERT level B = Potentially serious problem
   4 ALERT level C = Check and explain
   0 ALERT level G = General alerts; check

   2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   1 ALERT type 2 Indicator that the structure model may be wrong or deficient
   2 ALERT type 3 Indicator that the structure quality may be low
   0 ALERT type 4 Improvement, methodology, query or suggestion

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