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Acta Cryst. (2004). E60, i1-i2 [ doi:10.1107/S1600536803027375 ]
Na4Ni5[(As1-xPx)O4]2[(As2yP2-2y)O7]2 (x = 0.27 and y = 0.295)
R. Ben Smail and T. Jouini
Online 12 December 2003
Key indicators
- Single-crystal X-ray study
- T = 293 K
- Mean
![[sigma]](http://journals.iucr.org/logos/entities/sigma_rmgif.gif)
(Ni-O) = 0.003 Å
- Disorder in solvent or counterion
- R factor = 0.024
- wR factor = 0.065
- Data-to-parameter ratio = 10.4
checkCIF/PLATON results
No syntax errors found
Alert level C
PLAT041_ALERT_1_C Calc. and Rep. SumFormula Strings Differ .... ?
PLAT042_ALERT_1_C Calc. and Rep. MoietyFormula Strings Differ .... ?
PLAT045_ALERT_1_C Calculated and Reported Z Differ by ............ 0.50 Ratio
PLAT077_ALERT_4_C Unitcell contains non-integer number of atoms .. ?
PLAT128_ALERT_4_C Non-standard setting of Space group P21/c .... P21/a
PLAT301_ALERT_3_C Main Residue Disorder ......................... 9.00 Perc.
PLAT302_ALERT_4_C Anion/Solvent Disorder ......................... 33.00 Perc.
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P1
AS/P1 O8
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P1
AS/P1 O9
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P1
AS/P1 O6
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P1
AS/P1 O11
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P2
AS/P2 O10
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P2
AS/P2 O2
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P2
AS/P2 O7
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P2
AS/P2 O11
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P3
AS/P3 O4
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P3
AS/P3 O3
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P3
AS/P3 O1
PLAT711_ALERT_1_C BOND Unknown or Inconsistent Label .......... AS/P3
AS/P3 O5
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P1
O8 AS/P1 O9
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P1
O8 AS/P1 O6
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P1
O9 AS/P1 O6
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P1
O8 AS/P1 O11
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P1
O9 AS/P1 O11
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P1
O6 AS/P1 O11
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P2
O10 AS/P2 O2
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P2
O10 AS/P2 O7
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P2
O2 AS/P2 O7
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P2
O10 AS/P2 O11
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P2
O2 AS/P2 O11
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P2
O7 AS/P2 O11
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P3
O4 AS/P3 O3
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P3
O4 AS/P3 O1
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P3
O3 AS/P3 O1
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P3
O4 AS/P3 O5
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P3
O3 AS/P3 O5
PLAT712_ALERT_1_C ANGLE Unknown or Inconsistent Label .......... AS/P3
O1 AS/P3 O5
0 ALERT level A = In general: serious problem
0 ALERT level B = Potentially serious problem
37 ALERT level C = Check and explain
0 ALERT level G = General alerts; check
33 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
0 ALERT type 2 Indicator that the structure model may be wrong or deficient
1 ALERT type 3 Indicator that the structure quality may be low
3 ALERT type 4 Improvement, methodology, query or suggestion
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